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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Дрокина, Тамара Васильевна, Петраковский, Герман Антонович, Молокеев, Максим Сергеевич, Великанов, Дмитрий Анатольевич, Плетнев, Олег Николаевич, Баюков, Олег Артемьевич
Заглавие : Особенности кристаллической структуры и магнитные свойства соединения DyFeTi2O7
Место публикации : Физ. тверд. тела. - 2013. - Т. 55, Вып. 10. - С. 1922-1927
Аннотация: Представлены результаты исследования особенностей кристаллической структуры и распределения катионов железа по позициям в соединении DyFeTi2O7, проведено сравнение с изоструктурным соединением GdGaTi2O7. Методами мессбауэровской спектроскопии и рентгеновской дифракции подтвержден атомный беспорядок в распределении ионов железа Fe3+ по структурным позициям в DyFeTi2O7. Результаты магнитных измерений в низкотемпературной области показывают излом на температурной зависимости магнитного момента и его зависимость от магнитной предыстории образца. Полученные экспериментальные данные позволяют сделать вывод о реализации состояния спинового стекла с температурой замерзания Tf=6 K в соединении DyFeTi2O7
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Drokina T. V., Petrakovskii G. A., Molokeev M. S., Velikanov D. A., Pletnev N. O., Bayukov O. A.
Заглавие : Specific features of the crystal structure and magnetic properties of the DyFeTi2O7 compound
Место публикации : Phys. Solid State. - 2013. - Vol. 55, Is. 10. - P.2037-2042. - ISSN 1063-7834, DOI 10.1134/S1063783413100107
Аннотация: Results of studying the specific features of formation of the crystal structure and distribution of iron cations over the sites in the DyFeTi2O7 compound have been presented and the comparison with the GdGaTi2O7 isostructural compound has been performed. The atomic disorder in the distribution of the Fe3+ ions over structural sites in the DyFeTi2O7 compound is confirmed by the Mossbauer spectroscopy and X-ray diffractometry. The results of magnetic measurements in the low-temperature region have revealed an inflection point in the temperature dependence of the magnetic moment and its dependence on the magnetic prehistory of the sample. The obtained experimental data suggest that there is a spin glass state with freezing point Tf = 6 K in the DyFeTi2O7 compound. В© 2013 Pleiades Publishing, Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Val'kov V. V., Zlotnikov A. O.
Заглавие : Coexistence of superconductivity and antiferromagnetism in heavy-fermion intermetallic compound CeRhIn5
Место публикации : J. Supercond. Nov. Magn. - 2013. - Vol. 26, Is. 9. - P.2885-2886. - ISSN 1557-1939, DOI 10.1007/s10948-013-2222-4
Ключевые слова (''Своб.индексиров.''): coexistence superconductivity antiferromagnetism--heavy-fermion systems--periodic anderson model
Аннотация: An interference of heavy-fermion superconductivity (SC) and antiferromagnetism (AFM) has been studied in the framework of the periodic Anderson model with the superexchange interaction between localized electrons. It has been shown that pressure-induced energy change of the localized states leads to modifying antiferromagnetic and superconducting order parameters. Conditions have been found for the coexistence of SC and AFM in the model. Theoretical results of the pressure effects on the ground state character of the heavy-fermion systems are in good agreement with experimental data for a rare-earth intermetallic compound CeRhIn5. The divergence of the effective electron mass produced by suppressing the long-range antiferromagnetic order has also been analyzed in the same framework. В© 2013 Springer Science+Business Media New York.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Yakinci Z. D., Gokhfeld D. M., Altin E., Kurt F., Altin S., Demirel S., Aksan M. A., Yakinci M. E.
Заглавие : Jc enhancement and flux pinning of Se substituted YBCO compound
Место публикации : J. Mater. Sci.: Mater. Electron.: Springer, 2013. - Vol. 24. - P.4790–4797. - ISSN 0957-4522, DOI 10.1007/s10854-013-1476-8
Примечания : The work is supported by Project No. 7 of RAS Program ‘"Quantum physics of condensed matter"
Аннотация: Y2/3 Se1/3Ba2Cu3Ox compound was fabricated by using solid state fabrication technique. Optimum heat treatments conditions for Y0.77Se0.33Ba2Cu3Ox were investigated. It was determined that the XRD results of these samples were similar to Y-123 phase with some impurities. Magnetization dependence of applied magnetic fields was measured in the range of 0-9В T at 10-50В K. The symmetric and asymmetric M-H loops were obtained for the samples. Magnetization loops obtained from measurements were successfully described by the extended Valkov-Khrustalev model. The temperature and applied magnetic field dependencies of magnetization of sample were estimated and critical current density of samples was calculated by Bean model and pinning force of samples was calculated by using Lorentz force. It is found from critical current density values that Se additions were acted as a pinning center which increased critical current density. В© 2013 Springer Science+Business Media New York.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrakovskii G. A., Drokina T. V., Velikanov D. A., Bayukov O. A., Molokeev M. S., Kartashev A. V., Shadrina A. L., Mitsuk A. A.
