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Application of Raman spectroscopy for identification of rinneite (K3NaFeCl6) in inclusions in minerals / S. Grishina, P. Kodera, S. Goryainov [et al.] // J. Raman Spectrosc. - 2020. - Vol. 51, Is. 12. - P. 2505-2516, DOI 10.1002/jrs.6005. - Cited References: 55. - Russian Foundation for Basic Research, Grant/Award Numbers: 18-05-00682, 18-05-00682; European Regional Development Fund, Grant/Award Number: ITMS 26240220086; Vedecka Grantova Agentura MSVVaS SR a SAV, Grant/Award Number: 1/0313/20 . - ISSN 0377-0486. - ISSN 1097-4555

РУБ Spectroscopy
Рубрики:
SALT MELT
   IRON
   DEPOSIT
   FLUIDS
   TRANSFORMATIONS
   FERRIHYDRITE
Кл.слова (ненормированные):
daughter mineral -- Fe-oxyhydroxides -- fluid inclusion -- rinneite -- weathering
Аннотация: Solid daughter phases in fluid and salt melt inclusions in minerals provide important clues to characterization of mineral‐forming processes. The analysis of the fluid inclusions often requires the exposure of the daughter minerals. Rinneite (K3NaFeCl6), which is a hygroscopic mineral, decomposes in air and cannot thus be identified by conventional methods. A combined approach has been applied for investigation of synthetic and natural rinneite to acquire its diagnostic Raman spectrum for a nondestructive identification. We used natural rinneite inclusions in halite, suitable for applying a complex of methods, to clear up the reference spectrum. Improved high‐resolution X‐ray diffraction (XRD) data obtained from natural rinneite inclusion are comparable with that of previously published, with similar unit cell dimensions. Polarized Raman spectra of natural inclusions were obtained using different geometries and polarization of the incident and scattered light. Interpretation of experimental Raman spectra was performed within the framework of lattice dynamics simulations and group analysis. Individual spectral bands are interpreted in terms of Raman‐active vibrational modes of K3NaFeCl6 structural units. Raman spectrum of synthetic rinneite with main peaks at 75, 91, 103, 143, 167, 171, 187, and 239 cm−1 agrees well with the spectra of rinneite inclusions in halite from the Nepa potash deposit and rinneite daughter minerals in salt melt inclusions hosted by quartz veinlets from the porphyry gold systems in the Central Slovakia Volcanic Field. This provides a firm basis for any future identification of this mineral worldwide, using nondestructive Raman spectroscopy.

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Держатели документа:
Russian Acad Sci, Sobolev Inst Geol & Mineral, Dept Mineral, Siberian Branch, Novosibirsk, Russia.
Comenius Univ, Dept Econ Geol, Fac Nat Sci, Bratislava, Slovakia.
Kirensky Inst Phys, Mol Spect Lab, Krasnoyarsk, Russia.
Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk, Russia.
Novosibirsk State Univ, Dept Geol, Novosibirsk, Russia.
Slovak Acad Sci, Inst Inorgan Chem, Bratislava, Slovakia.
Russian Acad Sci, Inst Geol Ore Deposits Petrog Mineral & Geochem, Moscow, Russia.

