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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Yaroslavtsev R. N., Tyumentseva A.V., Velikanov D. A., Vazhenina I. G., Volochaev M. N., Stolyar S. V.
Заглавие : Fe3O4/Au nanocomposites: Characterization and cytotoxicity effects in vitro
Колич.характеристики :8 с
Место публикации : Mater. Chem. Phys. - 2024. - Vol. 322. - Ст.129524. - ISSN 02540584 (ISSN), DOI 10.1016/j.matchemphys.2024.129524. - ISSN 18793312 (eISSN)
Примечания : Cited References: 44
Аннотация: Magnetic nanocomposites containing iron oxide and gold components take great attention last years because of their relative biocompatibility and the ability to combine the magnetic properties of iron and the chemical bonding properties of gold for the possible drug delivery or diagnostics for various diseases. However, such particles have some toxicity to living cells, and the effect depends on many factors, including size, shape, the ratio of components in the composites, and the type of cells affected. And thus, the search for compositions and technologies for producing iron-gold particles with improved properties and reduced cytotoxicity remains relevant. The aim of the study was to synthesize and characterize Fe3O4/Au nanocomposites and evaluate their influence on living cells using the example of cell line HEK293. Fe3O4 nanoparticles (NPs) were synthesized by co-precipitation of Fe2+/Fe3+ water solution in alkaline conditions and then boiled with HAuCl4 in 0.1 M sodium citrate. The NPs properties were estimated by transmission electron microscopy (TEM), vibration magnetometry and ferromagnetic resonance (FMR). According to magnetometric measurements, nanoparticles are mainly in a superparamagnetic state. By fitting magnetization curves, the magnetic characteristics of nanoparticles were determined: saturation magnetization (59.3 emu/g) and magnetic anisotropy constant (K = 0.86·105 erg/cm3). The average particle size estimated from magnetic measurements was 8.7 nm. Considering the presence of a magnetically dead layer, this is in good agreement with the TEM results. The temperature dependence of the FMR linewidth was analyzed using two models. As a result, the parameters MSV and K/MS were determined. The models used showed good agreement. The values of the anisotropy constant (K = 1.06·105 erg/cm3) and the average particle size (6.8 nm) are estimated. The effect of the NPs on the HEK293 cells was studied by MTT-assay, flow cytometry and RT-PCR. The exposure with the NPs lead to a significant decrease of cell metabolic activity in HEK293 cell culture, but this effect was not accompanied by cell death. It was shown that the expression of antioxidant enzymes SOD1 and GPX1 was reduced at the mRNA stage. So the NPs synthesized may affect gene expression and metabolism of HEK293 cells, but this does not have fatal consequences for cell viability.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Qiu, Lei, Guan, Mengyu, Wang, Wei, Molokeev M. S., Polyutov, Sergey, Dai, Zhigao, Li, Guogang
Заглавие : Amino-bridged attapulgite@perovskite nanocomposites: The role of bridge linkage to optical property and stability
Колич.характеристики :11 с
Место публикации : Inorg. Chem. Front. - 2023. - Vol. 10, Is. 16. - P.4797-4807. - ISSN 20521553 (eISSN), DOI 10.1039/D3QI00863K
Примечания : Cited References: 50. - This work was supported by the National Natural Science Foundation of China (Grant Nos. 52072349 and 52172162). Z.D. acknowledges support from the Fundamental Research Funds for the Central Universities, China University of Geosciences (Wuhan) (No. 162301202610), the Natural Science Foundation of Guangdong Province (2022A1515012145), Shenzhen Science and Technology Program (JCYJ20220530162403007), and Key Research and Development Plan of Hubei Province. G.L. acknowledges support from the Natural Science Foundation of Zhejiang Province (LR22E020004). M.S. Molokeev and S.P. Polyutov acknowledge the support by the Ministry of Science and High Education of Russian Federation (Project No. FSRZ2023-0006)
Аннотация: Perovskite-based nanocomposites have garnered significant interests due to their potential in interfacial engineering, optical modification, and stability enhancement. However, current understanding of the construction models between perovskites and guest materials is limited, and the design concept of perovskite-based nanocomposites remains unclear. Herein, we thoroughly investigate the effects of amino bridge linkage in attapulgite@perovskite nanocomposites on the crystallization kinetics, optical properties, and stabilities of perovskites by monitoring the difference in structural, compositional, and morphological characteristics. The attapulgite@perovskite nanocomposite with amino bridge linkage exhibited a smaller average size distribution of 23.8 ± 5.8 nm, along with enhanced thermal stability (81% relative PL intensity after a heating-cooling cycle) and photo-stability (84% relative PL intensity after 30 h ultraviolet light irradiation). These improvements can be attributed to the adequate passivation of amino bridge linkages. Our work aims to provide a deeper understanding of perovskite-based nanocomposite construction and inspire new approaches for modifying their optical properties and enhancing their stability.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gan’shina, Elena A., Granovsky, Alexandr B., Garshin, Vladimir V., Pripechenkov, Ilya M., Sitnikov, Alexandr V., Volochaev M. N., Ryl’kov, Vladimir V., Nikolaev, Sergey N.
