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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korotkov L. N., Stekleneva L. S., Flerov I. N., Mikhaleva E. A., Rysiakiewicz-Pasek E., Molokeev M. S., Bondarev I. A., Gorev M. V., Sysoev O. I.
Заглавие : X-Ray, Dielectric, and Thermophysical Studies of Rubidium Tetrachlorozincate inside Porous Glasses
Место публикации : Bull. Russ. Acad. Sci. Phys. - 2019. - Vol. 83, Is. 9. - P.1072-1076. - ISSN 10628738 (ISSN), DOI 10.3103/S1062873819090132
Примечания : Cited References: 17
Аннотация: Results are presented from studying the X-ray diffraction, heat capacities, dielectric permittivities, and coefficients of the volumetric thermal expansion of composite materials obtained by embedding of Rb2ZnCl4 salt into the porous matrices of borosilicate glass with average pore diameters of 46 and 320 nm in the temperature range of 120–350 K. The temperatures of transitions to the incommensurate and ferroelectric phases are determined, along with the freezing temperature of the mobility of domain boundaries in Rb2ZnCl4 particles. A substantial increase in their Curie temperature is observed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhlin Y., Vorobyev S., Romanchenko A., Karasev S., Karacharov A., Zharkov S. M.
Заглавие : Ultrafine particles derived from mineral processing: A case study of the Pb-Zn sulfide ore with emphasis on lead-bearing colloids
Место публикации : Chemosphere: Elsevier, 2016. - Vol. 147. - P.60-66. - ISSN 00456535 (ISSN), DOI 10.1016/j.chemosphere.2015.12.096
Примечания : Cited References: 47. - This research was supported by the Russian Science Foundation, Grant No. 14-17-00280.
Предметные рубрики: GALENA DISSOLUTION
METALLIC COPPER
NANOPARTICLES
SOIL
ENVIRONMENT
SEPARATION
TRANSPORT
FLOTATION
WATER
SIZE
Ключевые слова (''Своб.индексиров.''): lead sulfide--lead-zinc ore--lead sulfide--ultrafine particles--aquatic nanoparticles
Аннотация: Although mining and mineral processing industry is a vast source of heavy metal pollutants, the formation and behavior of micrometer- and nanometer-sized particles and their aqueous colloids entered the environment from the technological media has received insufficient attention to date. Here, the yield and characteristics of ultrafine mineral entities produced by routine grinding of the Pb-Zn sulfide ore (Gorevskoe ore deposit, Russia) were studied using laser diffraction analysis (LDA), dynamic light scattering (DLS) and zeta potential measurement, microscopy, X-ray photoelectron spectroscopy, with most attention given to toxic lead species. It was revealed, in particular, that the fraction of particles less that 1 ?m in the ground ore typical reaches 0.4 vol. %. The aquatic particles in supernatants were micrometer size aggregates with increased content of zinc, sulfur, calcium as compared with the bulk ore concentrations. The hydrodynamic diameter of the colloidal species decreased with time, with their zeta potentials remaining about -12 mV. The colloids produced from galena were composed of 20-50 nm PbS nanoparticles associated with lead sulfate and thiosulfate, while the surface oxidation products at precipitated galena were largely lead oxyhydroxides. The size and zeta potential of the lead-bearing colloids decreased with time down to about 100 nm and from -15 mV to -30 mV, respectively. And, conversely, lead sulfide nanoparticles were mobilized before the aggregates during redispersion of the precipitates in fresh portions of water. The potential environmental impact of the metal-bearing colloids, which is due to the large-scale production and relative stability, is discussed. © 2015 Elsevier Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volochaev M. N., Granovsky A. B., Zhilova O. V., Kalinin Y. E., Ryl'kov V. V., Sumets M. P., Makagonov V. A., Pankov S. Y., Sitnikov A. V., Fadeev E., Lahderanta E., Foshin V.
