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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Laptash N. M., Gorev M. V., Pogoreltsev E. I.
Заглавие : Mixed-valence hydrated iron fluoridotitanate: synthesis, optics and calorimetry
Место публикации : J. Phys. Chem. Solids. - 2020. - Vol. 142. - Ст.109444. - ISSN 00223697 (ISSN), DOI 10.1016/j.jpcs.2020.109444
Примечания : Cited References: 35
Аннотация: Mixed-valence hydrated fluoridotitanate with idealized formula FeTiF6·6H2O is the main product of fluoride processing of natural mineral ilmenite with hydrofluoric acid. Its single crystals were grown and optical and calorimetric experiments were carried out in the temperature range 200–350 K. Charge re-distribution, Fe2+Ti4+ to Fe3+Ti3+, in the compound studied was evident in XPS spectra. A first order ferroelastic phase transition occurs at temperatures T0↓ = 271.5 K, T0↑ = 274 ÷ 275.5 K with the symmetry change P3‾↔ P1‾. The structural transformation is accompanied by the appearance of a very weak optical anisotropy in the slice (001), a small anomaly of the heat capacity (ΔS = 1.5 J/mol K = 0.2R), and positive baric coefficients dT0/dp ≈ 30 ± 10 K/GPa.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chen M., Nong S., Zhao Y., Riaz M. S., Xiao Y., Molokeev M. S., Huang F.
Заглавие : Renewable P-type zeolite for superior absorption of heavy metals: Isotherms, kinetics, and mechanism
Место публикации : Sci. Total Environ. - 2020. - Vol. 726. - Ст.138535. - ISSN 00489697 (ISSN), DOI 10.1016/j.scitotenv.2020.138535
Примечания : Cited References: 47. - This work was supported by the National Key Research and Development Program of China (Grant No. 2016YFB0901600 ); National Science Foundation of China (Grant No. 21871008 ); Science and Technology Commission of Shanghai Municipality (Grant No. 14520722000 ) and China Postdoctoral Science Foundation [Grant No. 8206300161 ]. Thank Shuying Nong for her experimental assistance
Аннотация: Zeolite is a characteristic material for removing heavy metals exhibiting by low tolerance quantities. It is particularly desirable although challenging to cultivate an unmodified and reusable zeolite for eradicating heavy metals with great capacity. Herein, we sought out and firstly synthesized the uniform octahedral zeolite Na6Al6Si10O32·12H2O for heavy metal ions trap, proven extraordinarily effective decontamination of M2+ (Pb2+, Cd2+, Cu2+, and Zn2+). The maximum capacities of Pb2+, Cd2+, Cu2+, and Zn2+ were 649, 210, 90 and 88 mg/g, and the distribution coefficients (Kd) was ~108 mL/g for Pb2+ which emphasized the superior effectiveness of Na6Al6Si10O32·12H2O contrasted with other zeolites. Rapid adsorption was observed that Pb2+ concentration (7.5 ppm) was reduced to 0.6 ppb in 2 min. The removal mechanism was ascribed to the ion exchange and hydroxyl groups thereby affording high adsorption capacity. We also investigated the heavy metal removal of zeolite 13X and 4A for comparison and concluded the determining factor affecting absorption capacity. The removal rate of Pb remained at 97% even after five regeneration recycles. The zeolite was therefore promising for practical water purification and industrialization.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Kartashev A. V., Bogdanov E. V., Flerov I. N., Laptash N. M.
Заглавие : Calorimetric, dilatometric and DTA under pressure studies of the phase transitions in elpasolite (NH4)2KZrF7
Место публикации : J. Fluor. Chem. - 2020. - Vol. 235. - Ст.109523. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2020.109523
Примечания : Cited References: 45. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: Heat capacity, thermal expansion, and sensitivity to the hydrostatic pressure of (NH4)2KZrF7 elpasolite are studied in a wide temperature range. The changes in deformation and entropy during successive phase transitions are determined: Δ(ΔV/V) = 3·10−4; ΔS = 8 J/mol K The temperatures and entropies of phase transitions turned out to be slightly sensitive to pressure changes. An analysis of the entropy of phase transformations was performed in the framework of the model of the cubic phase structure Fm-3 m. In the low temperature phase, an anomalous behavior of thermodynamic properties, which is not characteristic of phase transitions, was observed, accompanied by a significant change in the crystal lattice entropy.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Irtyugo L. A., Beletskii V. V., Belousova N. V., Denisov V. M.
