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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krasikov A. A., Balaev D. A., Balaev A. D., Stolyar S. V., Yaroslavtsev R. N., Iskhakov R. S.
Заглавие : Separating the contributions of the magnetic subsystems in antiferromagnetic ferrihydrite nanoparticles by analyzing the magnetization in fields of up to 250 kOe
Колич.характеристики :8 с
Место публикации : J. Magn. Magn. Mater. - 2024. - Vol. 592. - Ст.171781. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2024.171781. - ISSN 18734766 (eISSN)
Примечания : Cited References: 84. - This study was supported by his work was supported by the Russian Science Foundation, project no. 22–72-00134Authors thank to D.A. Velikanov, S.V. Komogortsev for fruitful discussions
Аннотация: Contributions of different magnetic subsystems formed in the systems of synthetic ferrihydrite nanoparticles (characterized previously) with an average size of ˂d˃ ≈ 2.7 nm coated with polysaccharide arabinogalactan in different degrees have been separated by measuring the dependences of their magnetization M on magnetic field H of up to 250 kOe on vibrating sample and pulsed magnetometers. The use of a wide measuring magnetic field range has been dictated by the ambiguity in identifying a linear M(H) portion for such antiferromagnetic nanoparticle systems within the conventional field range of 60–90 kOe. The thorough analysis of the magnetization curves in the temperature range of 100–250 K has allowed the verification of the contributions of (i) uncompensated magnetic moments µun in the superparamagnetic subsystem, (ii) the subsystem of surface spins with the paramagnetic behavior, and (iii) the antiferromagnetic susceptibility of the antiferromagnetically ordered ferrihydrite particle core. As a result, a model of the magnetic state of ferrihydrite nanoparticles has been proposed and the numbers of spins corresponding to magnetic subsystems (i)–(iii) have been estimated. An average magnetic moment μun of ∼ 145 μB (μB is the Bohr magneton) per particle corresponds approximately to 30 decompensated spins of iron atoms in a particle (about 3 % of all iron atoms), which, according to the Néel’s hypothesis μun ∼ ˂d˃3/2, are localized both on the surface and in the bulk of an antiferromagnetically ordered particle. The fraction of free (paramagnetic) spins is minimal in the sample without arabinogalactan coating of the nanoparticle surface (7 %) and is attained 20 % of all iron atoms in the sample with the highest degree of spatial separation of particles. According to this estimation, paramagnetic spins are located mainly on the edges and protruding areas of particles. Most magnetic moments of iron atoms are ordered antiferromagnetically and the corresponding magnetic susceptibility of this subsystem behaves as in an antiferromagnet with the randomly distributed crystallographic axes, i.e., increases with temperature.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zagorskiy D.L., Semenov S. V., Komogortsev S. V., Balaev D. A., Doludenko I.M., Panina L.V.
Заглавие : Magnetization processes in two-dimensional arrays of iron nanowires
Колич.характеристики :8 с
Место публикации : J. Magn. Magn. Mater. - 2024. - Vol. 595. - Ст.171573. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2023.171573. - ISSN 18734766 (eISSN)
Примечания : Cited References: 48. - This work was supported by Russian Scientific Foundation (RSF) Grant 22-22-00983
Аннотация: Arrays of iron nanowires (NWs) obtained by template-assisted electrodeposition constitute a promising composite material characterized by a combination of high magnetization in the filler and perpendicular magnetic anisotropy. The properties of these composites arise from the interplay between the behavior of individual NWs and their magnetostatic interactions. In this study, we investigated NW arrays with identical wire diameters but varying spatial arrangements. Major hysteresis loops were studied under various field directions relative to the NW axis. Key parameters such as the slope of the magnetization curve, saturation magnetization, and coercive force were quantified. Additionally, FORC (First Order Reversal Curve) measurements were conducted with the field oriented longitudinally with respect to the NW, offering insights into the inhomogeneity of the demagnetizing field influenced by the NW array's configuration. In the sample with the highest NW density, we observed isotropic behavior of the effective demagnetizing field, and we proposed an explanation for this phenomenon using the effective media approach. Micromagnetic simulations revealed that the magnetic behavior of individual NWs with a 100 nm diameter can be described as an interchange between volumes characterized by vortex and uniform magnetization patterns. Calculations of the demagnetizing field using the effective medium model demonstrated excellent agreement with experimental data across arrays featuring different NW densities. Remarkably, the quantitative consistency of coercive field values obtained from micromagnetic simulations and experimental measurements in the range of angles from 0° to 45° for the studied samples underscores the structural homogeneity of the obtained NWs.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Solovev P. N., Belyaev B. A., Boev N. M., Skomorokhov G. V., Izotov A. V.
