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Synthesis of Ni nanoclusters supported on diamond by plasma technique and their electrochemical properties / N. S. Nikolaev, V. G. Isakova, N. G. Vnukova [et al.] // Diam. Relat. Mater. - 2024. - Vol. 142. - Ст. 110844, DOI 10.1016/j.diamond.2024.110844. - Cited References: 35 . - ISSN 0925-9635. - ISSN 1879-0062
Кл.слова (ненормированные):
High pressure – high temperature (HTHP) diamond -- Nickel plasma -- Cyclic voltammetric -- Electrocatalytic activity -- Methanol -- Paracetamol
Аннотация: In this study, particles of synthetic undoped diamond (DN) obtained via the high pressure – high temperature method were coated with a nickel shell using metallic nickel plasma in a two-jet plasma generator with gas vortex and magnetic flux stabilization. Through the use of scanning electron microscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy, we observed the formation of a nickel diamond composite with a core-shell structure, where DN serves as the core and Ni nanoclusters form the shell (DN@Ni). The results of voltammetric analysis indicated that DN@Ni, when deposited on a graphite electrode, exhibited significant electrocatalytic activity in the oxidation of methanol and paracetamol in an alkaline electrolyte.

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Держатели документа:
Kirensky Institute of Physics, FSBSI "Federal Research Center "Krasnoyarsk Science Center SB RAS", Akademgorodok 50/38, Krasnoyarsk 660036, Russia
Institute of Engineering Physics and Radio Electronics, Siberian Federal University, Academician Kirensky str., 28, Krasnoyarsk 660074, Russia
Institute of Chemistry and Chemical Technology of the Siberian Branch of the Russian Academy of Sciences, FSBSI "Federal Research Center "Krasnoyarsk Science Center SB RAS", Akademgorodok 50/24, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Nikolaev, N. S.; Николаев, Никита Сергеевич; Isakova, V. G.; Исакова, Виктория Гавриловна; Vnukova, N. G.; Внукова, Наталья Григорьевна; Elesina, V. I.; Елесина, Виктория Игоревна; Glushenko, G. A.; Глущенко, Гарий Анатольевич; Tomashevich, Y. V.; Томашевич, Евгений Владимирович; Churilov, G. N.; Чурилов, Григорий Николаевич
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Effect of Cu on performance of self-dispersing Ni-catalyst in production of carbon nanofibers from ethylene / S. D. Afonnikova, Yu. I. Bauman, V. O. Stoyanovskii [et al.] // C – J. Carbon Res. - 2023. - Vol. 9, Is. 3 : Advanced Carbon Nanomaterials and Hybrids. - Ст. 77, DOI 10.3390/c9030077. - Cited References: 72. - This work was supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis (project AAAA-A21-121011390054-1). The physicochemical characterization of samples was supported by the Russian Science Foundation (project No. 22-13-00406, https://rscf.ru/en/project/22-13-00406/BIC SB RAS (accessed on 30 March 2023)). - Analysis of the physicochemical properties of the samples was performed using the equipment of the ‘National Center for Catalyst Research’ (Novosibirsk, BIC SB RAS) and Krasnoyarsk regional Center of the Collective Use (KSS SB RAS). The authors are grateful to A.N. Serkova for the performed SEM studies, B.A. Kolesov for the Raman spectra data, to A.B. Ayupov for analyzing samples by low-temperature adsorption/desorption of nitrogen, to Y.V. Shubin for the XRD analysis and to E.I. Belyaeva for the particle distribution analysis . - ISSN 2311-5629
Кл.слова (ненормированные):
nickel-copper alloys -- carbon erosion -- catalytic pyrolysis -- carbon nanofibers -- segmented structure
Аннотация: The development of effective catalysts for the pyrolysis of light hydrocarbons with the production of carbon nanomaterials represents a relevant direction. In the present work, the influence of copper addition on performance of a self-dispersed Ni-catalyst and structural features of the obtained carbon nanofibers (CNFs) was studied. The precursors of Ni and Ni-Cu catalysts were prepared by activation of metal powders in a planetary mill. During contact with the C2H4/H2 reaction mixture, a rapid disintegration of the catalysts with the formation of active particles catalyzing the growth of CNFs has occurred. The kinetics of CNF accumulation during ethylene decomposition on Ni- and Ni-Cu catalysts was studied. The effect of temperature on catalytic performance was explored and it was shown that introduction of copper promotes 1.5–2-fold increase in CNFs yield in the range of 525–600 °C; the maximum CNFs yield (100 g/gcat and above, for 30-min reaction) is reached on Ni-Cu-catalyst at 575–600 °C. A comparative analysis of the morphology and structure of CNF was carried out using electron microscopy methods. The growth mechanism of carbon filaments in the shape of “railway crossties” on large nickel crystals (d > 250 nm) was proposed. It was found that the addition of copper leads to a decrease in the bulk density of the carbon product from 40–60 to 25–30 g/L (at T = 550–600 °C). According to the low-temperature nitrogen adsorption data, specific surface area (SSA) of CNF samples (at T ˂ 600 °C) lies in the range of 110–140 m2/g, regardless of the catalyst composition; at T = 600 °C the introduction of copper contributed to an increase in the specific surface of CNF by 100 m2/g.