Доп.точки доступа:
Grishina, Svetlana; Kodera, Peter; Goryainov, Sergey; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Seryotkin, Yurii; Simko, Frantisek; Polozov, Alexander G.; Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [18-05-00682]; European Regional Development FundEuropean Union (EU) [ITMS 26240220086]; Vedecka Grantova Agentura MSVVaS SR a SAV [1/0313/20]
}
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    Atomic layer deposition ZnO on porous Al2O3 nanofibers film / A. S. Voronin, A. N. Masiygin, M. S. Molokeev, S. V. Khartov // J. Phys. Conf. Ser. - 2020. - Vol. 1679, Is. 2. - Ст. 022072DOI 10.1088/1742-6596/1679/2/022072. - Cited References: 10. - Studies by scanning electron microscopy and X-ray powder diffraction were performed on the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS». The transmission electron microscopy investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
   Перевод заглавия: Нанесение атомного слоя ZnO на пленку из пористых нановолокон Al2O3
Кл.слова (ненормированные):
Alumina -- Aluminum oxide -- Atomic layer deposition -- Atoms -- Composite structures -- High resolution transmission electron microscopy -- II-VI semiconductors -- Nanofibers -- Oxide minerals -- Scanning electron microscopy
Аннотация: The paper presents the results of the formation and study of the morphological and structural characteristics of the mesoporous ZnO / Al2O3 nanofibers film (ZANF). The deposition of a ZnO layer on Al2O3 nanofibers film (ANF) ~ 1 µm thick was carried out by the method of atomic layer deposition. The morphology of the mesoporous composite layer ZnO / Al2O3 (ZANF) has been studied by scanning and transmission electron microscopy. It is shown that in the process of atomic layer deposition, the ZnO layer grows according to the Stranski-Krastanov mechanism. A ZnO layer less than 5 nm thick gives an island structure in which Al2O3 nanofibers are uniformly coated with ZnO particles, an increase in the ZnO layer thickness to 15 nm demonstrates a continuous coating of Al2O3 nanofibers. The system has a core-shell structure. The resulting composite structures are promising for applications in photocatalysis and gas sensing.

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Держатели документа:
Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences (KSC SB RAS), Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Reshetnev Siberian State University Science and Technology, Krasnoyarsk, 660037, Russian Federation
Kirensky Institute of Physics (FRC KSC SB RAS), Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Voronin, A. S.; Masiygin, A. N.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Khartov, S. V.; International Scientific Conference on Applied Physics, Information Technologies and Engineering(2nd ; 25 September - 4 October 2020 ; Krasnoyarsk, Russian Federation)
}
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    Behavior of CaBSiO4(OH) datolite at high temperatures and pressures of a water medium / S. V. Goryainov [et al.] // Bull. Russ. Acad. Sci. Phys. - 2015. - Vol. 79, Is. 6. - P. 794-797, DOI 10.3103/S1062873815060118. - Cited References: 9. - This work was supported by the Russian Foundation for Basic Research, project nos. 13-05-00185 and 4-05-00616. . - ISSN 1062-8738
Рубрики:
Constant pressures
   Constant temperature
   High temperature
   Polymorphic transitions
   T parameter
   Tectonic plates
   Water mediums
   Silicate minerals
Аннотация: The behavior of CaBSiO4(OH) datolite compressed in a water medium at simultaneous high temperatures and pressures corresponding to the cold zones of tectonic plate subduction (up to P ~5.3 GPa and T ~250°C) is studied in situ via Raman spectroscopy. Two polymorphic transitions are found: (i) upon an increase of up to 2 GPa in pressure at a constant temperature of 22°C and (ii) upon heating to ~90°C at a constant pressure of ~5–5.3 GPa. Major trends of the variations in the Raman spectra are identified for all phases of the indicated P–T parameters. No overhydration and amorphization of datolite is observed. © 2015, Allerton Press, Inc.

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Публикация на русском языке Поведение датолита CaBSiO4(OH) при высоких температурах и давлениях водной среды [Текст] / С. В. Горяйнов [и др.] // Изв. РАН. Сер. физич. - 2015. - Т. 79 № 6. - С. 880–883

Держатели документа:
Sobolev Institute of Geology and Mineralogy, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russian Federation
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, Russian Federation
University of Saskatchewan, Saskatoon, SK, Canada