Заглавие : Structure and thermodynamic properties of the SmGaGe2O7 oxide
Место публикации : Phys. Solid State. - 2020. - Vol. 62, Is. 2. - P.384-387. - ISSN 10637834 (ISSN), DOI 10.1134/S1063783420020109
Примечания : Cited References: 10. - This study was carried out within the state assignment of the Ministry of Science and Higher Education of the Russian Federation to the Siberian Federal University in 2017–2019, project no. 4.8083.2017/8.9 “Formation of a Data Bank of Thermodynamic Characteristics of the Complex-Oxide Multifunctional Materials Containing Rare and Scattered Elements.”
Аннотация: The SmGaGe2O7 oxide material has been obtained from initial Sm2O3, Ga2O3, and GeO2 oxides by solid-phase synthesis with annealing in air in the temperature range of 1273–1473 K. The structure of the investigated germanate (sp. gr. P21/c, a = 7.18610(9) Å, b = 6.57935(8) Å, and c = 12.7932(2) Å) has been established by X-ray diffraction and the high-temperature heat capacity has been determined by differential scanning calorimetry. Using the experimental data on Cp = f(T), the thermodynamic properties of the compound have been calculated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Kartashev A. V., Pogorel'tsev E. I., Laptash N. M.
Заглавие : Heat capacity, thermal expansion and barocaloric effect in fluoride K2TaF7
Место публикации : J. Mater. Sci. - 2019. - Vol. 54, Is. 23. - P.14287–14295. - ISSN 00222461 (ISSN), DOI 10.1007/s10853-019-03924-8
Примечания : Cited References: 20. - The reported study was funded by RFBR according to the research Project No. 18-02-00269_a.
Аннотация: The heat capacity and thermal expansion of potassium heptafluorotantalate were studied. The room temperature phase P21/c is stable at least to 4 K. The strong first-order phase transition P21/c−Pnma at T0=486.2K is accompanied by giant changes in the entropy, ΔS0=22.3J(molK)−1, and volume strain, δV0/V=−3.6%. A rather high sensitivity of K2TaF7 to pressure was found, dT0/dp=−220KGPa−1. Significant extensive and intensive barocaloric effects are found at low pressure. The possibility of improving the barocaloric properties is discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Бедарев В. А., Меренков Д. Н., Кобец М. И., Звягин А. А., Попережай С. Н., Гнатченко С. Л., Zajarniuk T., Vasevych T., Gutowska M. U., Szewczyk A., Гудим, Ирина Анатольевна
Заглавие : Проявление спиновых корреляций в монокристалле ErAl3(BO3)4
Место публикации : Физ. низких температур. - 2019. - Т. 45, № 9. - С. 1217-1222. - ISSN 0132-6414. - ISSN 1816-0328 (eISSN)
Примечания : Библиогр.: 15
Аннотация: Установлено наличие существенного магнитного вклада в удельную теплоемкость монокристалла ErAl3(BO3)4 при температурах менее 5 К. Результаты измерений спектров ЭПР при 4,2 К также свидетельствуют о проявлении ближнего магнитного порядка. Полученные данные обсуждаются в рамках модели, учитывающей спин-спиновое взаимодействие между редкоземельными ионами в парных кластерах.Встановлено присутність суттєвого магнітного внеску в питому теплоємність монокристалу ErAl3(BO3)4 при температурах нижче 5 К. Результати вимірювань спектрів ЕПР при температурі 4,2 К також свідчать про прояв близького магнітного порядку. Отримані дані обговорюються у рамках моделі, яка враховує спін-спінову взаємодію між рідкісноземельними іонами у парних кластерах.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Mikhashenok N. V., Soloviev L. A., Nazarenko I. I., Eremin E. V., Sofronova S. N.
Заглавие : Heat capacity, structural and magnetic properties of mixed-valence Pb3(Mn,Cu)7O15
Коллективы : Российская академия наук, Уральское отделение РАН, Институт физики металлов им. М. Н. Михеева Уральского отделения РАН, Уральский федеральный университет им. первого Президента России Б.Н. Ельцина, Российский фонд фундаментальных исследований, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : Euro-asian symposium "Trends in magnetism" (EASTMAG-2019): Book of abstracts/ чл. конс. ком.: S. G. Ovchinnikov, N. V. Volkov [et al.] ; чл. прогр. ком. D. M. Dzebisashvili [et al.]. - 2019. - Vol. 1. - Ст.G.03. - P.555. - ISBN 978-5-9500855-7-4 (Шифр В33/E12-125657784)
Примечания : Cited References: 2
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Molokeev M. S., Gorev M. V., Kartashev A. V., Laptash N. M., Flerov I. N.