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Держатели документа:
Boreskov Institute of Catalysis SB RAS, 5 Lavrentyev Ave., Novosibirsk 630090, Russia
Kirensky Institute of Physics, Akademgorodok, 50/38, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Afonnikova, S. D.; Bauman, Yury I.; Stoyanovskii, Vladimir O.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Mishakov, Ilya V.; Vedyagin, Aleksey A.
}
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Synthesis and optical properties of nickel-doped copper metaborate crystals / A. D. Molchanova, E. M. Moshkina, M. S. Molokeev [et al.] // Opt. Spectrosc. - 2023. - Vol. 131, Is. 8. - P. 717-722, DOI 10.1134/S0030400X23060127. - Cited References: 18. - The study was performed with the support of Russian Science Foundation, RSF grant no. 19-12-00413 . - ISSN 0030-400X. - ISSN 1562-6911
Кл.слова (ненормированные):
3d-ions -- crystal growth -- optical spectroscopy -- magnetic ordering -- cuprates
Аннотация: This work presents information on the growth and spectroscopic study of single crystals of copper metaborate doped with nickel Cu1–xNixB2O4 (x = 0.05, 0.1). In the absorption spectra of both crystals, satellites related to Cu centers distorted by impurity Ni atoms were observed near the lines of zero phonon transitions. Polarization studies in the isotropic ab-plane of the tetragonal crystal Cu1–xNixB2O4 show the presence of linear magnetic dichroism in the magnetically ordered state, which was previously observed both in manganese-doped and undoped copper metaborates CuB2O4. The temperature of magnetic phase transitions into the collinear antiferromagnetic and into helicoidal structures, TN = 19.1 K and T * = 8.6 K, respectively, were determined from the temperature dependence of the dichroic signal.

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Публикация на русском языке Синтез и оптические свойства кристаллов метабората меди, легированного никелем [Текст] / А. Д. Молчанова, Е. М. Мошкина, М. С. Молокеев [и др.] // Оптика и спектроскопия. - 2022. - Т. 130 Вып. 1. - С. 111-115

Держатели документа:
Institute of Spectroscopy, Russian Academy of Sciences, 108840, Moscow, Troitsk, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia
Scientific and Innovation Department, Kemerovo State University, 650000, Kemerovo, Russia

Доп.точки доступа:
Molchanova, A. D.; Moshkina, E. M.; Мошкина, Евгения Михайловна; Molokeev, M. S.; Молокеев, Максим Сергеевич; Tropina, E. V.; Bovina, A. F.; Бовина, Ася Федоровна; Boldyrev, K. N.
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An effective method of magnetic hyperthermia based on the ferromagnetic resonance phenomenon / S. V. Stolyar, O. A. Li, E. D. Nikolaeva [et al.] // Phys. Met. Metallogr. - 2023. - Vol. 124, Is. 2. - P. 174-180, DOI 10.1134/S0031918X22601834. - Cited References: 15. - This study was supported by grant no. 22-14-20020 from the Russian Science Foundation and the Krasnoyarsk Regional Fund for Support of Scientific and Technological Activities. The authors are grateful to the Krasnoyarsk Regional Center for Collective Use at Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, for providing their research facilities . - ISSN 0031-918X. - ISSN 1555-6190
Кл.слова (ненормированные):
ferromagnetic resonance -- cobalt ferrite -- nickel ferrite -- magnetic hyperthermia
Аннотация: Nickel and cobalt ferrite nanoparticles have been synthesized using the chemical precipitation method; the nanoparticle sizes were found to be 63 ± 22 and 26 ± 4 nm, respectively. The static hysteresis loops and Mossbauer spectra have been measured. It is shown that cobalt ferrite powders are magnetically harder than nickel ferrite powders. Ferromagnetic resonance (FMR) curves have been studied. It is found that the FMR absorption for cobalt ferrite is observed at room temperature and above. The time dependences of the nanoparticle warm-up under FMR conditions have been measured. The maximum temperature changes for nickel ferrite and cobalt ferrite particles are 8 and 11 K, respectively. Using the example of cobalt ferrite powder, the possibility of effectively heating of particles in the FMR mode in their own field without using a DC magnetic field source is shown. The observed effect can be used in magnetic hyperthermia.

