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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chzhan A. V., Podorozhnyak S. A., Mal'tsev V. K., Krayukhin I. N., Patrin G. S.
Заглавие : Allotropic modifications of cobalt upon chemical deposition
Место публикации : Phys. Solid State. - 2021. - Vol. 63, Is. 1. - P.42-46. - ISSN 10637834 (ISSN), DOI 10.1134/S1063783421010054
Примечания : Cited References: 17. - This study was supported in part by the Russian Foundation for Basic Research, project no. 18-02-00161-a
Аннотация: The effect of the solution acidity on the crystal structure of cobalt during its chemical deposition is reported. It has been shown using the structural and magnetic examination and nuclear magnetic resonance study that the change in the working solution acidity leads to deposition of cobalt with different allotropic modifications in the nearest environment: the hcp type in the small (up to ~8.5) pH region and the fcc type in the large (over ~8.5) pH region. The formation of these cobalt modifications is attributed to the size effects caused by a decrease in the particle size with increasing pH.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mironov V. L., Sukhovskii A. A., Lukin Y. I., Aleksandrova I. P.
Заглавие : Measurement of the maximum content of bound water in bentonitic clay using dielectric and NMR methods
Место публикации : Russ. Phys. J.: SPRINGER, 2011. - Vol. 54, Is. 1. - P.71-76. - ISSN 1064-8887
Примечания : Cited References: 4
Ключевые слова (''Своб.индексиров.''): dielectric permittivity--nuclear magnetic resonance--bentonitic clay--bound water
Аннотация: An investigation of moisture dependences of refractive index and spectral width of the nuclear magnetic resonance (NMR) is performed for bentonitic clay specimens at different temperatures. These moisture dependences allowed identifying two types of moisture: bound and free water. The maximum content of water in the bentonitic clay is measured.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivanov Y. N., Totz J., Michel D., Klotzsche G., Sukhovsky A. A., Aleksandrova I. P.
Заглавие : Chemical exchange in NH4HSeO4 single crystals studied by two-dimensional H-2 nuclear magnetic resonance
Разночтения заглавия :авие SCOPUS: Chemical exchange in NH4HSeO4 single crystals studied by two-dimensional 2H nuclear magnetic resonance
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 1999. - Vol. 11, Is. 18. - P.3751-3760. - ISSN 0953-8984, DOI 10.1088/0953-8984/11/18/310
Примечания : Cited References: 16
Предметные рубрики: PHASE-TRANSITIONS
CONDUCTIVITY PROCESSES
AMMONIUM
Ключевые слова (''Своб.индексиров.''): hydrogen bonds--nuclear magnetic resonance--single crystals--thermal effects--ammonium hydrogen selenate--ammonium compounds
Аннотация: Processes of chemical exchange of deuterons in partially deuterated ammonium hydrogen selenate, NH4HSeO4 (AHSe), crystals are investigated by means of H-2 nuclear magnetic resonance (NMR) experiments over a wide temperature range. The temperature dependencies of the quadrupole line splittings in the one-dimensional spectra of AHSe above 350 K revealed lineshape changes which are characteristic for chemical exchange processes. A detailed study of these exchange processes in AHSe is achieved by means of two-dimensional H-2 NMR experiments. In the temperature range investigated, a chemical exchange occurs only between those deuteron (proton) sites which are involved in hydrogen bonds (alpha- and beta-positions). It was established that the rates of exchange between all types of hydrogen-bound deuteron are approximately the same. Exchange between these positions and the deuterons in the ND4 groups could not be detected. On the basis of our findings, we finally discuss a model for the microscopic mechanism of hydrogen transport in AHSe.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chzhan A.V., Patrin G. S., Kiparisov S. Ya., Seredkin V. A., Maltsev V. K., Krayukhin I. N.