Заглавие : Magnetic anisotropy and ferromagnetic resonance in inhomogeneous demagnetizing fields near edges of thin magnetic films
Колич.характеристики :12 с
Место публикации : J. Phys. Condens. Matter. - 2024. - Vol. 36, Is. 19. - Ст.195803. - ISSN 09538984 (ISSN), DOI 10.1088/1361-648X/ad258c. - ISSN 1361648X (eISSN)
Примечания : Cited References: 38
Аннотация: Using local ferromagnetic resonance spectroscopy, we have studied the magnetic properties near edges of thin tangentially magnetized permalloy films, in which a well-defined uniaxial magnetic anisotropy was induced perpendicular to one of the edges. In the experiment, two samples with thicknesses of 90 and 300 nm and with slightly different compositions were examined. To explain the magnetization dynamics near edges, we propose a simple yet effective model of a film in the form of a rectangular prism, which yields the modified Kittel formula for the resonance frequency. In this formula, the locally averaged distance-dependent demagnetizing field that emerges near the edges is included as an additional uniaxial anisotropy term. The measurements reveal that at a certain distance from the edge, the resulting (apparent) anisotropy, determined from the angular dependencies of the resonance field, almost vanishes. Moreover, its easy axis reorients to become parallel to the edge. The model predictions agree well with these results, proving that the main resonance mode behavior near the film edges can be accurately described by introducing additional effective uniaxial anisotropy, provided the measuring area is relatively large. However, for the thick (300 nm) sample, additional precession modes are also observed. These modes distort the angular dependence of the main mode, thus demonstrating the limitations of the model.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gokhfeld D. M.
Заглавие : Magnetic flux trapping in porous high-Tc superconductors
Колич.характеристики :4 с
Место публикации : Phys. C: Supercond. Appl. - 2024. - Vol. 619. - Ст.1354486. - ISSN 09214534 (ISSN), DOI 10.1016/j.physc.2024.1354486. - ISSN 18732143 (eISSN)
Примечания : Cited References: 39
Аннотация: Porosity affects the properties of high-Tc superconductors and can improve their performance by enhancing oxygenation, cryocooling, etc. Among other factors, the presence of pores plays a significant role in the process of magnetic flux trapping. Relationships with the porosity manifest in the irreversibility field, the full penetration field, and the remnant magnetization of the samples. To account for the effect of porosity on the trapped magnetic flux into type-II superconductors, a simple toy model is suggested. Generally, as the porosity increases, the trapped flux and related parameters tend to diminish. However, in the case of microscopic samples, porosity can enhance magnetic flux trapping.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Balaev D. A., Semenov S. V., Gokhfeld D. M.