Заглавие : Transport and magnetic phenomena in ZnO-С thin-film heterostructures
Место публикации : Superlattices Microstruct. - 2020. - Vol. 140. - Ст.106449. - ISSN 07496036 (ISSN), DOI 10.1016/j.spmi.2020.106449
Примечания : Cited References: 36. - The work was supported by the Ministry of Education and Science of Russia (project No. 3.1867.2017/4.6 ) and the RFBR (project No. 19-07-00471). The work was partially funded by the Academy of Finland
Аннотация: ZnO- and C-based heterostructures were fabricated by the layer-by-layer deposition technique using the ion-beam sputtering process. Structure, electrical and magnetic properties of fabricated heterostructures are discussed. The two-phase (ZnO and C) films are evolved into a multilayer structure, consisting of amorphous carbon and crystalline ZnO layers when the bilayer thickness increases. When carbon is added to ZnO, its electrical resistivity reduces. The conduction mechanism changes from the variable-range hopping in a narrow energy band to the nearest neighbors hopping in ZnO–C films with a thickness of h ˂ 150 nm. The temperature dependence of conductivity changes from the Arrhenius-like to logarithmic law, indicating that the strong charge localization turns into a weak one when the film thickness is about 150 nm. The negative magnetoresistance of up to 1% was detected at 77 K. The film ferromagnetism at the temperature of 10 K was not found.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bikbaev R. G., Vetrov S. Ya., Timofeev I. V.
Заглавие : Transparent conductive oxides for the epsilon-near-zero Tamm plasmon polaritons
Место публикации : J. Opt. Soc. Am. B. - 2019. - Vol. 36, Is. 10. - P.2817-2823. - ISSN 07403224 (ISSN), DOI 10.1364/JOSAB.36.002817
Примечания : Cited References: 44. - The reported study was funded by RFBR according to the research project No 18-32-00053 and financial support RFBR and MOST according to the research project No 19-52-52006.
Аннотация: We demonstrate the possibility of using transparent conducting oxides [aluminum-doped zinc oxide (AZO), gallium-doped zinc oxide (GZO), indium tin oxide (ITO)] to form Tamm plasmon polaritons in the near-infrared spectral range where the permittivity of oxides is near zero. The spectral properties of the structures are investigated in the framework of the temporal coupled-mode theory and confirmed by the transfer matrix method. It is found that in the critical coupling conditions, the maximal Q-factor of a Tamm plasmon polariton is achieved when a photonic crystal is conjugated with the AZO film, while at the conjugation with the ITO films, the broadest spectral line is obtained. The sensitivity of the wavelength and spectral width of the Tamm plasmon polariton to changes in the oxide film thickness, bulk concentration of a dopant, and angle of incidence is demonstrated.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Li O. A., Edelman I. S., Chun-Rong Lin, Hung-Yi Chen, Kai-Wun Wu, Ovchinnikov S. G.
Заглавие : The unusual size dependence of magnetic properties of nickel zinc ferrite nanoparticles synthesized by combustion method
Коллективы : Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium, Институт физики им. Л.В. Киренского Сибирского отделения РАН
Место публикации : VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016): abstracts/ ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk: KIP RAS SB, 2016. - Ст.P9.5. - P.391. - ISBN 978-5-904603-06-9 (Шифр -478014040)
Ключевые слова (''Своб.индексиров.''): nickel zinc ferrite--ferrite nanoparticles --superparamagnetism
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Abylgazina L., Senkovska I., Ehrling S., Bon V., St. Petkov P., Evans J. D., Krylova S. N., Krylov A. S., Kaskel S.