Заглавие : The induced anisotropy and its influence on absorption of the NMR and domain structure of Co-P amorphous films
Коллективы : Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : Solid State Phenomena. - 2011. - Vol. 168-169. - P.145-148. - ISSN 10120394 ; 9783037850213, DOI 10.4028/www.scientific.net/SSP.168-169.145
Ключевые слова (''Своб.индексиров.''): amorphous magnetic films--coercive force--domain structure--induced anisotropy--nuclear magnetic resonance--amorphous films--cobalt--coercive force--crystals--magnetic anisotropy--magnetic devices--magnetic domains--magnetic films--metallic films--palladium--resonance--amorphous films--anisotropy--cobalt--coercive force--magnetic anisotropy--magnetism--palladium--amorphous magnetic films--domain structure--experimental research--induced anisotropy--intermediate layers--magnetization process--co-p films--nuclear magnetic resonance(nmr)--nuclear magnetic resonance--nuclear magnetic resonance
Аннотация: The results of experimental research into magnetic properties of amorphous Co-P films obtained by chemical sedimentation on various intermediate layers have been represented. The nuclear magnetic resonance (NMR) spectra of films sedimentated on intermediate layers of Pd crystal and amorphous NiP compound have been measured .The features of formation of domain structures and magnetization processes in the presence and absence of the induced anisotropy have been described.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Morozov E. V., Il’ichev A. V., Bouznik V. M.
Заглавие : Magnetic resonance imaging study of water absorption of polymer composite materials subjected to mechanical and temperature impact
Колич.характеристики :9 с
Место публикации : Russ. J. Phys. Chem. B. - 2023. - Vol. 17, Is. 6. - P.1361-1369. - ISSN 19907931 (ISSN), DOI 10.1134/S1990793123060064. - ISSN 19907923 (eISSN)
Примечания : Cited References: 18. - The research was carried out as part of a state assignment of the Institute of Chemistry and Chemical Technology of the Siberian Branch of the Russian Academy of Sciences (project no. 0287-2021-0012) using the equipment of the Krasnoyarsk Regional Center for Collective Use of the Federal Research Center "Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences"
Аннотация: The results of a study of water absorption processes by samples of polymer composite materials (PCMs) based on fiberglass, subjected to low-speed impact with controlled impact energy and alternating temperature cycling are presented. Using magnetic resonance imaging (MRI), the distribution of absorbed water in the fiberglass structure is visualized and the dynamics of its accumulation in various areas of the sample are studied. It is found that mechanical impact leads to a nonuniform distribution of the absorbed water in the samples and a significant accumulation of free water in the areas of destruction and adjacent layers in the event of a violation of the integrity of the outer layer of the material. It is shown that cyclic alternating temperature effects do not lead to a noticeable change in the water absorption processes and are comparable in effect to mechanical nondestructive impacts. The results obtained using MRI are in close agreement with the data of traditional weight measurements, which shows the effectiveness of the method in diagnosing defects and mechanical damage to PCMs exposed to the humid environment.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Antonova A.B., Chudin O.S., Pavlenko N.I., Sokolenko W.A., Rubaylo A.I., Vasiliev A. D., Semeikin O.V.