Заглавие : Magneto-optical spectroscopy of nanocomposites (CoFeZr)x(Al2O3)100-x
Место публикации : SPIN. - 2023. - Vol. 13, Is. 1. - Ст.2340006. - ISSN 20103247 (ISSN), DOI 10.1142/S2010324723400064. - ISSN 20103255 (eISSN)
Примечания : Cited References: 17. - This work was supported in part by the Russian Foundation for Basic Research under Grant 22-29-00392. Magnetic and MO studies were performed using equipment purchased at the expense of the MSU The authors thank the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” for assistance
Аннотация: We present results of magneto-optical investigations of (CoFeZr)x(Al2O3)100-x film nanocomposites in transverse Kerr effect (TKE) geometry in the spectral range 0.5-4.0eV and magnetic field up to 3.0kOe. Nanocomposites were deposited onto a glass-ceramic substrate by ion-beam sputtering. The TKE response at room temperature strongly depends on the wavelength of light, applied magnetic field H and the volume metallic fraction. From the analysis of the field dependences of TKE at different wavelengths, it follows that in the as-deposited samples, the interaction between nanoparticles at x30at.% is small and the nanocomposite is an ensemble of superparamagnetic particles; as x increases to 32at.%, a superspinglass-type state arises, then, in the vicinity of 34at.%, along with individual superparamagnetic particles, superferromagnetic regions appear. Long-range ferromagnetic order arises at concentrations x less than the percolation threshold for conductivity xper
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Semenov S. V., Knyazev Yu. V., Balaev D. A., Karnachuk O. V., Ikkert O. P.
Заглавие : Biosyntesis of magnetic nanocomposites using sulfate-reducing bacteria
Коллективы : Байкальская международная конференция "Магнитные материалы. Новые технологии", "Магнитные материалы. Новые технологии", Байкальская международная конференция, "Magnetic materials. New tecnologies", Baikal International Conference, Иркутский государственный университет
Место публикации : Магнитные материалы. Новые технологии: тез. докл. IX Байкал. междунар. конф. BICMM-2023/ чл. прогр. ком.: S. S. Aplesnin [et al.] ; чл. орг. ком. R. S. Iskhakov [et al.]. - Иркутск, 2023. - P.170. - ISBN 978-5-00133-051-6, DOI 10.26516/978-5-9624-2178-0.2023.1-207
Примечания : Библиогр.: 2
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Semenov S. V., Ikkert O. P., Balaev D. A., Karnachuk O. V., Knyazev Yu. V.