Заглавие : Phase transition in RbCdZrF7: Structure and thermal properties
Место публикации : J. Fluor. Chem. - 2021. - Vol. 245. - Ст.109748. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2021.109748
Примечания : Cited References: 30. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: X-ray, calorimetric and dilatometric studies of RbCdZrF7 revealed the existence of the second order phase transition Cmcm - P21/m at T0 = 200 K. The structure of the initial and distorted phases is ordered. The phase transition is associated with displacements of fluorine atoms, which leads to minor rotations of the CdF7 and ZrF7 pentagonal bipyramids. A small change in entropy, 0.1R, is characteristic of displacive-type transformations. An anomalously high susceptibility of the transition temperature to hydrostatic pressure was found.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Nikolaev N. S., Elesina V. I., Glushenko G. A., Isakova V. G., Tomashevich Y. V.
Заглавие : Obtaining particles with the structure Mg@C and (Mg@C)@Pd, their properties and stability in the hydrogenation/dehydrogenation processes
Место публикации : Int. J. Hydrogen Energy. - 2022. - Vol. 47. Is. 11. - P.7299-7309. - ISSN 03603199 (ISSN), DOI 10.1016/j.ijhydene.2021.03.042
Примечания : Cited References: 46
Аннотация: In this work, we studied the change in the properties of powders with a core (magnesium) – shell structure (carbon and carbon/palladium) in the process of hydrogenation/dehydrogenation with hydrogen (99.995 wt%). Magnesium powders were obtained by plasma chemical synthesis in an atmosphere of argon containing a small amount of hydrogen (2–3 at.%) and nitrogen (8–9 at.%), when performing a low-frequency arc discharge between a tungsten electrode and a magnesium melt. The shell (carbon and carbon/palladium) was deposited in a plasma generator with vortex and magnetic stabilization. For all samples, a decrease in the sorption capacity of hydrogen was observed as a result of successive cycles of sorption and desorption reactions. It was found that the reason for this fall is associated with the formation of the MgO and Mg(OH)2 phase, which prevents the diffusion of hydrogen. The carbon shell provides a more complete hydrogenation of the magnesium particles, and an additional palladium shell increases the resistance to cyclic hydrogenation/dehydrogenation and reduces the temperature of these processes. According to the data obtained, powders with particles (Mg@C)@Pd can absorb the largest amount of hydrogen (6.9 wt%) for the duration of 5 cycles, after which the protective shell of the particles begins to collapse and a loss of sorption capacity is observed.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Ryabov V. V., Kargin Y. F., Chumilina L. G., Denisov V. M.
Заглавие : Crystal structure and thermodynamic properties of titanate ErGaTi2O7
Место публикации : Russ. J. Inorg. Chem. - 2021. - Vol. 66, Is. 4. - P.532-537. - ISSN 00360236 (ISSN), DOI 10.1134/S0036023621040082
Примечания : Cited References: 29
Аннотация: Erbium gallium titanate was prepared by solid-phase synthesis via the sequential calcination of precursor oxides in an air atmosphere at 1273 and 1573 K. The crystal structure of ErGaTi2O7 was characterized by full-profile analysis for the X-ray diffraction pattern of the synthesized powder sample as follows: space group Pcnb, a = 9.77326(15) Å, b = 13.5170(2) Å, c = 7.33189(11) Å, V = 918.58(3) Å3, ρ = 6.10 g/cm3. The high-temperature heat capacity of erbium gallium titanate was measured by differential scanning calorimetry within a temperature range of 320–1000 K. Based on these data, the basic thermodynamic functions of ErGaTi2O7 were calculated.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Chumilina L. G., Kargin Y. F., Denisov V. M., Ryabov V. V.
Заглавие : Synthesis, Crystal Structure and Thermodynamic Properties of LuGaTi2O7
Место публикации : Inorg. Mater. - 2020. - Vol. 56, Is. 12. - P.1242-1247. - ISSN 00201685 (ISSN), DOI 10.1134/S0020168520120055
Примечания : Cited References: 25
Аннотация: Single-phase LuGaTi2O7 samples have been prepared by solid-state reaction in a starting mixture of Lu2O3, Ga2O3, and TiO2 via sequential firing in air at temperatures of 1273 and 1573 K. The crystal structure of the lutetium gallium dititanate has been determined by the Rietveld method (profile analysis of X-ray diffraction patterns of polycrystalline powders): sp. gr. Pcnb; a = 9.75033(13) Å, b = 13.41425(17) Å, c = 7.29215(9) Å, V = 957.32(2) Å3, d = 6.28 g/cm3. The heat capacity of LuGaTi2O7 has been determined as a function of temperature by differential scanning calorimetry in the range 320–1000 K. The Cp(T) data thus obtained have been used to calculate the principal thermodynamic functions of the oxide compound.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Irtyugo L. A., Beletskii V. V., Kargin, Yu. F., Denisov V. M.