Доп.точки доступа:
Goryainov, S. V.; Krylov, A. S.; Крылов, Александр Сергеевич; Vtyurin, A. N.; Втюрин, Александр Николаевич; Pan, Y.
}
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    Colloidal and deposited products of the interaction of tetrachloroauric acid with hydrogen selenide and hydrogen sulfide in aqueous solutions / S. Vorobyev [et al.] // Minerals. - 2018. - Vol. 8, Is. 11. - Ст. 492, DOI 10.3390/min8110492. - Cited References: 63. - This research was funded by the Siberian Branch of the Russian Academy of sciences, Program of Interdisciplinary Studies, grant number 64 (project 303). . - ISSN 2075-163X
   Перевод заглавия: Коллоидные и осажденные продукты взаимодействия золотохлористоводородной кислоты с селеноводородом и сероводородом в водных растворах
Кл.слова (ненормированные):
Gold selenide -- Gold sulfoselenide -- Colloids -- Nanoparticles -- Nucleation -- Liquid intermediates -- Deposition
Аннотация: The reactions of aqueous gold complexes with H2Se and H2S are important for transportation and deposition of gold in nature and for synthesis of AuSe-based nanomaterials but are scantily understood. Here, we explored species formed at different proportions of HAuCl4, H2Se and H2S at room temperature using in situ UV-vis spectroscopy, dynamic light scattering (DLS), zeta-potential measurement and ex situ Transmission electron microscopy (TEM), electron diffraction, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and Raman spectroscopy. Metal gold colloids arose at the molar ratios H2Se(H2S)/HAuCl4 less than 2. At higher ratios, pre-nucleation “dense liquid” species having the hydrodynamic diameter of 20–40 nm, zeta potential −40 mV to −50 mV, and the indirect band gap less than 1 eV derived from the UV-vis spectra grow into submicrometer droplets over several hours, followed by fractional nucleation in the interior and coagulation of disordered gold chalcogenide. XPS found only one Au+ site (Au 4f7/2 at 85.4 eV) in deposited AuSe, surface layers of which partially decomposed yielding Au0 nanoparticles capped with elemental selenium. The liquid species became less dense, the gap approached 2 eV, and gold chalcogenide destabilized towards the decomposition with increasing H2S content. Therefore, the reactions proceed via the non-classical mechanism involving “dense droplets” of supersaturated solution and produce AuSe1−xSx/Au nanocomposites.

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Держатели документа:
Institute of Chemistry and Chemical Technology of the Siberian Branch of the Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Kirensky Institute of Physics of the Siberian Branch of the Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Electron Microscopy Laboratory, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Vorobyev, S.; Likhatski, M.; Romanchenko, A.; Maksimov, N.; Zharkov, S. M.; Жарков, Сергей Михайлович; Krylov, A. S.; Крылов, Александр Сергеевич; Mikhlin, Y.
}
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    Composition and Ligand Microstructure of Arsenopyrite from Gold Ore Deposits of the Yenisei Ridge (Eastern Siberia, Russia) / A. M. Sazonov [et al.] // Minerals. - 2019. - Vol. 9, Is. 12. - Ст. 737, DOI 10.3390/min9120737. - Cited References: 62. - The work was supported by the Russian Foundation for Basic Research (project number 19-35-90017) and the Government of the Russian Federation (project 14.Y26.31.0012). . - ISSN 2075-163X
   Перевод заглавия: Состав и лигандная микроструктура арсенопирита золоторудных месторождений Енисейского хребта (Восточная Сибирь, Россия)
Кл.слова (ненормированные):
arsenopyrite -- crystal lattice -- ligand surroundings -- non-equal positions -- Mössbauer Effect -- gold -- “invisible” gold -- gold ore deposits
Аннотация: The Mössbauer spectroscopy method was used to study the ligand microstructure of natural arsenopyrite (31 specimens) from the ores of the major gold deposits of the Yenisei Ridge (Eastern Siberia, Russia). Arsenopyrite and native gold are paragenetic minerals in the ore; meanwhile, arsenopyrite is frequently a gold carrier. We detected iron positions with variable distribution of sulfur and arsenic anions at the vertexes of the coordination octahedron {6S}, {5S1As}, {4S2As}, {3S3As}, {2S4As}, {1S5As}, {6As} in the mineral structure. Iron atoms with reduced local symmetry in tetrahedral cavities, as well as iron in the high-spin condition with a high local symmetry of the first coordination sphere, were identified. The configuration {3S3As} typical for the stoichiometric arsenopyrite is the most occupied. The occupation degree of other configurations is not subordinated to the statistic distribution and varies within a wide range. The presence of configurations {6S}, {3S3As}, {6As} and their variable occupation degree indicate that natural arsenopyrites are solid pyrite {6S}, arsenopyrite {3S3As}, and loellingite {6As} solutions, with the thermodynamic preference to the formation of configurations in the arsenopyrite–pyrite–loellingite order. It is assumed that in the variations as part of the coordination octahedron, the iron output to the tetrahedral positions and the presence of high-spin Fe cations depend on the physical and chemical conditions of the mineral formation. It was identified that the increased gold concentrations are typical for arsenopyrites with an elevated content of sulfur or arsenic and correlate with the increase of the occupation degree of configurations {5S1As}, {4S2As}, {1S5As}, reduction of the share of {3S3As}, and the amount of iron in tetrahedral cavities.