Заглавие : Developing a concept of an effective field in the intergrain medium of a granular superconductor: Effect of the intragrain Meissner currents and Abrikosov vortices trapped in grains on the magnetotransport properties of a Y-Ba-Cu-O granular HTS
Колич.характеристики :18 с
Место публикации : J. Supercond. Nov. Magn. - 2023. - Vol. 36, Is. 7-9. - P.1631-1648. - ISSN 15571939 (ISSN), DOI 10.1007/s10948-023-06608-2. - ISSN 15571947 (eISSN)
Примечания : Cited References: 58. - The authors are grateful to M.I. Petrov, A.D. Balaev, and V.M. Sosnin for fruitful discussions and A.V. Shabanov and I.V. Nemtsev for scanning electron microscopy investigations. The scanning electron microscopy investigations and a part of magnetic measurements (performed on a LakeShore VSM 8604 facility) were carried out at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch of the Russian Academy of Sciences. The study is performed within the state assignment of Kirensky Institute of Physics
Аннотация: Granular high-temperature superconductors (HTSs) are characterized by the hysteretic field dependences of magnetoresistance R(H) and critical current IC(H). These hysteretic effects are described within the concept of an effective field in the intergrain medium. The effective field is a superposition of external magnetic field H and the field induced by the magnetic moments of superconducting grains into intergrain spacings (grain boundaries). The magnetization of superconducting grains is determined by two contributions: Meissner (shielding) currents (MC) and trapped magnetic fluxes (Abrikosov vortices (AV)). To develop the concept of an effective field in the intergrain medium, the magnetotransport properties (R and IC) have been compared for two cases: (AV) the magnetization of superconducting grains is only determined by the trapped magnetic flux (zero external field) and (MC) HTS grains are in the Meissner state (the external field is weaker than the first critical field of grains). In a set of experiments, the main features of the hysteretic R(H) and M(H) dependences have been illustrated and the external conditions for implementing the AV and MC states have been established. It has been found that the effects of the Abrikosov vortices and intragrain Meissner currents on an effective field in the intergrain medium at the same magnetization values are noticeably different. This is a nontrivial fact that requires a thorough study of the impact of the anisotropy of the superconducting properties of grains on the configuration of the Meissner currents in them, as well as on the orientation of vortices both inside grains and near their surface. We suggest the explanation of observed stronger effect of the Meissner currents on the intergrain medium as compared with the effect of the Abrikosov vortices.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Komogortsev S. V., Iskhakov R. S., Li O. A, Sukhachev A. L., Velikanov D. A., Nemtsev I. V.
Заглавие : Magnetic anisotropy of nanostructured Fe-Ni-C coating produced by electroless deposition
Колич.характеристики :5 с
Коллективы : Nanophysics and Nanoelectronics, International Symposium
Место публикации : Phys. Solid State. - 2023. - Vol. 65, Is. 6. - P.851-855. - ISSN 10637834 (ISSN), DOI 10.21883/PSS.2023.06.56090.14H. - ISSN 10906460 (eISSN)
Примечания : Cited References: 20. - The study was done with financial support from the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory and the Krasnoyarsk Regional Fund of Science within scientific project No. 20-43-240003
Аннотация: The structural and magnetic properties of nanostructured Fe100–xNix-C (0 ˂ x ˂ 100) coatings produced by electroless plating with different carbohydrates as reducing agents have been investigated. The phase-structural state of the films was studied by diffraction and electron microscopy. The Ni concentration ranges of FCC and BCC phases existence in electroless deposited films were determined. The surface morphology, saturation magnetization, local magnetic anisotropy field and coercivities of films are dependent on the iron content and type of reducing agent. The correlation between coercivity Hc and the anisotropy field of the magnetic stochastic domain which were established by correlation magnetometry suggests that the magnitude of Hc is mainly determined by this anisotropy.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Zagorskiy D. L., Semenov S. V., Komogortsev S. V., Doludenko I. M., Balaev D. A., Panina L. V.
Заглавие : Magnetization curves of 2D iron nanowires array
Коллективы : Samarkand International Symposium on Magnetism, Samarkand State University
Место публикации : Book of abstacts of Samarkand International Symposium on Magnetism (SISM-2023)/ int. adv. com. S. G. Ovchinnikov [et al.]. - 2023. - Ст.2PO-L4-23. - P.121. - ISBN 978-5-00202-320-2
Примечания : РНФ № 22-22-00983
Материалы конференции,
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gokhfeld D. M., Semenov S. V., Petrov M. I., Nemtsev I. V., Balaev D. A.