Заглавие : Synthesis, structure, and thermophysical properties of EuGaGe2O7
Место публикации : Inorg. Mater. - 2020. - Vol. 56, Is. 8. - P.854-858. - ISSN 0020-1685, DOI 10.1134/S002016852008004X. - ISSN 1608-3172(eISSN)
Примечания : Cited References: 18
Предметные рубрики: TEMPERATURE HEAT-CAPACITY
THERMODYNAMIC PROPERTIES
CRYSTAL-STRUCTURE
Аннотация: The europium gallium germanate EuGaGe2O7 has been prepared by solid-state reaction in air in the temperature range 1273–1473 K using a stoichiometric mixture of Eu2O3, Ga2O3, and GeO2. Its crystal structure has been determined by X-ray diffraction (sp. gr. P21/c, a = 7.1693(7) Å, b = 6.57008(6) Å, c = 12.7699(1) Å, β = 117.4522(5)°, V = 533.768(8) Å3). The heat capacity of polycrystalline samples has been determined by differential scanning calorimetry in the temperature range 350–1053 K and the experimental data have been used to calculate the thermodynamic properties (enthalpy increment, entropy change, and reduced Gibbs energy change) of EuGaGe2O7.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zobov V. E., Pichkovskiy I. S.
Заглавие : Associative memory on qutrits by means of quantum annealing
Место публикации : Quantum Inf. Process. - 2020. - Vol. 19, Is. 9. - Ст.342. - ISSN 1570-0755, DOI 10.1007/s11128-020-02851-x. - ISSN 1573-1332(eISSN)
Примечания : Cited References: 23
Аннотация: When associative memory is implemented on the well-studied Hopfield network, patterns are recorded in the interaction constants between binary neurons. These constants are chosen so that each pattern should have its own minimum energy of the system described by the Ising model. In the quantum version of the Hopfield network, it was proposed to recall such states by the adiabatic change of the Hamiltonian in time. Qubits, quantum elements with two states, for example, spins with S=1/2 were considered as neurons. In this paper, for the first time, we study the function of associative memory using three-level quantum elements-qutrits, represented by spins with S=1. We record patterns with the help of projection operators. This choice is due to the need to operate with a state with a zero spin projection, whose interaction with the magnetic field vanishes. We recall the state corresponding to one of the patterns recorded in the memory, or superposition of such states by means of quantum annealing. To equalize the probabilities of finding the system in different states of superposition, an auxiliary Hamiltonian is proposed, which is turned off at the end of evolution. Simulations were performed on two and three qutrits and an increase in the memory capacity after replacing qubits with qutrits was shown.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Molokeev M. S., Kartashev A. V., Pogoreltsev E. I., Mel'nikova S. V., Laptash N. M., Flerov I. N.
Заглавие : Investigation of thermal properties and structure of complex fluoride K3ZrF7
Место публикации : J. Fluor. Chem. - 2021. - Vol. 241. - Ст.109677. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2020.109677
Примечания : Cited References: 44. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: X-ray, calorimetric and dilatometric studies of K3ZrF7 revealed the existence of the phase transition Fm-3m ↔ R-3m at T0 = 320 K. The structural model assumes a disorder of a pentagonal bipyramid ZrF7 with the following ratio of equivalent orientation positions in the initial and distorted phases: 12 to 6. A good agreement was found between the experimental and model-calculated changes in strain and entropy during the phase transition. A comparative analysis of entropy and structural parameters of related fluorides K3ZrF7 - (NH4)2KZrF7 - (NH4)3ZrF7 was performed. The anomalous behavior of thermodynamic properties in the range 140−230 K is not typical for phase transitions and is accompanied by a significant change in the entropy of the crystal lattice.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pogoreltsev E. I., Mel'nikova S. V., Molokeev M. S., Flerov I. N., Laptash N. M.