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Держатели документа:
Institute of Mining, Geology and Geotechnology, Siberian Federal University, 79 pr. Svobodny, 660041 Krasnoyarsk, Russia
Kirensky Institute of Physics, Federal Research Center Krasnoyarsk Scientific Center of the Siberian Branch of the Russian Academy of Sciences, 50 Bld. 38 Akademgorodok, 660036 Krasnoyarsk, Russia
Faculty of Geology and Geography, Tomsk National Research State University, 36 Lenina, 634050 Tomsk, Russia

Доп.точки доступа:
Sazonov, A. M.; Silyanov, S. A.; Bayukov, O. A.; Баюков, Олег Артемьевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Zvyagina, Y. A.; Tishin, P. A.
}
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Current-driven channel switching and colossal positive magnetoresistance in the manganite-based structure / N. V. Volkov [et al.] // J. Phys. D. - 2009. - Vol. 42, Is. 6. - Ст. 65005, DOI 10.1088/0022-3727/42/6/065005. - Cited References: 20. - This study was supported by the RFBR, Projects No 08-02-00259-a and 08-02-00397-a, the KRSF-RFBR 'Enisey-2007', Project No 07-02-96801-a and the Division of Physical Sciences of RAS, Program 'Spin-dependent Effects in Solids and Spintronics' (Project No 2.4.2 of SB RAS). . - ISSN 0022-3727

РУБ Physics, Applied

Кл.слова (ненормированные):
Colossal magnetoresistance -- Electric resistance -- Electronic structure -- Magnetic field effects -- Magnetoelectronics -- Manganese -- Manganites -- Oxide minerals -- Schottky barrier diodes -- Semiconductor junctions -- Silicides -- Tunnel junctions -- Tunnels -- Bottom layers -- Channel switching -- Conducting channels -- Conducting layers -- Current-driven -- Current-in-plane geometries -- Depletion layers -- Ferromagnetic state -- Layered structures -- Low-resistance contacts -- Magnetic tunnel junctions -- Magneto-transport properties -- Manganese silicides -- Manganite films -- New mechanisms -- Positive magnetoresistances -- Positive MR -- Potential barriers -- Spin-polarized -- Tunnel structures -- Voltage-current characteristics -- Current voltage characteristics
Аннотация: The transport and magnetotransport properties of a newly fabricated tunnel structure manganite/depletion layer/manganese silicide have been studied in the current-in-plane (CIP) geometry. A manganite depletion layer in the structure forms a potential barrier sandwiched between two conducting layers, one of manganite and the other of manganese silicide. The voltage-current characteristics of the structure are nonlinear due to switching conducting channels from an upper manganite film to a bottom, more conductive MnSi layer with an increase in the current applied to the structure. Bias current assists tunnelling of a carrier across the depletion layer; thus, a low-resistance contact between the current-carrying electrodes and the bottom layer is established. Below 30 K, both conducting layers are in the ferromagnetic state (magnetic tunnel junction), which allows control of the resistance of the tunnel junction and, consequently, switching of the conducting channels by the magnetic field. This provides a fundamentally new mechanism of magnetoresistance (MR) implementation in the magnetic layered structure with CIP geometry. MR of the structure under study depends on the bias current and can reach values greater than 400% in a magnetic field lower than 1 kOe. A positive MR value is related to peculiarities of the spin-polarized electronic structures of manganites and manganese silicides.