Заглавие : Chemistry of vinylidene complexes. XVIII. Synthesis and molecular structure of the novel trinuclear mu(3)-vinylidene complex CpReFePt(mu(3)-C=CHPh)(CO)(6)(PPh(3))
Место публикации : J. Organomet. Chem. - 2009. - Vol. 694, Is. 1. - P.127-130. - ISSN 0022-328X, DOI 10.1016/j.jorganchem.2008.08.037
Примечания : Cited Reference Count: 17. - Гранты: This work was supported by the Council of the Russian Federation President for Support of Young Scientists and Leading Scientific Schools (Project No. NSch-4137.2006.2) and the Krasnoyarsk Regional Science Foundation (Grants 10TS145 and 17G002).Финансирующая организация: Council of the Russian Federation President for Support of Young Scientists and Leading Scientific Schools [NSch-4137.2006.2]; Krasnoyarsk Regional Science Foundation [10TS145, 17G002]
Предметные рубрики: CLUSTERS
CRYSTAL
MNFEPT
Ключевые слова (''Своб.индексиров.''): vinylidene complexes--heterometallic clusters--rhenium--iron--platinum--crystal structure--crystal structure--heterometallic clusters--iron--platinum--rhenium--vinylidene complexes--atomic physics--atoms--bond length--chemical bonds--coordination reactions--crystal structure--iron compounds--nuclear magnetic resonance--nuclear magnetic resonance spectroscopy--platinum--quantum chemistry--rhenium--rhenium compounds--bond angles--co groups--double bonds--fe atoms--heterometallic--heterometallic clusters--pt atoms--trimetallic--vinylidene complexes--x-ray diffractions--platinum compounds
Аннотация: The interaction between Cp(CO)(2)RePt(mu-C=CHPh)(PPh(3))(2) (1) and Fe(2)(CO)(9) afforded the new heterometallic mu(3)-vinylidene cluster CpReFePt(mu(3)-C=CHPh)(CO)(6)(PPh(3)) (2). An X-ray diffraction study shows the complex 2 possesses a trimetallic Re-Fe-Pt chain core. The bond lengths are Re-Fe 2.8221(8), Fe-Pt 2.5813(8) angstrom; the Re center dot center dot center dot Pt distance is 3.3523(7) angstrom; the bond angle Re-Fe-Pt is 76.55(3)degrees. The mu(3)-C=CHPh ligand is eta(1)-bound to the Re and Pt atoms and eta(2)-coordinated to the Fe atom. The C=C bond length is 1.412(4) angstrom. The Pt atom is coordinated by the PPh(3) and CO groups. Complex 2 is characterized by the IR and (1)H, (13)C and (31)P NMR spectra. (C) 2008 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova E. A., Iskhakov R. S., Stolyar S. V., Komogortsev S. V., Chekanova L. A., Maltsev V. K., Kalinin Y. E., Sitnikov A. V.
Заглавие : Exchange interaction in the Co-SiO2 nanocomposite films
Место публикации : TRENDS IN MAGNETISM. - 2011. - Vol. 168-169. - С. 265-268. - ISSN 10120394 (ISSN); 9783037850213 (ISBN), DOI 10.4028/www.scientific.net/SSP.168-169.265
Ключевые слова (''Своб.индексиров.''): exchange coupling parameter--ferromagnetic resonance--granular composite films--cobalt--exchange coupling--exchange interactions--ferromagnetic materials--ferromagnetic resonance--ferromagnetism--magnetic resonance measurement--nanocomposite films--nanocomposites--nuclear magnetic resonance--resonance--silicon compounds--spin waves--cobalt--exchange coupling--exchange interactions--ferromagnetic materials--ferromagnetic resonance--ferromagnetism--magnetic resonance measurement--magnetism--nanocomposite films--nuclear magnetic resonance--spin fluctuations--spin waves--co content--coupling parameters--dispersion relations--granular composite films--magnetic measurements--nanogranulars--nmr studies--structural state--granular composites--nano-granular--standing spin waves--composite films--composite films
Аннотация: The properties of Co-SiO2 nanogranular composite films, containing a Co volume fraction ranging from 0.3 to 0.8, have been characterized by means of magnetic measurements, NMR study, and ferromagnetic resonance. Thermal decrease of CoX(SiO2)100-X magnetization follows the T3/2 law and allows to estimate the exchange interaction constant A. With growing nominal Co content the transitions from granular to continuous structural state at 36% Co are registered by FMR measurements. The spectrum of standing spin-wave has been detected in the perpendicular experiment configuration for films with the Co content above 52 vol. %. It is found that the type of the dispersion relation of spin waves in Co-SiO2 composite films is affected by the exchange coupling fluctuations.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zobov V. E., Popov M. A.