Заглавие : Anisotropy and crystallite misalignment in textured superconductors
Место публикации : J. Supercond. Nov. Magn. - 2023. - Vol. 36, Is. 1. - P.59-65. - ISSN 15571939 (ISSN), DOI 10.1007/s10948-022-06454-8. - ISSN 15571947 (eISSN)
Примечания : Cited References: 21. - This work was supported by the Russian Foundation for Basic Research and the Government of the Krasnoyarsk Territory, Krasnoyarsk Territorial Foundation for Support of Scientific and R&D Activities, project “Superconducting properties of YBCO incorporated by paramagnetic rare-earth elements” No. 20–42–240008
Аннотация: A misalignment of anisotropic crystallites causes small values of anisotropy and decreases the critical current density of textured polycrystalline superconductors. To relate the crystallite misalignment and out-plane anisotropy, the magnetic properties of the textured Bi2223 polycrystalline superconductor were investigated. A distribution of orientation angles of crystallites was determined using different data: scanning electron microscopy images and hysteresis magnetization loops when an external magnetic field was applied at different angles with respect to the texturing plane of the sample. It was demonstrated that the standard deviation of the distribution and the magnetic disorder angle of crystallites in textured samples can be determined from the magnetization data in perpendicular directions. These data may be either the irreversible magnetization measured for two different orientations of the sample or the simultaneously measured magnetization projections parallel and perpendicular to the magnetic field.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krasikov A. A., Balaev D. A.
Заглавие : Analysis of magnetization processes in antiferromagnetic nanoparticles in strong pulse fields (Brief review)
Коллективы : Eurasian Symposium “Trends in Magnetism”
Место публикации : J. Exp. Theor. Phys. - 2023. - Vol. 136, Is. 1. - P.97-105. - ISSN 10637761 (ISSN), DOI 10.1134/S1063776123010132. - ISSN 10906509 (eISSN)
Примечания : Cited References: 43. - The authors are grateful to V.L. Kirillov for synthesis of a set of NiO samples, O.N. Mart’yanov for cooperation and discussion of results for NiO nanoparticles, V.P. Ladygina for synthesis of nanoferrihydrite, S.V. Stolyar and R.S. Iskhakov for cooperation and discussion of results for ferrihydrite, and A.D. Balaev, K.A. Shaikhutdinov, and S.I. Popkov for the decisive contribution to the realization of pulse field setup
Аннотация: We present a brief review of investigations and analysis of magnetization curves M(H) for NiO and ferrihydrite antiferromagnetic nanoparticles in external fields up to 250 kOe. For correct interpretation of magnetic properties of systems of antiferromagnetic nanoparticles, it is important to take into account the segment of M(H) dependences, which corresponds to high fields (exceeding 100 kOe). We analyze the regularities in the formation of additional magnetic subsystems in antiferromagnetically ordered nanoparticles due to the influence of size effects. These additional subsystems (the ferromagnetic subsystem associated with uncompensated magnetic moment and the subsystem of surface free spins) are estimated quantitatively. It is shown that antiferromagnetic nanoparticles with a size of 5 nm acquire the properties of “nanomagnets,” which are not inferior to those for iron-oxide ferromagnetic nanoparticles of the same size.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Izotov A. V., Belyaev B. A., Boev N. M., Burmitskikh A. V., Skomorokhov G. V., Zharkov S. M., Solovev P. N.
Заглавие : Ferromagnetic resonance line broadening and shift effect in nanocrystalline thin magnetic films: Relation with crystalline and magnetic structure
Коллективы : RFBRRussian Foundation for Basic Research (RFBR); Government of Krasnoyarsk Territory; Krasnoyarsk Regional Fund; JSC "NPP "Radiosviaz" [20-42-242901]; Ministry of Science and Higher Education of the Russian Federation [075-11-2019-054, FSRZ-2020-0011]
Место публикации : J. Alloy. Compd. - 2022. - Vol. 900. - Ст.163416. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2021.163416. - ISSN 1873-4669(eISSN)
Примечания : Cited References: 52. - The reported study was funded by RFBR, the Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund and JSC "NPP "Radiosviaz", project number 20-42-242901 and was supported by the Ministry of Science and Higher Education of the Russian Federation, agreement number 075-11-2019-054 dated 22.11.2019.; The electron microscopy investigations were conducted in the SFU Joint Scientific Center whose infrastructure was supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
Предметные рубрики: SUSCEPTIBILITY
RIPPLE
ANISOTROPIES
ALLOYS
Аннотация: With the rapid development of telecommunication technologies and highly integrated electronic devices, researchers show great interest in nanocrystalline soft magnetic thin films with unique characteristics for microwave applications. An important direction of the current research in this field is the study of high-frequency magnetization dynamics that directly depends on the damping processes in a magnetic medium. This paper reports on the effect of sharp broadening and shift of the ferromagnetic resonance (FMR) line revealed experimentally in a 40-nm-thick nanocrystalline permalloy (Fe20Ni80) thin film at a frequency of about 5 GHz. The effect arises only in films with crystallite size exceeding some critical value Dcr. The micromagnetic simulation demonstrates that exchange and dipolar interactions between randomly oriented crystallites form in the film a quasiperiodic magnetic structure with a characteristic wavelength in the range from 36 nm to 3.3 µm. An analysis of the two-magnon scattering model and simulation results shows that the formed magnetic structure provides the energy transfer from uniform magnetization oscillations (uniform FMR) to spin waves, which results in an additional energy dissipation channel and, consequently, sharp FMR line broadening. A theoretical estimate of the critical crystallite size Dcr based on this model yields a value of ~14.3 nm for 40-nm-thick Fe20Ni80 films.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Maksimova A. N., Kashurnikov V. A., Moroz A. N., Gokhfeld D. M.