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Держатели документа:
[Volkov, N. V.
Eremin, E. V.
Tsikalov, V. S.
Patrin, G. S.
Kim, P. D.] SB RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Volkov, N. V.
Patrin, G. S.] Siberian Fed Univ, Dept Phys, Krasnoyarsk 660041, Russia
[Seong-Cho, Yu
Kim, Dong-Hyun] Chungbuk Natl Univ, Dept Phys, Cheongju 361763, South Korea
[Chau, Nguyen] Natl Univ Hanoi, Ctr Mat Sci, Hanoi, Vietnam
ИФ СО РАН
Kirensky Institute of Physics, SB RAS, Krasnoyarsk 660036, Russian Federation
Department of Physics, Siberian Federal University, Krasnoyarsk 660041, Russian Federation
Department of Physics, Chungbuk National University, Cheongju 361-763, South Korea
Center for Materials Science, National University of Hanoi, 334 Nguyen Trai, Hanoi, Viet Nam

Доп.точки доступа:
Volkov, N. V.; Волков, Никита Валентинович; Eremin, E. V.; Еремин, Евгений Владимирович; Tsikalov, V. S.; Patrin, G. S.; Патрин, Геннадий Семёнович; Kim, P. D.; Ким, Пётр Дементьевич; Seong-Cho, Y.; Kim, D. H.; Chau, N.; RFBR [08-02-00259-a, 08-02-00397-a]; KRSF-RFBR [07-02-96801-a]; Division of Physical Sciences of RAS; Program 'Spin-dependent Effects in Solids and Spintronics' [2.4.2]
}
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Effect of Heat Treatment on the Stability of Nanosized (Co40Fe40B20)34(SiO2)66/ZnO/In2O3 Multilayers / I. V. Babkina, M. N. Volochaev, O. V. Zhilova [et al.] // Bull. Russ. Acad. Sci. Phys. - 2020. - Vol. 84, Is. 9. - P. 1100-1103, DOI 10.3103/S1062873820090051. - Cited References: 11. - This work was supported by the RF Ministry of Science and Higher Education as part of State Task no. FZGM-2020-0007 . - ISSN 1062-8738
Кл.слова (ненормированные):
After-heat treatment -- Binary alloys -- Film preparation -- II-VI semiconductors -- Ion beams -- Magnetic semiconductors -- Multilayers -- Oxide minerals -- Semiconducting indium compounds -- Semiconducting silicon compounds -- Semiconducting zinc compounds -- Silica -- Silicon -- Sputtering -- Wide band gap semiconductors -- Zinc oxide
Аннотация: An investigation is performed of the thermal stability and phase transformations of thin-film heterogeneous [(Co40Fe40B20)34(SiO2)66/ZnO/In2O3]85 multilayers obtained via ion beam sputtering. The system contains 85 layers, each consisting of a (Co40Fe40B20)34(SiO2)66 composite layer and ZnO and In2O3 semiconductor spacers. The sample structure in the initial state and after heat treatment is studied by means of X-ray diffraction. It is shown that the samples are stable at temperatures of up to 500°С. Zn2SiO4, InBO3, CoFe, and In2O3 phases form during annealing.