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Публикация на русском языке Эффективный способ магнитной гипертермии, основанный на явлении ферромагнитного резонанса [Текст] / С. В. Столяр, О. А. Ли, Е. Д. Николаева [и др.] // Физ. металлов и металловед. - 2023. - Т. 124 № 2. - С. 182-189

Держатели документа:
Federal Research Center, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia
Institute of Physics, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia

Доп.точки доступа:
Stolyar, S. V.; Li, O. A.; Nikolaeva, E. D.; Vorotynov, A. M.; Воротынов, Александр Михайлович; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Bayukov, O. A.; Баюков, Олег Артемьевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; P’yankov, V. F.; Volochaev, M. N.; Волочаев, Михаил Николаевич
}
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Second harmonic generation as a probe of parametric spin wave instability processes in thin magnetic films / P. N. Solovev, A. O. Afonin, B. A. Belyaev [et al.] // Phys. Rev. B. - 2022. - Vol. 106, Is. 6. - Ст. 064406, DOI 10.1103/PhysRevB.106.064406. - Cited References: 33. - This work was supported by the Russian Science Foundation under Grant No. 19-72-10047. The equipment of the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” was used during the measurements . - ISSN 2469-9950
Кл.слова (ненормированные):
Dynamic response -- Harmonic generation -- Nickel alloys -- Nonlinear optics -- Spin waves -- Dynamic component -- High amplitudes -- Microstrip-line -- Microwave field -- Parametric instabilities -- Second harmonic signals -- Spin-wave instabilities -- Thin magnetic films -- Thin permalloy films -- Threshold effect -- Iron alloys
Аннотация: We have explored the dynamic response of in-plane magnetized thin permalloy films excited by microwave fields of high amplitudes (up to 3 Oe) at 1 GHz. The response was detected using a microstrip line by measuring the second harmonic signal generated by the dynamic components of the uniform magnetization. The data measured at ferromagnetic resonance showed the threshold effect of the Suhl parametric instability process. With the increase of the microwave power above the threshold value, the dynamic response revealed an intricate nonlinear behavior, including the emergence of an additional threshold. This second threshold can be explained in terms of the "stage by stage"process of parametric spin wave excitation following the S theory of Zakharov, L'vov, and Starobinets.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Institute of Engineering Physics and Radio Electronics, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Solovev, P. N.; Соловьев, Платон Николаевич; Afonin, A. O.; Афонин, Алексей Олегович; Belyaev, B. A.; Беляев, Борис Афанасьевич; Boev, N. M.; Боев, Никита Михайлович; Govorun, I. V.; Говорун, Илья Валерьевич; Izotov, A. V.; Изотов, Андрей Викторович; Ugrymov, A. V.; Угрюмов, Андрей Витальевич; Leksikov, An. A.; Лексиков, Андрей Александрович
}
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Synthesis and optical properties of nickel-doped copper metaborate crystals / A. D. Molchanova, E. M. Moshkina, M. S. Molokeev [et al.] // Opt. Spectrosc. - 2022. - Vol. 130, Is. 1. - P. 105-109, DOI 10.21883/EOS.2022.01.52994.41-21. - Cited References: 18. - The study was performed with the support of Russian Science Foundation, RSF grant № 19-12-00413 . - ISSN 0030-400X. - ISSN 1562-6911
Кл.слова (ненормированные):
3d-ions -- crystal growth -- optical spectroscopy -- magnetic ordering -- cuprates
Аннотация: This work presents information on the growth and spectroscopic study of single crystals of copper metaborate doped with nickel Cu1–xNixB2O4 (x = 0.05, 0.1). In the absorption spectra of both crystals, satellites related to Cu centers distorted by impurity Ni atoms were observed near the lines of zero phonon transitions. Polarization studies in the isotropic ab-plane of the tetragonal crystal Cu1–xNixB2O4 show the presence of linear magnetic dichroism in the magnetically ordered state, which was previously observed both in manganese-doped and undoped copper metaborates CuB2O4. The temperature of magnetic phase transitions into the collinear antiferromagnetic and into helicoidal structures, TN = 19.1 K and T* = 8.6 K, respectively, were determined from the temperature dependence of the dichroic signal.