Заглавие : Tailoring adsorption induced switchability of a pillared layer MOF by crystal size engineering
Место публикации : CrystEngComm. - 2021. - Vol. 23, Is. 3. - P.538-549. - ISSN 14668033 (ISSN), DOI 10.1039/d0ce01497d
Примечания : Cited References: 71. - The authors thank the DFG (FOR 2433 MOF Switches, Project No. 279409724) for financial support. P.P. and J. D. E. thank Center for Information Services and High Performance Computing (ZIH) at TU Dresden for providing high-performance computing facilities. Authors acknowledge Helmholtz-Zentrum Berlin für Materialien und Energie for allocated beamtime at KMC-2 and MX14.2 beamlines. J. D. E. acknowledges the support of the Alexander von Humboldt foundation and HPC platforms provided by a GENCI grant (A0070807069)
Аннотация: The pillared layer framework DUT-8(Zn) (Zn2(2,6-ndc)2(dabco), 2,6-ndc = 2,6-naphthalenedicarboxylate, dabco = 1,4-diazabicyclo-[2.2.2]-octane, DUT = Dresden University of Technology) is a prototypical switchable MOF, showing characteristic adsorption and desorption induced open phase (op) to closed phase (cp) transformation associated with huge changes in cell volume. We demonstrate switchability strongly depends on a framework-specific critical particle size (dcrit). Superposed, the solvent removal process (pore desolvation stress contracting the framework) significantly controls the cp/op ratio after desolvation and, subsequently, the adsorption induced switchability characteristics of the system. After desolvation, the dense cp phase of DUT-8(Zn) shows no adsorption-induced reopening and therefore is non-porous for N2 at 77 K and CO2 at 195 K. However, polar molecules with a higher adsorption enthalpy, such as chloromethane at 249 K and dichloromethane (DCM) at 298 K can reopen the macro-sized crystals upon adsorption. For macro-sized particles, the outer surface energy is negligible and only the type of metal (Zn, Co, Ni) controls the DCM-induced gate opening pressure. The node hinge stiffness increases from Zn to Ni as confirmed by DFT calculations, X-ray crystal structural analysis, and low frequency Raman spectroscopy. This softer Zn-based node hinges and overall increased stabilization of cp vs. op phase shift the critical particle size at which switchability starts to become suppressed to even lower values (dcrit ‹ 200 nm) as compared to the Ni-based system (dcrit ≈ 500 nm). Hence, the three factors affecting switchability (energetics of the empty host, (Eop–Ecp) (I), particle size (II), and desolvation stress (III)) appear to be of the same order of magnitude and should be considered collectively, not individually.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krinitsyn D. O., Romanchenko A. S., Vorob'ev S. A., Likhatskii M. N., Karacharov A. A., Krylov A. S., Volochaev M. N., Mikhlin, Yu L.
Заглавие : Synthesizing zinc sulfide films on the gold surface as the sensor for electrochemical quartz crystal microbalance
Коллективы : Russian Scientific FoundationRussian Science Foundation (RSF) [18-17-00135]
Место публикации : Russ. J. Electrochem. - 2021. - Vol. 57, Is. 12. - P.1157-1163. - ISSN 1023-1935, DOI 10.1134/S1023193521120041. - ISSN 1608-3342(eISSN)
Примечания : Cited References: 23. - The study was supported by the Russian Scientific Foundation (grant no. 18-17-00135)
Предметные рубрики: CHEMICAL BATH DEPOSITION
ZNS
SPHALERITE
ELECTRODES
ACTIVATION
Аннотация: A zinc sulfate film is deposited from aqueous solutions of zinc sulfate onto the gold surface with the aim of preparation of a sensor for electrochemical quartz crystal microbalance (EQCM). The kinetics of this process, the particles formed in solution, and the film itself are studied by the methods of electrochemical quartz crystal microbalance, X-ray photoelectron spectroscopy, transmission electron microscopy, atomic force microscopy, optical and Raman spectroscopies, and dynamic light scattering. The effect of the procedure of gold surface preparation, the reagent concentration, and the temperature on the film adhesion, the length of induction period, the kinetics of film growth, and its structure and thickness are studied. It is shown that the film formation proceeds as a result of deposition of sufficiently coarse 200-700 nm colloid particles of sphalerite. It is demonstrated that this sensor can be used in studying the electrochemical reactions of ZnS and the interface phenomena by the methods of EQCM and cyclic voltammetry.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tambasov I. A., Volochaev M. N., Voronin A. S., Evsevskaya N. P., Masyugin A. N., Aleksandrovskii A. S., Smolyarova T. E., Nemtsev I. V., Lyashchenko S. A., Bondarenko G. N., Tambasova E. V.
Заглавие : Structural, Optical, and Thermoelectric Properties of the ZnO:Al Films Synthesized by Atomic Layer Deposition
Место публикации : Phys. Solid State. - 2019. - Vol. 61, Is. 10. - P.1904-1909. - ISSN 10637834 (ISSN), DOI 10.1134/S1063783419100354
Примечания : Cited References: 33. - This study was supported by the Russian Science Foundation, project no. 17-72-10079.