Заглавие : On the coordinate of a singular point of time correlation functions for the system of nuclear magnetic moments of a crystal
Место публикации : J. Exp. Theor. Phys.: AMER INST PHYSICS, 2003. - Vol. 97, Is. 1. - P78-84. - ISSN 1063-7761, DOI 10.1134/1.1600799
Примечания : Cited References: 22
Предметные рубрики: DIPOLAR FLUCTUATION SPECTRUM
FREE-INDUCTION DECAY
CROSS-RELAXATION
DOUBLE-RESONANCE
SPIN SYSTEMS
NMR-SPECTRA
LINE SHAPE
IRREVERSIBILITY
ABSORPTION
CAF2
Ключевые слова (''Своб.индексиров.''): absorption spectroscopy--barium compounds--crystallography--lattice constants--magnetic fields--nuclear magnetic resonance--absorption spectrum--dipole-dipole interaction--magnetic field directions--nuclear magnetic moments--magnetic moments
Аннотация: The hypothesis concerning the existence of singular points on the imaginary time axis for a correlation function of a system with the dipole-dipole interaction of nuclear spins of a crystal is verified. Within the framework of the self-consistent fluctuating field theory taking into account the principal corrections related to the correlation of local fields, a result for this coordinate is obtained in terms of the ratios of lattice sums. Experimental values of this coordinate are calculated from the wings of the nuclear magnetic resonance absorption spectrum of a BaF2 crystal for the magnetic field directions along the three crystallographic axes. Good agreement of the theoretical and experimental results justifies this hypothesis. (C) 2003 MAIK "Nauka / Interperiodica".
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Shauro V. P.
Заглавие : Exact solutions for time-optimal control of spin I=1 by NMR
Коллективы : Russian Foundation for Basic Research [14-07-31086]
Место публикации : Quantum Inf. Process.: Springer, 2015. - Vol. 14, Is. 7. - P.2345-2355. - ISSN 1570, DOI 10.1007/s11128-015-0999-8. - ISSN 15731332(eISSN)
Примечания : Cited References:34. - The author thanks V.E. Zobov for fruitful discussions. This study was supported by the Russian Foundation for Basic Research, Project No. 14-07-31086.
Предметные рубрики: QUANTUM COMPUTATION
SYSTEMS
Ключевые слова (''Своб.индексиров.''): quantum gate--qutrit--time-optimal control--nuclear magnetic resonance
Аннотация: We consider the problem of time-optimal control of quadrupole nucleus with the spin I = 1 by NMR. In contrast to the conventional methods based on selective pulses, the control is implemented using nonselective pulses separated by free-evolution intervals. Using the Cartan decomposition, the system of equations is obtained for finding parameters of a control field. Partial time-optimal solutions for the important single-qutrit gates (selective rotations and quantum Fourier transform) are found. The strong dependence of minimum gate implementation times on global phase of the gate is observed. The analytical values of minimum times are consistent with the numerical data.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zobov V. E.
Заглавие : Quantum and classical correlations in high temperature dynamics of two coupled large spins : conference paper
Коллективы : International Conference on Micro- and Nano-Electronics (Oct. 1-5, 2012; Zvenigorod, Russia)
Место публикации : Proc. SPIE. - 2012. - Vol.8700. - Ст.87001D. - P. - ISSN 0277-786X, DOI 10.1117/12.2016982. - ISSN 978-081949487-0
Примечания : Cited References: 17
Ключевые слова (''Своб.индексиров.''): dynamical correlations--measurement--mutual information--nuclear magnetic resonance--spin coherent states
Аннотация: We study dynamical correlations of two coupled large spins depending on the time and on the spin quantum numbers. In the high-temperature approximation, we obtain analytical expressions for the mutual informations, quantum and classical parts of correlations. The latter was obtained performing the non-orthogonal projective (POVM) measurements onto the spin coherent states of two spins or one spin, as well as by means of the orthogonal projective measurement of von Neumann. Contribution from quantum correlations is much less than that from classical ones and decreasing with the increase in spin quantum numbers at short times. However, it is not so in a time equal to half of the quantum period. © 2012 SPIE.
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