Заглавие : Structural, thermal and optical properties of elpasolite-like (NH4)2KZrF7
Место публикации : J. Solid State Chem. - 2019. - Vol. 277. - P.376-380. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2019.06.013
Примечания : Cited References: 28. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a . The authors are grateful to Krasnoyarsk Center of collective use of SB RAS for providing X-ray analytical equipment.
Аннотация: New fluoride compound (NH4)2KZrF7 with the elpasolite structure (sp. gr. Fm-3m) was synthesized by partial cationic substitution in (NH4)3ZrF7 cryolite. Due to small difference in ionic radii of K+ and NH4+, non-equivalent crystallographic positions 8c and 4b are occupied by both cations. Investigations of thermal, optical and structural properties in a wide range of temperature revealed two phase transitions Fm-3m ↔ P42/ncm ↔ P42/nmc of the first order. The results obtained are discussed in comparison with the data for the previously studied related cryolite (NH4)3ZrF7.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : MELERO J. J., BARTOLOME J., BURRIEL R., ALEKSANDROVA I. P., PRIMAK S.
Заглавие : HEAT-CAPACITY MEASUREMENT OF THE SUCCESSIVE PHASE-TRANSITIONS IN CS2ZNI4
Разночтения заглавия :us: Heat capacity measurement of the successive phase transitions in Cs2ZnI4
Место публикации : Solid State Commun.: PERGAMON-ELSEVIER SCIENCE LTD, 1995. - Vol. 95, Is. 4. - P201-206. - ISSN 0038-1098, DOI 10.1016/0038-1098(95)00261-8
Примечания : Cited References: 20
Предметные рубрики: INCOMMENSURATE PHASE
SEQUENCE
CRYSTALS
CS2CDI4
Ключевые слова (''Своб.индексиров.''): ferroelectrics--heat capacity--phase transitions--incommensurate phases
Аннотация: The heat capacity of a Cs2ZnI4 single crystal has been measured by means of AC calorimetry. Three anomalies have been detected corresponding to a normal to inconmensurate phase transition at T-I = 116.9+/-0.1 K, an incommensurate to commensurate lock-in transition at T-L = 107.58+/-0.05 K, and a structural transition from a commensurate orthorhombic to a monoclinic phase at T-C = 93.77+/-0.05 K with thermal hysteresis. The lock-in transition has the peculiarity of being discontinuous but not showing any measurable hysteresis. After comparison with the Landau model predictions for the heat capacity, derived for the k(Delta) = (1/2 + Delta)a* case, it is concluded that Cs2ZnI4 lies close to the Lifschitz point of coexistence of the normal, incommensurate and commensurate phases.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pankrats A. I., Petrakovskii G. A., Kartashev A., Eremin E. V., Temerov V. L.
Заглавие : Low-temperature magnetic phase diagram of HoFe3(BO3)(4) holmium ferroborate: a magnetic and heat capacity study
Разночтения заглавия :авие SCOPUS: Low-temperature magnetic phase diagram of HoFe3(BO 3)4 holmium ferroborate: A magnetic and heat capacity study
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2009. - Vol. 21, Is. 43. - Ст.436001. - ISSN 0953-8984, DOI 10.1088/0953-8984/21/43/436001
Примечания : Cited References: 20
Предметные рубрики: SINGLE-CRYSTAL
DYFE3(BO3)(4)
ND3+
Ключевые слова (''Своб.индексиров.''): antiferromagnetic state--applied magnetic fields--characteristic temperature--crystal axis--heat capacities--low temperatures--magnetic field parallel--magnetic phase diagrams--magnetic phase transitions--magnetization jump--schottky anomaly--spin reorientation transitions--thermal measurements--antiferromagnetic materials--antiferromagnetism--holmium--magnetic fields--phase diagrams--single crystals--specific heat--phase transitions
Аннотация: We present the results of the magnetic and heat capacity study of a magnetic phase diagram of a HoFe3(BO3)(4) single crystal. Two magnetic phase transitions are found in the low-temperature region. The transition from the paramagnetic to easy-plane antiferromagnetic state occurs at T-N = 37.4 K and is independent of an applied magnetic field. The sharp heat capacity peaks and magnetization jumps corresponding to the spontaneous and field-induced spin-reorientation transitions between the easy-axis and easy-plane states are observed below 4.7 K. Also, the additional heat capacity peaks, which can be attributed to the Schottky anomalies with the field-dependent characteristic temperatures, are found. According to the magnetic and thermal measurement data, the magnetic phase diagrams of HoFe3(BO3)(4) for the magnetic field parallel and perpendicular to the crystal axis are constructed.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Bondarev V. S., Flerov I. N., Maglione M., Simon A., Sciau P., Boulos M., Guillemet-Fritsch S.