Заглавие : Forc analysis of interparticle interactions in biomineralized magnetic nanocomposites
Коллективы : Байкальская международная конференция "Магнитные материалы. Новые технологии", "Магнитные материалы. Новые технологии", Байкальская международная конференция, "Magnetic materials. New tecnologies", Baikal International Conference, Иркутский государственный университет
Место публикации : Магнитные материалы. Новые технологии: тез. докл. IX Байкал. междунар. конф. BICMM-2023/ чл. прогр. ком.: S. S. Aplesnin [et al.] ; чл. орг. ком. R. S. Iskhakov [et al.]. - Иркутск, 2023. - P.143. - ISBN 978-5-00133-051-6, DOI 10.26516/978-5-9624-2178-0.2023.1-207
Примечания : Библиогр.: 3
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Вид документа : Однотомное издание
Шифр издания :
Автор(ы) : Loiko V. A., Konkolovich A. V., Miskevich A. A., Krakhalev M. N., Prishchepa O. O., Shabanov A. V., Zyryanov V. Ya.
Заглавие : Electro-optical response of a monolayer polymer dispersed nematic liquid crystal film doped with surfactant
Место публикации : Liquid Crystal Polymer Nanocomposites: Woodhead Publishing, 2022. - Chapter 7. - P.163-211. - , DOI 10.1016/B978-0-12-822128-0.00006-6
Примечания : Cited References: 86
Аннотация: Light scattering and transmission by a monolayer polymer dispersed liquid crystal film containing liquid crystal droplets with inhomogeneous anchoring of liquid crystal molecules at the polymer-droplet interface is considered theoretically and experimentally. The developed optical model is based on the anomalous diffraction and interference approximations of the theory of scattering of waves. It is applied to describe the interference quenching effect for the coherently transmitted light and electrically controllable symmetry breaking effect in small-angle structure of light scattered by film containing droplets with inhomogeneous anchoring. The analysis of transmittance and reflectance of the one-dimensional photonic crystals composed of monolayers is carried out. The formation of the photonic band gaps is analyzed.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Loiko V. A., Konkolovich A. V., Misckevich A. A., Krakhalev M. N., Prishchepa O. O., Shabanov A. V., Zyryanov V. Ya.
Заглавие : Electro-optical response of a monolayer polymer dispersed nematic liquid crystal film doped with surfactant
Место публикации : Liquid crystal polymer nanocomposites/ ed.: P. M. Visakh [et al.]: Elsevier, 2022. - Chap. 7. - P.163-211. - (Woodhead publishing in materials). - ISBN 978-0-12-822128-0, DOI https://doi.org/10.1016/B978-0-12-822128-0.00006-6
Примечания : References: 86
Аннотация: Light scattering and transmission by a monolayer polymer dispersed liquid crystal film containing liquid crystal droplets with inhomogeneous anchoring of liquid crystal molecules at the polymer-droplet interface is considered theoretically and experimentally. The developed optical model is based on the anomalous diffraction and interference approximations of the theory of scattering of waves. It is applied to describe the interference quenching effect for the coherently transmitted light and electrically controllable symmetry breaking effect in small-angle structure of light scattered by film containing droplets with inhomogeneous anchoring. The analysis of transmittance and reflectance of the one-dimensional photonic crystals composed of monolayers is carried out. The formation of the photonic band gaps is analyzed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Федоров Л. Ю., Дрокин, Николай Александрович, Карпов И. В., Ушаков А. В.