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Держатели документа:
Institute of Spectroscopy, Russian Academy of Sciences, Troitsk, Moscow, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, Krasnoyarsk, Russia
Siberian Federal University, Krasnoyarsk, Russia
Scientific and innovative management, Kemerovo State University, Kemerovo, Russia

Доп.точки доступа:
Molchanova, A. D.; Moshkina, E. M.; Мошкина, Евгения Михайловна; Molokeev, M. S.; Молокеев, Максим Сергеевич; Tropina, E. V.; Bovina, A. F.; Бовина, Ася Федоровна; Boldyrev, K. N.
}
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Improving corrosion resistance of Cu-Al-based anodes in KF-AlF3-Al2O3 melts / S. K. Padamata, A. Yasinskiy, A. Shabanov [et al.] // Trans. Nonferrous Met. Soc. China. - 2022. - Vol. 32, Is. 1. - P. 354-363, DOI 10.1016/S1003-6326(22)65800-X. - Cited References: 24. - The work is performed as a part of the State Assignment for the Science of Siberian Federal University, Russia (No. FSRZ-2020-0013) . Use of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS" is acknowledged . - ISSN 1003-6326. - ISSN 2210-3384

РУБ Metallurgy & Metallurgical Engineering
Рубрики:
NI-FE
   ALUMINUM ELECTROLYSIS
   INERT ANODES
   NICKEL FERRITE
   BEHAVIOR
Кл.слова (ненормированные):
inert anodes -- potassium cryolite -- Cu-Al alloys -- corrosion -- aluminium electrolysis -- oxygen-evolving electrodes
Аннотация: The anodic behaviour of pre-oxidised and non-oxidised Cu−Al-based anodes (Cu−10Al and Cu−9.8Al−2Mn) in KF−AlF3−Al2O3 melts was studied through galvanostatic and potentiodynamic polarization techniques. The alloy compositions were oxidised for a short-term (8 h) at 700 °C, followed by galvanostatic polarization for 1 h at 800 °C with an applied current density of 0.4 A/cm2. The potentiodynamic curves were recorded with a sweep rate of 0.01 V/s. XRD analysis was conducted on frozen melt samples collected on the surface of the anode, and SEM observation was performed on the anode after the experiment to study the phases of the scales formed on the alloys. All the anode materials had a steady potential between 2.30 and 2.50 V(vs Al/AlF3). The corrosion rates of the anodes were calculated from the data acquired through potentiodynamic polarization. It was seen that pre-oxidised anodes possess a low corrosion rate compared to those without pre-oxidation treatment.

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Держатели документа:
Siberian Fed Univ, Lab Phys & Chem Met Proc & Mat, Krasnoyarsk, Russia.
Krasnoyarsk Sci Ctr SB RAS, Lab Mol Spect, Krasnoyarsk, Russia.
Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China.

Доп.точки доступа:
Padamata, Sai Krishna; Yasinskiy, Andrey; Shabanov, A. V.; Шабанов, Александр Васильевич; Bermeshev, Timofey; Yang, You-jian; Wang, Zhao-wen; Cao, Dao; Polyakov, Peter; State Assignment for the Science of Siberian Federal University, Russia [FSRZ-2020-0013]
}
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Metal dusting as a key route to produce functionalized carbon nanofibers / A. R. Potylitsyna, I. V. Mishakov, Y. I. Bauman [et al.] // React. Kinet. Mech. Catal. - 2022. - Vol. 135, Is. 3. - P. 1387-1404, DOI 10.1007/s11144-022-02169-y. - Cited References: 65. - This work was supported by the Ministry of Science and Higher Education of the Russian Federation (Project numbers AAAA-A21-121011390054-1 (ID: 0239-2021-0010) and 121031700315-2) . - ISSN 1878-5190. - ISSN 1878-5204