Заглавие : Thermal expansion, polarization and phase diagrams of Ba1-yBi2y/3Ti1-xZrxO3 and Ba1-yLayTi1-y/4O3 compounds
Коллективы : Russian Foundation for Basic Research [07-02-00069]; Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools [NSh-1011.2008.2]
Разночтения заглавия :авие SCOPUS: Thermal expansion, polarization and phase diagrams of Ba 1-yBi2y/3Ti1-xZrxO3 and Ba1-yLayTi1-y/4O3 compounds
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2009. - Vol. 21, Is. 7. - Ст.75902. - С. P. - ISSN 0953-8984, DOI 10.1088/0953-8984/21/7/075902
Примечания : Cited References: 28. - This work was supported by the Russian Foundation for Basic Research ( project no. 07-02-00069) and the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools ( project no. NSh-1011.2008.2).
Предметные рубрики: HEAT-CAPACITY
CERAMICS
BA(TI1-XZRX)O-3
FERROELECTRICS
BEHAVIOR
BATIO3
BATI0.65ZR0.35O3
CONDUCTIVITY
PEROVSKITES
CHEMISTRY
Ключевые слова (''Своб.индексиров.''): barium--dielectric properties--lanthanum--phase diagrams--polarization--thermal stress--zirconium--ceramic compositions--root mean squares--temperature ranges--temperature-dependent measurements--thermal expansion co-efficient--thermal-expansion properties--thermal expansion
Аннотация: The thermal expansion properties of the ceramic compositions Ba1-yLayTi1-y/4O3 (y = 0.0, 0.026, 0.036, 0.054) and Ba1-yBi2y/3Ti1-xZrxO3 (y = 0.10; x = 0.0, 0.04, 0.05, 0.10, 0.15) were determined in the temperature range 120-700 K. We report the temperature- dependent measurements of the strain, thermal expansion coefficient and the magnitude of root mean square polarization. The results obtained are discussed together with the data on the structure and dielectric properties.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M., Bondarev V., Sciau P., Savariault J. M.
Заглавие : Heat capacity study of relaxors BaTi0.65Zr0.35O3 and BaTi0.60Zr0.40O3
Разночтения заглавия :авие SCOPUS: Heat capacity study of relaxors BaTi0.65Zr0.35O 3 and BaTi0.60Zr0.40O3
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2006. - Vol. 18, Is. 17. - P.4407-4416. - ISSN 0953-8984, DOI 10.1088/0953-8984/18/17/026
Примечания : Cited References: 21
Предметные рубрики: CERAMICS
BA(TI1-XZRX)O-3
BATIO3
Ключевые слова (''Своб.индексиров.''): calorimetry--composition--data reduction--lead compounds--mathematical models--permittivity--specific heat--adiabatic calorimetry--burns temperature--diffuse anomalies--barium compounds
Аннотация: The heat capacity of two relaxors BaTi(1-x)ZrxO(3) (x = 0.35, 0.40) was measured using adiabatic calorimetry in the temperature range 100-360 K. The Cp(T) dependence of both compositions is characterized by the presence of two diffuse anomalies near the Burns temperature T-d and the temperature of the maximum in permittivity T-m in the temperature ranges 250-350 K and 120 200 K. The anomalous heat capacity near T-d was analysed taking into account the distribution of Zr concentration in nanoregions leading to the distribution of their transition temperatures into the polar phase. Excess heat capacity near Tm was discussed in the framework of the spherical random bond-random field model. The results are compared with the data obtained by the same procedures for PbMg1/3Nb2/3O3 studied experimentally earlier.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Flerov I. N., Sciau P.
Заглавие : Heat capacity and the p-T phase diagram of Pb2MgTeO6 elpasolite
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2001. - Vol. 43, Is. 2. - P345-349. - ISSN 1063-7834, DOI 10.1134/1.1349486
Примечания : Cited References: 17
Предметные рубрики: ORDERED PEROVSKITE PB2MGTEO6
CRYSTAL-STRUCTURE
PB2COWO6
PB2MGWO6
Аннотация: The heat capacity of Pb2MgTeO6 is measured in the temperature range 80-300 K. It is found that the heat capacity exhibits an anomaly associated with the phase transition at T-0 = 186.9 K. The thermodynamic parameters of the structural transformation are determined. The effect of hydrostatic pressure up to 0.5 GPa on the phase transition temperature is examined. (C) 2001 MAIK "Nauka/Interperiodica".
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