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Публикация на русском языке Влияние термообработки на стабильность наноразмерных многослойных структур (Co40Fe40B20)34(SiO2)66/ZnO/In2O3 [Текст] / И. В. Бабкина, М. Н. Волочаев, О. В. Жилова [и др.] // Изв. РАН. Сер. физич. - 2020. - Т. 84 № 9. - С. 1293-1296

Держатели документа:
Voronezh State Technical University, Voronezh, 394026, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Babkina, I. V.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Zhilova, O. V.; Kalinin, Y. E.; Kashirin, M. A.; Sitnikov, A. V.; Chehonadskih, M. V.; Yanchenko, L. I.
}
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Val'kov, V. V.
Effect of pressure on antiferromagnetic and superconducting ordering in systems with heavy fermions / V. V. Val'kov, A. O. Zlotnikov // Bull. Russ. Acad. Sci.: Phys. - 2012. - Vol. 76, Is. 7. - P. 733-736, DOI 10.3103/S1062873812070362. - Cited References: 7. - This work was supported by the Department of Physical Sciences, Russian Academy of Sciences (the Strong Electron Correlations Program); the Russian Foundation for Basic Research, projects nos. 100200251 and 110200741; the RFBR Sibir’, project no. 110298007; and by the federal target program Scientific and Pedagogical Personnel of an Innovative Russia, 2009–2013. . - ISSN 0022-2860
Кл.слова (ненормированные):
Antiferromagnetic orderings -- Antiferromagnetic orders -- Antiferromagnetic phasis -- Antiferromagnetics -- Cooper instability -- Effect of pressure -- External pressures -- Heavy fermion -- Impurity level -- Localized state -- Periodic Anderson model -- Seed energy -- Spin moments -- Superconducting ordering -- Superexchange interaction -- Superconductivity -- Antiferromagnetism
Аннотация: Characteristics of the superconducting and antiferromagnetic phases of heavy-fermion intermet-allides are described within a periodic Anderson model with allowance for the superexchange interaction between spin moments of the localized states. It is shown that an external pressure that changes the seed energy of an impurity level can rapidly destroy the long-range antiferromagnetic order. The development of the Cooper instability near such an order-disorder transition induces the experimentally observed state in which superconductivity coexists with the antiferromagnetic ordering. В© 2012 Allerton Press, Inc.

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Публикация на русском языке Вальков, Валерий Владимирович. Влияние давления на антиферромагнитное и сверхпроводящее упорядочение в системах с тяжелыми фермионами [Текст] / В. В. Вальков, A. O. Злотников // Изв. РАН. Сер. физич. - 2012. - Т. 76 № 7. - С. 821-824

Доп.точки доступа:
Zlotnikov, A. O.; Злотников, Антон Олегович; Вальков, Валерий Владимирович; International Interdisciplinary Symposium “Ordering in Minerals and Alloys” (14th ; 8 -13 Sept. 2011 ; Rostov-on-Don)
}
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    Muzalevskiy, K. V.
    Effects of organo-mineral structure of arctic topsoil on the own thermal radiation in the L-band / K. V. Muzalevskiy, L. Yury // Int. Sib. Conf. on Control and Communicat. (SIBCON 2015) : Proceedings : IEEE-Institute Electrical and Electronics Engineers, 2015, DOI 10.1109/SIBCON.2015.7147152 . - ISBN 9781479971022 (ISBN)
   Перевод заглавия: Влияние органо-минеральной структуры верхнего слоя арктической почвы на собственное тепловое излучение в L-диапазоне"
Кл.слова (ненормированные):
Artic tundra -- Mineral soil -- Organic soil -- Permafrost -- SMOS -- Soil temperature -- Atmospheric humidity -- Balloons -- Heat radiation -- Landforms -- Luminance -- Minerals -- Permafrost -- Permittivity -- Radiation effects -- Soils -- Temperature -- Artic tundra -- Mineral soils -- Organic soil -- SMOS -- Soil temperature -- Soil surveys
Аннотация: In this paper, the influence of organic-mineral Arctic tundra soils on own thermal radiation in the L-band was theoretically investigated. For modeling of brightness temperature there were used semi-empirical L-band Microwave Emission of the Biosphere (L-MEB) model. An integral part of this model is permittivity models of tundra organic and mineral soils, which links the brightness temperature with moisture, temperature and density of soil. The permittivity models were developed based on the measurements of the organic rich and mineral soil samples collected at the Vaskiny Dachi weather station test-site in Yamal peninsular. As a result, the potential error of soil temperature retrieval in case of layered and homogeneous organic-mineral soil are shown based on simulated brightness temperature at 1.4 GHz. © 2015 IEEE.