Заглавие : Magnetic state of the GdFeTi2O7 compound
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2012. - Vol. 54, Is. 9. - P.1813-1816. - ISSN 1063-7834, DOI 10.1134/S1063783412090235
Примечания : Cited References: 11
Предметные рубрики: SPIN-GLASS
GD
SM
Аннотация: The X-ray diffraction, Mossbauer, calorimetric, and magnetic characteristics of zirconolite GdFeTi2O7 have been measured to determine the ground magnetic state. A kink dependent on the magnetic prehistory of the sample has been revealed in the temperature dependence of the magnetic moment at T = 3 K. Mossbauer spectroscopy has confirmed the nonequivalence of the iron ion positions in GdFeTi2O7. The experimental data obtained allow the conclusion on the formation of a spin glass state with the freezing temperature T (f) = 3 K in the GdFeTi2O7 compound.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Drokina T. V., Petrakovskii G. A., Velikanov D. A., Molokeev M. S.
Заглавие : Specific features of magnetic ordering in the SmFeGe2O7 compound
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2014. - Vol. 56, Is. 6. - P.1131-1136. - ISSN 1063-7834, DOI 10.1134/S1063783414060122. - ISSN 1090-6460
Примечания : Cited References: 10
Предметные рубрики: NEUTRON-DIFFRACTION
PR
FERGE2O7
R=LA
Аннотация: The results of the experimental investigation of the magnetic properties of the SmFeGe2O7 compound have been presented. It has been found that the temperature dependence of the susceptibility exhibits two features that coincide with the anomalies in the temperature dependence of the specific heat and indicate magnetic phase transitions in SmFeGe2O7. The external magnetic field induces a magnetic transition, the critical field of which depends on the temperature.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronkov M. G., Zel'bst E. A., Vasil'ev A. D., Molokeev M. S., Kuznetsova G. A.
Заглавие : Oxatrane is a parent compound of a new atrane family: Crystal and molecular structure of triethanolamine N-oxide
Коллективы : Council for Grants of the President of the Russian Federation for Support of Leading Scientific Schools [NSh-3649.2014.3]
Место публикации : Dokl. Chem.: Pleiades Publishing, 2014. - Vol. 458. - P.172-175. - ISSN 0012-5008, DOI 10.1134/S0012500814090031. - ISSN 1608-3113
Примечания : This work was supported by the Council for Grants of the President of the Russian Federation for Support of Leading Scientific Schools (grant no. NSh-3649.2014.3).
Предметные рубрики: TERTIARY-AMINES
DIETHANOLAMINE
SILATRANES
OXIDATION
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aver'yanov E. M.
Заглавие : Structural and thermodynamic consequencies of the interaction of conformational degrees of freedom of azomethines in the nematic phase
Место публикации : J. Struct. Chem.: Springer, 2014. - Vol. 55, Is. 4. - P.605-611. - ISSN 0022-4766, DOI 10.1134/S0022476614040039. - ISSN 1573-8779
Примечания : Cited References: 21
Предметные рубрики: CONJUGATED POLY(AZOMETHINE)S
TERMINAL SUBSTITUENTS
ELECTRONIC-STRUCTURES
FLUORINATED ANALOGS
INTERNAL-ROTATION
MOLECULES
COMPOUND
ANGLES
STATE
NMR
Ключевые слова (''Своб.индексиров.''): azomethines--benzylideneaniline--conformation--steric effects of substituents--nematic-isotropic liquid transition--conformational polymorphism
Аннотация: The interaction of the conformational degrees of freedom of azomethines in the nematic phase, which is induced by electronic donor-acceptor properties of the terminal substituents of the benzylideneaniline core is studied. These degrees of freedom related to the rotation angles phi (k) around the bonds between the substituent and the aniline ring (phi(1)) and also between the CH=N bridge and the aniline ring (omega(2)) are characterized by the parameters Q (k) = aOE (c) cos(2)phi (k) . It is found that the interaction of these degrees of freedom is manifested in the linear dependence Q (2)(Q (1)). Within the phenomenological theory the effect of this interaction on changes delta (k) in the Q (k) values during the nematic liquid crystal-isotropic liquid phase transition is revealed along with the temperature T (NI) and character of this transition. The derivation of previously established empirical dependences T (NI)(Q (k) ) is presented in the presence of direct and indirect steric effects of side substituents affecting the Q (k) values. A diverse combination of delta (k) signs in the nematic phase, which is a prerequisite for the conformational polymorphism of the nematic phases of azomethines, is shown.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kuzubov A. A., Eliseeva N. S., Krasnov P. O., Kuklin A. V., Kovaleva E. A., Kholtobina A. S.