Заглавие : Электрофизические характеристики полимерного композита на основе сверхвысокомолекулярного полиэтилена с наночастицами CuO
Место публикации : Журн. СФУ. Техн. и технол. - 2022. - Т. 15, № 7. - С. 802-811. - ISSN 1999494X (ISSN), DOI 10.17516/1999-494X-0437; J. Sib. Fed. Univ. Eng. Technol. - ISSN 23136057 (eISSN)
Примечания : Библиогр.: 19. - Исследование выполнено за счет гранта Российского научного фонда (проект № 20-19-00021)
Аннотация: Методом импедансной спектроскопии исследованы электрофизические свойства композитного материала на основе сверхвысокомолекулярного полиэтилена с ограниченной массовой концентрацией 0,5 мас.% оксида меди CuO в диапазоне частот от 102 до 108 Гц. Предполагается, что введение в состав полимера малых концентраций наночастиц способствует более равномерному их осаждению на поверхностях полимерных гранул. Это позволяет в процессе тестирования таких образцов выявить наиболее вероятные механизмы их поляризации и протекания электрического тока в относительно однородном ансамбле наночастиц в полимерной матрице. Установлено, что внедряемые в полимерную матрицу наночастицы незначительно влияют на процессы электрической поляризации, но приводят к появлению частотно-зависимой проводимости в широком диапазоне частот. Этот процесс сопровождается существенным возрастанием диэлектрических потерь. Электрофизические характеристики полученных композитов обсуждаются с учётом переноса электрических зарядов (ионов или электронов) как по внутренней, так и по поверхностной структуре наночастиц CuO.The electrophysical properties of a composite material based on ultrahigh molecular weight polyethylene with a limited mass concentration of 0.5 wt% copper oxide CuO in the frequency range from 102 to 108 Hz were studied by impedance spectroscopy. It is assumed that the introduction of low concentrations of nanoparticles into the polymer composition contributes to their more uniform deposition on the surfaces of polymer granules. This makes it possible to reveal the most probable mechanisms of their polarization and the flow of electric current in a relatively homogeneous ensemble of nanoparticles in a polymer matrix during testing of such samples. It has been established that nanoparticles introduced into the polymer matrix have little effect on the processes of electric polarization, but lead to the appearance of frequency-dependent conductivity in a wide frequency range. This process is accompanied by a significant increase in dielectric losses. The electrophysical characteristics of the resulting composites are discussed taking into account the transfer of electric charges (ions or electrons) both along the internal and surface structures of CuO nanoparticles.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Yaroslavtsev R. N., Stolyar S. V., Velikanov D. A., Volochaev M. N.
Заглавие : Magnetic properties of Fe3O4-Au nanocomposites
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 2, Sect. M: Magnetism in biology and medicine. - Ст.M.P12. - P.446-447. - ISBN 978-5-94469-051-7
Примечания : Cited References: 2
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Cheng, Lian, Liu, Kai, Wang, Mengqi, Fan, Pengyuan, Zhou, Changrong, Vtyurin A. N., Deng, Heming, Zhang, Ling, Zhang, Haibo, Hu, Yongming, Nan, B.o., Liu, Yang
Заглавие : Improvement of dielectric properties and energy storage performance in sandwich-structured P(VDF-CTFE) composites with low content of GO nanosheets
Место публикации : Nanotechnology. - 2021. - Vol. 32, Is. 42. - Ст.425702. - ISSN 0957-4484, DOI 10.1088/1361-6528/ac1295. - ISSN 1361-6528(eISSN)
Примечания : Cited References: 56. - The authers gratefully acknowledge the support by the National Natural Science Foundation of China: 51902111; DongGuan Innovation Research Team Program: 2020607101007; Dongguan Postgraduate Joint Training (Practice) Workstation: 2019707102018; Guangdong HUST Industrial Technology Research Institute, Guangdong Provincial Key Laboratory of Manufacturing Equipment Digitization: 2020B1212060014
Предметные рубрики: CHARGE-DISCHARGE EFFICIENCY
POLYMER NANOCOMPOSITES
BREAKDOWN STRENGTH
Аннотация: Polymer-based dielectric capacitors play a notable part in the practical application of energy storage devices. Graphene oxide (GO) nanosheets can improve the dielectric properties of polymer-based composites. However, the breakdown strength will greatly reduce with the increase of GO content. Hence, the construction of sandwich structure can enhance the breakdown strength without reducing the dielectric constant. Herein, single-layered and sandwich-structured poly(vinylidene fluoride-co-chlorotrifluoroethylene) (P(VDF-CTFE)) nanocomposites with low content of GO nanosheets (1.0 wt%) are prepared via employing a straightforward casting method. Compared with the single-layered composites and pure P(VDF-CTFE), the sandwich-structured composites exhibit comprehensively better performance compared. The sandwich-structured composite with 0.4 wt% GO nanosheets show an excellent dielectric constant of 13.6 (at 1 kHz) and an outstanding discharged energy density of 8.25 J cm−3 at 3400 kV cm−1. These results demonstrate that the growth of the dielectric properties is owing to 2D GO nanosheets and the enhancement of breakdown strength due to the sandwich structure. The results from finite element simulation provide theoretical support for the design of high energy density composites.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhaleva E. A., Flerov I. N., Bogdanov E. V., Bondarev V. S., Gorev M. V., Rysiakiewicz-Pasek E.