РУБ Chemistry, Physical
Рубрики:
CHLORINATED HYDROCARBONS
   NI-CU
   DECOMPOSITION
   NANOTUBES
   CATALYST
Кл.слова (ненормированные):
Metal dusting -- Ternary nickel-molybdenum-tungsten alloy -- Trichloroethylene -- Acetonitrile -- Functionalized carbon nanofibers
Аннотация: The present paper reports a new method of producing N-doped carbon nanofibers via metal dusting of a ternary NiMoW alloy in the atmosphere containing C2HCl3 and CH3CN vapors at 600 °C. The initial alloy was prepared by a co-precipitation technique. The carbon deposition was monitored gravimetrically. The early stages of the metal dusting process were studied in detail using scanning and transmission electron microscopies. It was established that the rapid disintegration of the microdispersed NiMoW alloy with the formation of nanosized particles catalyzing the growth of carbon filaments occurs within the first 5 min of the reaction. The presence of C2HCl3 vapors in the reaction medium was shown to be the urgent condition to provide efficient metal dusting. The effect of the CH3CN concentration in the trichloroethylene-containing reaction mixture on the carbon deposition is investigated. As observed, the CH3CN content noticeable affects the carbon yield (after 2 h of reaction). The dome-shaped dependence of carbon yield reaches its maximal value of ~ 200 g/g(cat) at a CH3CN concentration of 33 vol%. According to X-ray photoelectron spectroscopy, the obtained carbon filaments are functionalized with Cl (0.1–1.2 wt%), O (3–6 wt%), and N (0.5–1.3 wt%). The prepared carbon filaments possess a segmented secondary structure, which is typical for carbon nanomaterials derived via catalytic decomposition of chlorine-substituted hydrocarbons. Low-temperature nitrogen adsorption measurement revealed that the specific surface area of the N-containing samples varies in a range from 370 to 550 m2/g.

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Держатели документа:
Boreskov Inst Catalysis, Pr Ac Lavrentieva 5, Novosibirsk 630090, Russia.
Novosibirsk State Univ, Str Pirogova 2, Novosibirsk 630090, Russia.
Nikolaev Inst Inorgan Chem, Ac Lavrentieva 3, Novosibirsk 630090, Russia.
Kirensky Inst Phys, Akad Gorodok 50-38, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Potylitsyna, Arina R.; Mishakov, Ilya, V; Bauman, Yury, I; Kibis, Lidia S.; Shubin, Yury, V; Volochaev, M. N.; Волочаев, Михаил Николаевич; Melgunov, Maxim S.; Vedyagin, Aleksey A.; Ministry of Science and Higher Education of the Russian Federation [AAAA-A21-121011390054-1, 0239-2021-0010, 121031700315-2]
}
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Core-shell and bi-segmented cobalt-nickel nanorods prepared by electroless deposition / E. A. Denisova, L. A. Chekanova, S. V. Komogortsev [et al.] // IEEE Trans. Magn. - 2022. - Vol. 58, Is. 2. - Ст. 2300805, DOI 10.1109/TMAG.2021.3098747. - Cited References: 27. - This work was funded by RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20-43-240003. The authors thank the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center“ Krasnoyarsk Science Center SB RAS” for the provided equipment . - ISSN 0018-9464
Кл.слова (ненормированные):
bi-segmented Co-Ni rods -- core-shell rods -- magnetic properties -- electroless deposition
Аннотация: A porous polymer loaded with segmented nanorods of magnetic metal is very promising for the design of novel microwave devices. Arrays of bi-segmented Ni/Co and core-shell Ni@Co rods were prepared by electroless deposition into porous of polycarbonate track etched membrane. An intrinsic effective magnetic field of the magnetic composite nanorods aligned in the nonmagnetic template was studied by magnetization curves and ferromagnetic resonance. The effect of the interface boundaries for two types of bi-segmented rods with coaxial and along-axis Co/Ni segmentation to effective field was established.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation.
Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation.
Far Eastern Federal University, Vladivostok, 690950, Russian Federation.

Доп.точки доступа:
Denisova, E. A.; Денисова, Елена Александровна; Chekanova, L. A.; Чеканова, Лидия Александровна; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Rautsky, M. V.; Рауцкий, Михаил Владимирович; Nemtsev, I. V.; Немцев, Иван Васильевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Plotnikov, V. S.; Tkachev, V. V.; Li, O. A.; Dolgopolova, M. V.
}
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10.

Molchanova, A. D.
Spectroscopic study and analysis of d-d transitions in Ni ions in nickel orthoborate (Cu, Ni)B2O4 / A. D. Molchanova, K. N. Boldyrev, E. M. Moshkina // 4th International Baltic Conference on Magnetism (IBCM 2021) : Book of abstracts. - 2021. - P. 165. - Cited References: 7. - This work was supported by the Russian Science Foundation, grant № 19-12-00413

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS

Доп.точки доступа:
Boldyrev, K. N.; Болдырев, Кирилл Николаевич; Moshkina, E. M.; Мошкина, Евгения Михайловна; International Baltic Conference on Magnetism: focus on nanobiomedicine and smart materials(4 ; 2021 ; Aug. 29-Sept. 2 ; Svetlogorsk, Russia); Балтийский федеральный университет им. И. Канта
}
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