Заглавие : Theoretical investigation of the adsorption and diffusion of hydrogen on the surface and in the bulk of the intermetallic compound Mg2Ni
Место публикации : Phys. Solid State: Pleiades Publishing, 2014. - Vol. 56, Is. 10. - P.2035-2042. - ISSN 1063-7834, DOI 10.1134/S1063783414100187. - ISSN 1090-6460
Примечания : Cited References: 30
Предметные рубрики: STORAGE MATERIAL Mg2NiH4
INITIO MOLECULAR-DYNAMICS
AUGMENTED-WAVE METHOD
MINIMUM ENERGY PATHS
ELASTIC BAND METHOD
TEMPERATURE STRUCTURE
SADDLE-POINTS
ALLOYS
TRANSITION
MAGNESIUM
Аннотация: The intermetallic compound Mg2Ni as a potential material for hydrogen storage has been investigated theoretically. The sorption and diffusion of a hydrogen atom in the bulk and on the surface of this material, as well as the step-by-step process of dissociative chemisorption of a H-2 molecule on the surface, have been considered. The dependence of the sorption energy of atomic hydrogen on the structural characteristics of the intermetallic compound Mg2Ni has been analyzed.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Golovnev N. N., Molokeev M. S., Sterkhova I. V., Goryunov Y. V., Atuchin V. V.
Заглавие : New class of bicyclic compounds derived from thiobarbituric acid with representative compound 1,3-diethyl-7-hydroxy-5,5,7-trimethyl-2-thioxo-1,2,3,5,6,7-hexahydro-4H-pyrano[2,3-d]pyrimidin-4-one. Preparation, crystal structure, mass spectrometry and IR spectroscopy
Место публикации : J. Mol. Struct.: Elsevier, 2015. - Vol. 1102. - P.101-107. - ISSN 0022-2860, DOI 10.1016/j.molstruc.2015.08.046
Примечания : Cited References: 40. - The work was carried out within the public task of the Ministry of Education and Science of the Russian Federation for research engineering of the Siberian Federal University in 2015 (Contract 3049). V.V.A. is grateful to the Ministry of Education and Science of the Russian Federation for the financial support of the investigation (Contract 14.607.21.0106). The authors also thank SFU CEJU for the technical support
Предметные рубрики: 1,3-diethyl-2-thiobarbituric acid
Crystal-structure
2-thiobarbituric acid
Barbituric-acid
Hydrogen-bond
Derivatives
Diffraction
Equilibria
Inhibitors
Series
Ключевые слова (''Своб.индексиров.''): bicyclic compounds--thiobarbiturates--heterocycles--x-ray diffraction--ir spectroscopy--theoretical calculations
Аннотация: The colorless crystals of 1,3-diethyl-7-hydroxy-5,5,7-trimethyl-2-thioxo-1,2,3,5,6,7-hexahydro-4H-pyrano[2,3-d]pyrimidin-4-one (1) have been crystallized from the solution containing 1,3-diethyl-2-thiobarbituric acid (HDETBA) and equal volumes of concentrated HCl and acetone A possible stoichiometric reaction mechanism has been suggested. The crystal structure of 1 has been determined by X-ray single crystal analysis. The phase purity of the precipitate has been verified by powder X-ray diffraction analysis. Compound 1 crystallizes in the orthorhombic structure, space group P212121, with cell parameters a = 9.7454(4), b = 11.2225(4), c = 13.9171(5) Å, Z = 4, V = 1522.1(1) Å3. The molecules of 1 contain the bicyclic ring constructions new in thiobarbiturates. The molecules of 1 are linked by O-H...O hydrogen bonds to infinite molecule chains. The results of mass spectrometric analysis, theoretical studies and IR spectroscopy confirm the structure of 1. Using the PASS software, the general pharmacological potential of 1 was analyzed.
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