Заглавие : Size effect on sensitivity to external pressure and caloric effects in TGS: Ceramics and nanocomposites
Место публикации : Mater. Today Commun. - 2020. - Vol. 25. - Ст.101463. - ISSN 23524928 (ISSN), DOI 10.1016/j.mtcomm.2020.101463
Примечания : Cited References: 39
Аннотация: Experimental study of temperature-pressure phase diagrams revealed a slight difference in the sensitivity to hydrostatic pressure of triglycine sulfate (TGS) as a bulk (single crystal, ceramics), and nanoparticles embedded in porous glass (TGS + PG). An analysis of the pressure sensitivity, dT0/p and dT0/dσ, and entropies of the P21 ↔ P21/m phase transition showed the closeness of the barocaloric parameters in various materials under study. Due to the strong anisotropy of thermal expansion, the piezocaloric effect under pressure along the axis c exceeds the barocaloric effect in single-crystal TGS. The reasons for the strong reduction in the electrocaloric effect in the ferroelectric component of nanocomposites compared with a single-crystal are discussed.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Moseenkov S. I., Kuznetsov V. L., Zavorin A. V., Golubtsov G. V., Korovin, E. Yu., Suslyaev V. I., Ishchenko A. V., Serkova A. N., Sergeenko D. I., Velikanov D. A.
Заглавие : Electrophysical properties of composites based on polyethylene modified with multi-walled carbon nanotubes with high content of Fe-Co-catalyst
Коллективы : Russian Science FoundationRussian Science Foundation (RSF) [17-73-20293]
Место публикации : Russ. J. Appl. Chem. - 2020. - Vol. 93, Is. 4. - P.586-594. - ISSN 1070-4272, DOI 10.1134/S107042722004014X. - ISSN 1608-3296(eISSN)
Примечания : Cited References: 30. - This work was financially supported by the Russian Science Foundation, project no. 17-73-20293.
Предметные рубрики: POLYMER COMPOSITES
NANOPARTICLES
ACTIVATION
NANOCOMPOSITES
Аннотация: The effect of the residual catalyst for the synthesis of multi-walled carbon nanotubes (MWCNTs) on the electrophysical properties of MWCNT-polyethylene composites produced by melt mechanical mixing was studied. The residual catalyst content was varied by changing the MWCNTs synthesis time. The nanotubes used in the work were characterized using transmission and scanning electron microscopy, atomic emission analysis, X-ray phase analysis, and magnetic permeability measurements. The structure of the synthesized composites was studied using optical and scanning electron microscopy. The dependences of the specific magnetization on the applied magnetic field, bulk electrical conductivity on the volumetric content of the filler in the composite, and the frequency dependences of the reflection, transmission, and absorption of electromagnetic radiation in the range 0.01-18 GHz were obtained. It was established that the obtained composites are characterized by a uniform distribution of nanotubes in the polymer matrix, and the dependence of the bulk electrical conductivity on the content of MWCNTs in the composite has a percolation character. Variation in the synthesis time of nanotubes allows producing MWCNTs with a high content of ferromagnetic particles, which are an alloy close in stoichiometry to the composition of the active component of the catalyst. It was shown that the use of composites modified with MWCNTs with a high content of residual catalyst is more effective for absorbing electromagnetic radiation due to an increase in their magnetic losses.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bykova L. E., Myagkov V. G., Zhigalov V. S., Matsynin A. A., Velikanov D. A., Bondarenko G. N., Patrin G. S.