Заглавие : Trapped field in superconductors with perforations
Коллективы : RFBRRussian Foundation for Basic Research (RFBR) [20-21-00085]; ROSATOM [20-21-00085]
Место публикации : J. Supercond. Nov. Magn. - 2022. - Vol. 35, Is. 1. - P.283-290. - ISSN 1557-1939, DOI 10.1007/s10948-021-06067-7. - ISSN 1557-1947(eISSN)
Примечания : Cited References: 35. - The reported study was funded by RFBR and ROSATOM according to the research project No 20-21-00085 (V.A. Kashurnikov, A.N. Moroz)
Предметные рубрики: MAGNETIZATION
BULK
Аннотация: The Monte Carlo method has been used to calculate the trapped magnetic field in superconducting plates with holes. The mechanism of flux pinning on the holes is implemented with special subprocesses added to the algorithm: vortex capture and emission, both occurring on the hole boundaries. Secondary peaks related to the holes emerge on the calculated profiles of the trapped magnetic field. It has been found that these peaks disappear in plates with sufficiently strong pinning or when the computational mesh is coarse (the case corresponding to a low resolution of probes in experiments). The dependence of the trapped field on the hole radius has been analyzed.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhailov A. A., Maksimova A. N., Moroz A. N., Gokhfeld D. M.
Заглавие : Temperature and dimensional dependence of the irreversibility field of a layered high-temperature superconductor
Колич.характеристики :6 с
Место публикации : Phys. At. Nucl. - 2022. - Vol. 85, Is. 10. - P.1652-1657. - ISSN 10637788 (ISSN), DOI 10.1134/S1063778822100398. - ISSN 1562692X (eISSN)
Примечания : Cited References: 23. - The work was supported by the “Prioritet-2030” program of National Research Nuclear University MEPhI
Аннотация: The Monte Carlo method was used in a 2D model of the layered HTSC to calculate the magnetization curves of a granulated high-temperature superconductor for various sizes of granules. In this approach magnetization of granules alone is taken into account, while the contribution of the gaps between granules is small and neglected. The irreversibility field has been found to decrease with temperature at the fixed size of granules and increase as the granule size increases at fixed temperature. The time dependence of residual magnetization has been studied at various temperatures. The relaxation rate is shown not to depend on the granule size at low temperatures but to decrease with the increasing size (provided that the granule size is less than 3 μm) at a high temperature when the magnetic flux creep becomes of importance.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Balaev D. A., Semenov S. V., Gokhfeld D. M.