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Доп.точки доступа:
Lukin, Y. I.; Лукин, Юрий Иванович; Музалевский, Константин Викторович; International Siberian Conference on Control and Communications(11 ; 2015 ; May 21-23 ; Omsk)
}
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10.

Formation of noble metal phases (Pt, Pd, Rh, Ru, Ir, Au, Ag) in the process of fractional crystallization of the CuFeS2 melt / E. F. Sinyakova, I. G. Vasilyeva, A. S. Oreshonkov [et al.] // Minerals. - 2022. - Vol. 12, Is. 9. - Ст. 1136, DOI 10.3390/min12091136. - Cited References: 61. - This work was supported by the Russian Federation state assignment of Sobolev Institute of Geology and Mineralogy of SB RAS, Nikolaev Institute of Inorganic Chemistry SB RAS, and Kirensky Institute of Physics of Federal Research Center KSC SB RAS. The grant number is projects II.1.64. and 40330-2016-0001 . - ISSN 2075-163X
Кл.слова (ненормированные):
Cu-Fe-S system -- noble metals -- directional crystallization -- intermediate solid solution -- fine inclusions
Аннотация: The quasi-equilibrium directional crystallization of the melt composition (at. %): Cu 24.998, Fe 25.001, S 49.983, with Ag 0.002, Pd 0.003, Ru 0.004, Rh 0.006, and Au, Pt, Ir (each as 0.001) was carried out. The crystallized cylindrical ingot consisted of two primary zones and three secondary zones with different chemical and phase compositions. The compositions of the primary zones corresponded to high-temperature intermediate solid solution (zone I) and liquid enriched in sulfur (zone II). The compositions of the secondary zones corresponded to low-temperature intermediate solid solution and chalcopyrite (zone Ia), the same intermediate solid solution with chalcopyrite and bornite (zone Ib), and again with bornite, chalcocite, and idaite (zone II). We plotted the distribution curves of Fe, Cu, and S along the ingot, calculated the distribution coefficients of the components during directional crystallization, and clearly showed that, from the initial stoichiometric composition CuFeS2, the intermediate solid solution enriched in Fe and depleted in S is crystallized. Based on the data of directional crystallization and thermal analysis, a cross section was constructed in the intermediate solid solution-sulfide melt region of the Cu-Fe-S system. With solubility in the solid Cu-Fe sulfides lying below detection limit of scanning electron microscopy/energy-dispersive X-ray spectrometry (SEM/EDS), noble elements occurred as individual phases of a size more often <10 µm. They were identified as Ag, RuS2, PdS, Au* (an Au based alloy), (Rh, Ir, Ru)3S8, (Rh, Ir)3S8, Rh3S8, and (Cu, Fe)~2(Pt, Rh)1S~5 phases by electron microprobe. Based on ab initio calculations of crystal structure, electronic band structure, and lattice dynamics of idealized laurite RuS2 phase and the idealized Ir3S8, Rh3S8, and Ru3S8 phases, the interpretation of Raman spectrum of the cation-mixed (Ru, Rh, Ir)S2 sulfide was presented for the first time.

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Держатели документа:
V.S. Sobolev Institute of Geology and Mineralogy, Siberian Branch of the Russian Academy of Sciences, pr. Akademika Koptyuga 3, Novosibirsk, 630090, Russian Federation
Nikolaev Institute of Inorganic Chemistry, Siberian Branch of the Russian Academy of Sciences, Ac. Lavrentieva ave. 3, Novosibirsk, 630090, Russian Federation
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
School of Engineering and Construction, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Sinyakova, E. F.; Vasilyeva, I. G.; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Goryainov, S. V.; Karmanov, N. S.
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