Заглавие : Magnetic and structure properties of CoPt-In2O3 nanocomposite films
Коллективы : Russian Foundation for Basic Research, Government of Krasnoyarsk Territory [19-43-240003]
Место публикации : J. Sib. Fed. Univ. Math. Phys. - 2020. - Vol. 13, Is. 4. - P.431-438. - ISSN 1997-1397, DOI 10.17516/1997-1397-2020-13-4-431-438; Журн. СФУ. Матем. и физика. - ISSN 2313-6022(eISSN)
Примечания : Cited References: 29. - This study was supported by the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science to the research projects no. 19-43-240003
Предметные рубрики: THIN-FILMS
TEMPERATURE
PHASE
Аннотация: The structural and magnetic properties of CoPt-In2O3 nanocomposite films formed by vacuum annealing of the In/(Co3O4 + Pt)/MgO film system in the temperature range of 100–800 °C have been investigated. The synthesized nanocomposite films contain ferromagnetic CoPt grains with an average size of 5nm enclosed in an In2O3 matrix, and have a magnetization of 600 emu/cm3, and a coercivity of 150 Oe at room temperature. The initiation 200 °C and finishing 800 °C temperatures of synthesis were determined, as well as the change in the phase composition of the In/(Co3O4 + Pt)/MgO film during vacuum annealing.Исследованы структурные и магнитные свойства нанокомпозитных пленок CoPt- In2O3, полученных вакуумным отжигом пленочной системы In/(Co3O4 + Pt)/MgO в интервале температур 100 – 800 °C. Синтезированные нанокомпозитные пленки содержали ферромагнитные CoPt-кластеры со средним размером 5 nm, заключенные в матрицу In2O3, и имели намагниченность 600 emu/cm3, коэрцитивную силу 150 Oe при комнатной температуре. Определены температуры начала 200 °C и окончания 800 °C синтеза, а также изменение фазового состава пленки In/(Co3O4 + Pt)/MgO при вакуумном отжиге.
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14.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ivantsov R. D., Petrov D. A., Ivanova O. S., Edelman I. S., Zharkov S. M., Velikanov D. A., Chun-Rong Lin
Заглавие : Magnetooptics of nanocomposites based on iron chalcogenide nanoparticles
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : The Fifth Asian School-Conference on Physics and Technology of Nanostructured Materials: Proceedings. - VLadivostok: Dalnauka Publishing, 2020. - Ст.IV.03.05o. - P.105. - ISBN 978-5-8044-1698-1
Примечания : The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: № 19-42-240005, by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Petrov D. A., Ivanova O. S., Edelman I. S., Zharkov S. M., Velikanov D. A., Lin, Chun-Rong
Заглавие : Magnetooptics of nanocomposites based on iron chalcogenide nanoparticles
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : Solid State Phenom. - 2020. - Vol. 312. - P.160-165. - ISSN 1012-0394, DOI 10.4028/www.scientific.net/SSP.312.160. - ISSN 1662-9779
Примечания : Cited References: 13. - The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: № 19-42-240005 «Features of the electronic structure, magnetic properties and optical excitations in nanocrystals of the multifunctional magnetic chalcogenides Fe3S4 and FeSe», by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3.
Аннотация: Morphology, structure, magnetic properties and magnetic circular dichroism (MCD) were studied for the FexSy and FexSey nanoparticles (NPs) synthesized with the polyol mediated and the thermal decomposition processes, correspondingly, at different regimes. For all NPs samples, but Fe3S4, MCD was measured for the first time. It has been shown that in the case of sulfides, the character of the MCD spectrum changes as the NPs phase composition transforms from Fe3S4 to FeS with the synthesis temperature increase. At the same time, the shape of the MCD spectrum is almost independent of the NPs phase in the case of iron selenides.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zhigalov V. S., Bykova L. E., Myagkov V. G., Pavlova A. N., Volochaev M. N., Matsynin A. A., Patrin G. S.