Заглавие : Influence of intragranular Meissner currents and magnetic flux trapped in granules on the effective field in the intergranular medium and the magnetoresistance hysteresis of a granular HTSC
Место публикации : Phys. Solid State. - 2022. - Vol. 64, Is. 12. - P.1846-1854. - ISSN 10637834 (ISSN), DOI 10.21883/PSS.2022.12.54376.442. - ISSN 10906460 (eISSN)
Примечания : Cited References: 61. - The study was carried out with the financial support of the Russian Foundation for Basic Research, the Government of the Krasnoyarsk Territory, the Krasnoyarsk areal Science Foundation within the framework of the scientific project No. 20-42-240008 ”The effect of the introduction of paramagnetic ions of rare earth elements on the superconducting properties of materials based on YBCO“. The study of the microstructure and magnetic measurements were carried out using the equipment of the Center for Collective Use of the FITC KNC SB RAS
Аннотация: The concept of an effective field in an intergranular medium is used to describe the hysteresis magnetoresistance of granular HTSCs. This effective field is a superposition of the external magnetic field and the field induced by the magnetic moments of the superconducting granules. The magnetic moment of the granules is contributed by the shielding currents and the trapped magnetic flux. We studied and analyzed the effect of the trapped flux on the magnetoresistance. It has been experimentally shown that the dependence of the residual resistance RRem (after applying of the external field) on the trapped flux clearly correlates with the behavior of the remanent magnetization. In addition, special attention was paid to a detailed comparison of the magnetoresistance of the granular YBa2Cu3O7-δ for two cases: (a) the magnetization of HTSC-granules is caused only by the trapped magnetic flux (in a zero external field) and (b) HTSC-granules are in the Meissner state (the external field is smaller than the first critical field of the granules). It has been found that Abrikosov vortices and intragranular Meissner currents differently affect the effective field in the intergranular medium (for the same values (of magnetization for cases (a) and (b) ). A possible reason for this difference is discussed.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Komogortsev S. V., Semenov S. V., Varnakov S. N., Balaev D. A.
Заглавие : Features of the phase composition and structure of hypoeutectoid steel, manifested in the behavior of magnetization near magnetic saturation
Место публикации : Phys. Solid State. - 2022. - Vol. 64, Is. 1. - P.23-30. - ISSN 10637834 (ISSN), DOI 10.21883/PSS.2022.01.52484.192. - ISSN 10906460 (eISSN)
Примечания : Cited References: 46. - The research has been conducted with financial support by the Russian Foundation for Basic Research, Government of the Krasnoyarsk Territory, Krasnoyarsk Regional Science Foundation within the framework of the scientific project No. 20-48-242905 p_Yenisei Siberia ”Determining the impact of ferromagnetic magnetization on MHD parameters of electrolyser operation“
Аннотация: Investigation of the temperature evolution of magnetization curves near magnetic saturation makes it possible to extract new information on the features of the phase composition and structure of hypoeutectoid steel. It is shown that the main contribution to the magnitude and the temperature behavior of the energy density of the local magnetic anisotropy of hypoeutectoid steel is due to the lamellar structure of pearlite. The peculiarity of the temperature behavior of the energy of the magnetic anisotropy, along with the behavior of the paraprocess, indicates the formation of Mn-substituted cementite in the studied steel sample. The observation of the crossover of power-law regularities in the approximation of magnetization to saturation indicates the formation of two-dimensional nano-inhomogeneities of the local axis of easy magnetization in the plates of alpha iron, which are part of the pearlite.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Grigoriev, Maxim V., Solovyov, Leonid A., Ruseikina, Anna V., Aleksandrovsky A. S., Chernyshev, Vladimir A., Velikanov D. A., Garmonov, Alexander A., Molokeev M. S., Oreshonkov A. S., Shestakov N. P., Matigorov, Alexey V., Volkova, Svetlana S., Ostapchuk, Evgeniy A., Kertman, Alexander V., Schleid, Thomas, Safin, Damir A.