Аннотация: Aluminum-doped zinc oxide thin films have been grown by atomic layer deposition at a temperature of 200°C. Using X-ray diffraction, it has been established that the ZnO:Al thin films exhibits the reflections from the (100), (002), (110), and (201) ZnO hexagonal phase planes. The (101) and (102) planes have also been detected by electron diffraction. The ZnO:Al thin films grow smooth with a root-mean-square roughness of Rq = 0.33 nm and characteristic nanocrystallite sizes of ~70 and ~15 nm without additional aluminum or aluminum oxide phases. The transmission at a wavelength of 550 nm with regard to the substrate has been found to be 96%. The refractive indices and absorption coefficients of the ZnO:Al thin films in the wavelength range of 250–900 nm have been determined. The maximum refractive indices and absorption coefficients have been found to be 2.09 at a wavelength of 335 nm and 0.39 at a wavelength of 295 nm, respectively. The optical band gap is 3.56 eV. The resistivity, Seebeck coefficient, and power factor of the ZnO:Al thin films are ∼1.02 × 10–3 Ω cm, –60 μV/K, and 340 μW m–1 K–2 at room temperature, respectively. The maximum power factor attains 620 μW m–1 K–2 at a temperature of 200°C.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Plotnikova A. A., Bragin V. I., Knyazev Yu. V.
Заглавие : Structural Characteristics and Processability of Sphalerite in Lead-Zinc Ore of the Gorevka Deposit
Место публикации : J. Min. Sci. - 2019. - Vol. 55, Is. 6. - P.995-1006. - ISSN 1062-7391, DOI 10.1134/S1062739119066381. - ISSN 1573-8736(eISSN)
Примечания : Cited References: 33
Аннотация: The theoretical and experimental substantiation of the behavior of ferrous sphalerite in magnetic separation is given in terms of the Gorevka deposit ore. In sphalerite of this deposit, the content of isomorphous iron ranges as 4-9%. The Mossbauer spectroscopy showed the singlet and two doublet lines of iron, demonstrating separate arrays of iron atoms in sphalerite lattice, with formation of Fe-Fe pairs and clusters of three or more iron atoms. It is found that distribution of iron in sphalerite into three forms coincides for magnetic and nonmagnetic products of zinc concentrate separation. It is determined that magnetic separation undivides sphalerite grains by the isomorphous iron content but is governed by the genetic features of the deposit formation-association of sphalerite with magnetic minerals (pyrrhotine and siderite) and the absence of such associations in galena.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Li O. A., Lin C. -R., Chen H. -Y., Hsu, Hua-Shu, Shih K. -Y., Edelman I. S., Wu K. -W., Tseng Y. -T., Ovchinnikov S. G., Lee J. -S.
Заглавие : Size dependent magnetic and magneto-optical properties of Ni0.2Zn0.8Fe2O4 nanoparticles
Место публикации : J. Magn. Magn. Mater.: Elsevier, 2016. - Vol. 408. - P.206-212. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2016.02.062
Примечания : Cited References: 51. - This work is supported by the Ministry of Science and Technology of Taiwan (MOST 103-2811-M-153 -001 and MOST 102-2112-M-153 -002 -MY3), and by the Russian Foundation for Basic Researches, grant No 14-02-01211.
Предметные рубрики: Zinc ferrite
Cation distribution
Sol-gel
Ni
ZnFe2O4
Spinel
Fe3O4
Particles
Spectra
State
Ключевые слова (''Своб.индексиров.''): nickel zinc ferrite--nanoparticles--magnetic properties--mcd
Аннотация: Ni0.2Zn0.8Fe2O4 spinel nanoparticles have been synthesized by combustion method. Average particles size varies from 15.5 to 50.0 nm depending on annealing temperature. Correlations between particles size and magnetic and magneto-optical properties are investigated. Magnetization dependences on temperature and external magnetic field correspond to the sum of paramagnetic and superparamagnetic response. Critical size of single-domain transition is found to be 15.9 nm. Magnetic circular dichroism (MCD) studies of nickel zinc spinel are presented here for the first time. The features in magnetic circular dichroism spectrum are assigned to the one-ion d-d transitions in Fe3+ and Ni2+ ions, as well to the intersublattice and intervalence charge transfer transitions. The MCD spectrum rearrangement was revealed with the change of the nanoparticles size. © 2016 Elsevier B.V. All rights reserved.
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