Заглавие : CoPt-Al2O3 nanocomposite films: synthesis, structure, and magnetic properties
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR); Government of Krasnoyarsk Territory; Krasnoyarsk Regional Fund of Science [18-42-243009 r_mol_a, 19-43-240003 r_a]; Foundation for Assistance to Small Innovative Enterprises in Science and Technology [11843GU/2017, 0033636]
Место публикации : J. Surf. Ingestig. - 2020. - Vol. 14, Is. 1. - P.47-53. - ISSN 1027-4510, DOI 10.1134/S102745102001022X. - ISSN 1819-7094(eISSN)
Примечания : Cited References: 29. - This study was supported by the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science to the research projects no. 18-42-243009 r_mol_a and no. 19-43-240003 r_a, and the Foundation for Assistance to Small Innovative Enterprises in Science and Technology, contract no. 11843GU/2017, code 0033636, U.M.N.I.K. competition.
Предметные рубрики: SOLID-STATE SYNTHESIS
GRANULAR THIN-FILMS
THERMITE SYNTHESIS
PHASE
Аннотация: The structure and magnetic properties of CoPt–Al2O3 nanocomposite films synthesized by the annealing of Al/(Co3O4 + Pt) bilayers on a MgO(001) substrate at 650°C in vacuum are investigated. The synthesized composite films contain ferromagnetic CoPt grains with an average size of 25–45 nm enclosed in a nonconducting Al2O3 matrix. The saturation magnetization (Ms ~ 330 G) and coercivity (Hc ≈ 6 kOe) of the films are measured in the film plane and perpendicular to it. The obtained films are characterized by a spatial rotational magnetic anisotropy, which makes it possible to arbitrarily set the easy magnetization axis in the film plane or perpendicular to it using a magnetic field stronger than the coercivity (H ˃ Hc).
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17.

Вид документа : Статья из журнала
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Автор(ы) : Bykova L. E., Zharkov S. M., Myagkov V. G., Zhigalov V. S., Patrin G. S.
Заглавие : In situ electron diffraction investigation of solid state synthesis of Co-In2O3 ferromagnetic nanocomposite thin films
Место публикации : JOM. - 2020. - Vol. 72, Is. 6. - P.2139–2145. - ISSN 10474838 (ISSN), DOI 10.1007/s11837-019-03919-5
Примечания : Cited References: 52. - The investigation was conducted under the partial financial support of the Russian Foundation for Basic Research (Grants #18-03-01173 and #19-43-240003).
Аннотация: In situ electron diffraction was used to study structural transformations during the formation of Co-In2O3 ferromagnetic nanocomposite thin films in a thermite reaction of In/Co3O4 bilayer thin films. Heating was performed from room temperature to 600°C at a rate of 4°C/min, while simultaneously electron diffraction patterns were recorded at a speed of 4 frames/min. This made it possible to determine the initiation, 185°C, and finishing, 550°C, temperatures of the solid-state synthesis, as well as the change in the phase composition during the thermite reaction. The synthesized Co-In2O3 film nanocomposite contained ferromagnetic cobalt nanoclusters surrounded by an In2O3 layer, with an average size of 20 nm, and had a magnetization of 400 emu/cm3 and a coercivity of 50 Oe at room temperature. The estimate of the effective interdiffusion coefficient of the reaction suggests that the main mechanism for the formation of the Co-In2O3 nanocomposite is diffusion along the grain boundaries and dislocations.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhaleva E. A., Flerov I. N., Kartashev A. V., Gorev M. V., Molokeev M. S., Korotkov L. N., Rysiakiewicz-Pasek E.
Заглавие : Specific heat and thermal expansion of triglycine sulfate-porous glass nanocomposites
Коллективы : Russian Foundation for Basic Research [16-32-00092 mol-a]
Место публикации : Phys. Solid State. - 2018. - Vol. 60, Is. 7. - P.1338-1343. - ISSN 1063-7834, DOI 10.1134/S1063783418070181. - ISSN 1090-6460(eISSN)
Примечания : Cited References: 27. - This study was supported by the Russian Foundation for Basic Research, project no. 16-32-00092 mol-a.