Заглавие : Quaternary selenides EuLnCuSe3: Synthesis, structures, properties and in silico studies
Место публикации : Int. J. Mol. Sci. - 2022. - Vol. 23, Is. 3. - Ст.1503. - ISSN 1422-0067(eISSN), DOI 10.3390/ijms23031503
Примечания : Cited References: 90
Предметные рубрики: RARE-EARTH
CRYSTAL-STRUCTURES
MAGNETIC-PROPERTIES
THERMOELECTRIC PERFORMANCE
Аннотация: In this work, we report on the synthesis, in-depth crystal structure studies as well as optical and magnetic properties of newly synthesized heterometallic quaternary selenides of the Eu+2Ln+3Cu+1Se3 composition. Crystal structures of the obtained compounds were refined by the derivative difference minimization (DDM) method from the powder X-ray diffraction data. The structures are found to belong to orthorhombic space groups Pnma (structure type Ba2MnS3 for EuLaCuSe3 and structure type Eu2CuS3 for EuLnCuSe3, where Ln = Sm, Gd, Tb, Dy, Ho and Y) and Cmcm (structure type KZrCuS3 for EuLnCuSe3, where Ln = Tm, Yb and Lu). Space groups Pnma and Cmcm were delimited based on the tolerance factor t’, and vibrational spectroscopy additionally confirmed the formation of three structural types. With a decrease in the ionic radius of Ln3+ in the reported structures, the distortion of the (LnCuSe3) layers decreases, and a gradual formation of the more symmetric structure occurs in the sequence Ba2MnS3 → Eu2CuS3 → KZrCuS3. According to magnetic studies, compounds EuLnCuSe3 (Ln = Tb, Dy, Ho and Tm) each exhibit ferrimagnetic properties with transition temperatures ranging from 4.7 to 6.3 K. A negative magnetization effect is observed for compound EuHoCuSe3 at temperatures below 4.8 K. The magnetic properties of the discussed selenides and isostructural sulfides were compared. The direct optical band gaps for EuLnCuSe3, subtracted from the corresponding diffuse reflectance spectra, were found to be 1.87–2.09 eV. Deviation between experimental and calculated band gaps is ascribed to lower d states of Eu2+ in the crystal field of EuLnCuSe3, while anomalous narrowing of the band gap of EuYbCuSe3 is explained by the low-lying charge-transfer state. Ab initio calculations of the crystal structures, elastic properties and phonon spectra of the reported compounds were performed.
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16.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Shiyan Ya. G., Lee L. A.
Заглавие : FMR method for determining the magnetization of thin cobalt films
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 1, Sect.: Spin dynamics and magnetic resonances. - Ст.B.P20. - P.296. - ISBN 978-5-94469-051-7
Примечания : Cited References: 5. - This work was supported by the State order of the Ministry of Science and Higher Education of the Russian Federation (topic No. FSRZ-2020-0011)
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17.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Gritsenko Ch., Lepalovskij V. N., Volochaev M. N., Komanický V., Gorkovenko A. N., Pazniak H., Andreev N. V., Rodionova V.
Заглавие : Magnetization reversal mechanisms of FeNi/FeMn bilayers depending on growth conditions
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 1, Sect.: Spintronics and magnetic nanostructures. - Ст.A.O30. - P.86. - ISBN 978-5-94469-051-7
Примечания : Cited References: 4. - The electron microscopy investigations were carried out on the equipment of Krasnoyarsk Regional
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Lin C. -R., Chen Y. -Z., Ivanova O. S., Altunin R. R., Knyazev Yu. V., Molokeev M. S., Zharkov S. M., Shestakov N. P., Sukhachev A. L., Edelman I. S.