Предметные рубрики: PHASE-TRANSITIONS
DIELECTRIC-PROPERTIES
FERROELECTRIC COMPOSITES
Аннотация: The effect of restricted geometry on specific heat capacity and thermal expansion of the triglycine sulfate (TGS)–borosilicate glass composites have been studied first. A decrease in the entropy and temperature of the P21 ↔ P21/m phase transition in the TGS component with decreasing the glass matrix pore diameter at the invariable specific heat and thermal expansion coefficient has been observed. The estimates are indicative of the minor effect of internal pressure on the TGS pressure coefficient dTC/dp in the composites.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Usenko A., Moskovskikh D., Korotitskiy A., Gorshenkov M., Zakharova E., Fedorov A. S., Parkhomenko Y., Khovaylo V.
Заглавие : Thermoelectric properties and cost optimization of spark plasma sintered n-type Si0.9Ge0.1 - Mg2Si nanocomposites
Место публикации : Scripta Mater. - 2018. - Vol. 146. - P.295-299. - ISSN 13596462 (ISSN), DOI 10.1016/j.scriptamat.2017.12.019
Примечания : Cited References: 28. - This work was supported by Russian Science Foundation (project No. 16-13-00060). Part of the work (structural characterization of the samples) was carried out with financial support of the Ministry of Education and Science of the Russian Federation in the framework of Increase Competitiveness Program of NUST “MISiS”. Partial support by Act 211 Government of the Russian Federation, contract # 02.A03.21.0011, is also acknowledged.
Ключевые слова (''Своб.индексиров.''): cost optimization--lattice thermal conductivity--magnesium silicides--spark plasma--thermo-electric materials--thermoelectric figure of merit--thermoelectric performance--thermoelectric properties
Аннотация: We report on thermoelectric properties of low Ge content n-type Si0.9Ge0.1–Mg2Si nanocomposite. Introduction of the Mg2Si phase into a SiGe matrix resulted in a dramatic drop of the lattice thermal conductivity beyond the previously reported lowest limit for SiGe alloys due to intensification of phonon scattering on SiGe–Mg2Si grain boundaries. For a sample doped with 1 at.% of Mg2Si, the peak value of thermoelectric figure of merit ZT reached ~ 0.8 at 800 °C. Sintered nanocomposites still exhibit high thermoelectric performance while being almost two times cheaper than Si0.8Ge0.2.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lepeshev A. A., Patrin G. S., Yurkin G. Yu., Vasiliev A. D., Nemtsev I. V., Gokhfeld D. M., Balaev A. D., Demin V. G., Bachurina E. P., Karpov I. V., Ushakov A. V., Fedorov, L. Yu., Irtyugo L. A., Petrov M. I.
Заглавие : Magnetic properties and critical current of superconducting nanocomposites (1 −x)YBa2Cu3O7−δ + xCuO
Коллективы : Russian Science Foundation [16-19-10054]
Место публикации : J. Supercond. Nov. Magn. - 2018. - Vol. 31, Is. 12. - P.3841-3845. - ISSN 1557-1939, DOI 10.1007/s10948-018-4676-x. - ISSN 1557-1947(eISSN)
Примечания : Cited References: 15. - The work was performed with a support of the grant of the Russian Science Foundation (project no. 16-19-10054).
Предметные рубрики: PULSED-ARC DISCHARGE
COMPOSITES
PLASMA
LOOPS
Ключевые слова (''Своб.индексиров.''): superconducting polycrystals--ybco ceramics--critical current--magnetic properties
Аннотация: The aim of this paper was to study the effect of nanoscale inclusions of CuO as the second ingredient of composites on transport properties of superconducting YBa2Cu3O7 polycrystals. The samples of YBa2Cu3O7−δ with different content of CuO nanoparticles were synthesized. The analysis of the magnetic properties was carried out within the extended critical state model. It was found that the addition of 0.5 and 1% of CuO nanoparticles leads to an increase in the intragranular density of the critical current at T= 4.2 K. A further increase of x from 2 to 15% and more than 40% decreases the critical current density. The critical current density higher than in the reference sample was also found in the samples with x= 20% and x= 24%.
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