Заглавие : Effect of surfactants on the structure, phase composition, and magnetic properties of FexSy nanoparticles synthesized by thermal decomposition
Место публикации : Nanobiotechnol. Rep. - 2022. - Vol. 17, Is. 3. - P.336-344. - ISSN 26351676 (ISSN), DOI 10.1134/S2635167622030089
Примечания : Cited References: 27. - This study was supported by the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project no. 19-42-240005: “Features of the Electronic Structure, Magnetic Properties, and Optical Excitations in Nanocrystals of Multifunctional Magnetic Chalcogenides Fe3S4 and FeSe” and the Russian Foundation for Basic Research and the Ministry of Science and Technology of Taiwan, joint projects nos. 19-52-52002 and 109-2112-M-153-003 and 108-2923-M-153-001-MY3The electron-microscopy study was carried out at the Laboratory of Electron Microscopy of the Center for Collective Use of the Siberian Federal University within the state assignment of the Ministry of Science and Higher Education of the Russian Federation (research code FSRZ-2020-0011). The magnetic measurements were carried out on a vibrating sample magnetometer at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
Аннотация: The effect of surfactants on the structure, morphology, and magnetic properties of FexSy iron-sulfide nanoparticles synthesized by thermal decomposition is studied. Oleylamine, hexadecylamine, and octadecylamine are used as surfactants. It is established by X-ray and electron-diffraction analysis combined with Mossbauer spectroscopy that, in samples 1 and 2 prepared using oleylamine and hexadecylamine, respectively, the Fe3S4 greigite phase dominates, with an inverse spinel structure isostructural to the iron oxide Fe3O4 magnetite with minor Fe9S11 impurities. Deviations in the distribution of iron cations over the tetrahedral and octahedral sites relative to the bulk greigite crystals are observed. The nanoparticles synthesized using octadecylamine (sample 3) are found to be multiphase with a greigite fraction of ~20%. In all three cases, as showed the results of transmission electron microscopy and Fourier transform infrared spectroscopy together with thermogravimetry analysis, the magnetic nanoparticles have an organic shell chemically bonded to their magnetic core, which prevents the agglomeration of the particles. This shell is much more massive in samples 2 and 3. The magnetization values for samples 1 and 2 are similar to those of greigite nanoparticles reported in publications, while the magnetization of sample 3 is several times lower, in accordance with the greigite fraction in it. The combination of fairly high magnetization with a massive organic shell allows one to consider hexadecylamine to be a promising surfactant for the synthesis of iron-sulfide nanoparticles protected from external impact and agglomeration.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Usmanov O. V., Ovsianikov A. K., Zobkalo I. A., Shaykhutdinov K. A., Terentjev K. Yu., Semenov S. V.
Заглавие : Crystal field parameters and magnetic properties correlations in rare-earth orthoferrite HoFeO3
Место публикации : J. Surf. Invest. - 2022. - Vol. 16, Is. 6. - P.1041-1047. - ISSN 10274510 (ISSN), DOI 10.1134/S1027451022060258. - ISSN 18197094 (eISSN)
Примечания : Cited References: 28. - This work was supported by the Russian Foundation for Basic Research grant no. 19-52-12 047, and DFG grant no. SA 3688/1-1
Аннотация: The crystal structure and magnetic properties investigations of holmium orthoferrite compound HoFeO3 were performed in temperature range 7–300 K. Obtained XRD data confirm that HoFeO3 retains the orthorhombic perovskite structure of Pbnm space group. The crystal electric field (CEF) parameters of Ho3+ ion subsystem has been revealed numerically on the base of point charge model in the same temperature range. By this set of parameters CEF the splitting of Ho3+ energy levels was calculated and their temperature evolution was obtained. Modelling of isothermal magnetization M(H) with obtained set of parameters was carried out. Ho3+ single ion anisotropy due to CEF effects was demonstrated. Bulk magnetization evaluated from CEF was compared to experimental data.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Svalov A. V., Gorkovenko A. N., Larranaga A., Volochaev M. N., Kurlyandskaya G. V.
Заглавие : Structural and magnetic properties of FeNi films and FeNi-based trilayers with out-of-plane magnetization component
Место публикации : Sensors. - 2022. - Vol. 22, Is. 21. - Ст.8357. - ISSN 14248220 (ISSN), DOI 10.3390/s22218357
Примечания : Cited References: 50. - This research was funded by the Russian Science Foundation (RSF), project no. 22-29-00980, https://rscf.ru/en/project/22-29-00980/ and in part by the Research Groups of the UPV-EHU
Аннотация: FeNi films of different thickness and FeNi/(Fe, Co)/FeNi trilayers were prepared by magnetron sputtering deposition onto glass substrates. The permalloy films had a columnar microstructure. The detailed analysis of the magnetic properties based on the magnetic and magneto-optical measurements showed that at thicknesses exceeding a certain critical thickness, hysteresis loops acquire a specific shape and the coercive force of the films increase sharply. The possibility of the estimation of the perpendicular magnetic anisotropy constant using the Murayama equation for the thickness dependence of saturation field was demonstrated. The results of studies of the structural and magnetic properties of FeNi films laminated by Fe and Co spacers with different thickness are presented.
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