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Raman investigation of hydrostatic and nonhydrostatic compressions of OH- and F-apophyllites up to 8 GPa / S. V. Goryainov [et al.] // J. Raman Spectrosc. - 2012. - Vol. 43, Is. 3. - P. 439-447, DOI 10.1002/jrs.3049. - Cited References: 18. - This work was supported by the Siberian Division of RAS (Integration Project 109), the Russian Ministry of Science and Education and the CRDF (BRHE - REC-008 grant) and the Russian Foundation for Basic Research (RFBR-11-05-01121). . - ISSN 0377-0486

РУБ Spectroscopy
Рубрики:
RADIATION-INDUCED DEFECTS
   ALPHA-QUARTZ
   ROOM-TEMPERATURE
   MEMORY GLASS
   PRESSURE
   FLUORAPOPHYLLITE
   PHASE
   MODEL
Кл.слова (ненормированные):
Raman spectroscopy -- high pressure -- apophyllite -- layer silicate -- amorphization
Аннотация: Layer silicates F- and OH-apophyllites, KCa4Si8O20(F, OH)·8H2O, have been investigated by Raman spectroscopy at hydrostatic and nonhydrostatic pressures up to 8 GPa in diamond anvil cells using a 4 : 1 methanol–ethanol mix as pressure-transmitting medium. Our experiments show that at hydrostatic compression, apophyllites retain their crystalline states (i.e. no amorphization) up to 5 GPa. The wavenumbers of most bands exhibit linear dependences on pressure, except for a few ones, e.g. at 162 and 3565 cm–1 in OH-form (160.5 and 3558 cm–1 in F-form) that show nonlinear dependences. Nonhydrostatic compression with additional uniaxial loading induces amorphization of apophyllites. The majority of the bands in OH-apophyllite decreases markedly in intensity and shows considerable broadening under nonhydrostatic compression up to 3–6 GPa. In addition, the wavenumbers of several bands at nonhydrostatic compression exhibit considerable nonlinear dependences on pressure with strong hysteresis. These bands are mainly associated with vibrations of the interlayer ions and molecules and also of stretching and bending silicate sheets, hence being highly sensitive to the interlayer distance. Finally, we have calculated the lattice dynamics of F-apophyllite and interpreted the majority of bands, and these data are used to explain the complex baric behavior of the bands. Copyright © 2011 John Wiley & Sons, Ltd.

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Держатели документа:
[Goryainov, Sergei V.
Madyukov, Iliya A.] SB RAS, Inst Geol & Mineral, Novosibirsk 630090, Russia
[Goryainov, Sergei V.
Pan, Yuanming] Univ Saskatchewan, Dept Geol Sci, Saskatoon, SK S7N 5E2, Canada
[Goryainov, Sergei V.] Novosibirsk State Univ, Novosibirsk 630090, Russia
[Krylov, Alexander S.
Vtyurin, Alexander N.] SB RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Smirnov, Mikhail B.] St Petersburg State Univ, Fac Phys, St Petersburg 198504, Russia

Доп.точки доступа:
Goryainov, S. V.; Krylov, A. S.; Крылов, Александр Сергеевич; Pan, Y. M.; Madyukov, I. A.; Smirnov, M. B.; Vtyurin, A. N.; Втюрин, Александр Николаевич
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Udod, L. V.
NMR-study of the crystalline and amorphous CuB2O4 / L. V. Udod, K. A. Sablina, Y. N. Ivanov // J. Supercond. Nov. Magn. - 2007. - Vol. 20, Is. 2. - P. 183-186, DOI 10.1007/s10948-006-0122-6. - Cited References: 9 . - ISSN 1557-1939

РУБ Physics, Applied + Physics, Condensed Matter
Рубрики:
COPPER METABORATE
BORATE GLASSES
Кл.слова (ненормированные):
Amorphous states -- Copper metaborate -- Amorphization -- Amorphous materials -- Crystalline materials -- Ground state -- Magnetic properties -- Molecular structure -- Nuclear magnetic resonance spectroscopy -- Copper compounds
Аннотация: B-11 nuclear magnetic resonance (NMR) spectroscopy was applied to study the crystalline, amorphous and crystallizing from an amorphous states of copper metaborate. The occurrence of trigonal BO3 units at the expense of converting tetragonal BO4 units was observed in amorphous CuB2O4. This fact explains the essential change of CuB2O4 magnetic properties under amorphization.

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Держатели документа:
RAS, SB, LV Kirensky Inst Phys, Krasnoyarsk 660036, Russia
ИФ СО РАН
L. V. Kirensky Institute of Physics, SB, RAS, Akademgorodok, 660036, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Sablina, K. A.; Саблина, Клара Александровна; Ivanov, Y. N.; Иванов, Юрий Николаевич; Удод, Любовь Викторовна
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Structural phase transitions in flexible DUT-8(Ni) under high hydrostatic pressure / A. Krylov, I. Yushina, E. Slyusareva [et al.] // Phys. Chem. Chem. Phys. - 2022. - Vol. 24, Is. 6. - P. 3788-3798, DOI 10.1039/d1cp05021d. - Cited References: 57. - This work was financially supported by the RFBR (Russian Foundation for Basic Research, project number: 21-52-12018) and DFG (Deutsche Forschungsgemeinschaft, project number: 448809307). The Raman and high hydrostatic pressure experiments were performed in the Center for Common Use of the Krasnoyarsk Scientific Center SB RAS. The authors thank M. Maliuta for sample synthesis and characterisation . - ISSN 1463-9076. - ISSN 1463-9084

РУБ Chemistry, Physical + Physics, Atomic, Molecular & Chemical
Рубрики:
METAL-ORGANIC FRAMEWORK
   RAMAN-SPECTROSCOPY
   PORE-SIZE
   AMORPHIZATION
Аннотация: The behaviours of the open pore (op) and closed pore (cp) phases of the flexible Ni2(ndc)2(dabco) (ndc – 2,6-naphthalene dicarboxylate, dabco – 1,4-diazabicyclo[2.2.2]octane, DUT-8(Ni)) metal–organic framework under high hydrostatic pressures up to 10 GPa in isopropanol and silicone oil were studied by Raman spectroscopy. Ab initio simulations of vibrational spectra were performed for the open and closed pore phases, which allowed us to disclose the characteristic vibrational modes affected by the structural transitions under pressure. Analysis of theoretical and experimental Raman data suggests that the op–cp transition involves gateway vibrations at 25 and 67 cm−1, corresponding to trampoline/rotational motions of aromatic linkers. The experiments reveal the formation of new distorted cp phases at pressures higher than 2 GPa, which are formed without amorphisation. The transition between the cp phase and the distorted cp phase is reversible. The experiments also reveal the pivotal role of the pressure transmitting medium on the phase transition behaviour.

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Держатели документа:
Fed Res Ctr KSC SB RAS, Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
South Ural State Univ, SEC Nahenotechnol, Lenin Ave 76, Chelyabinsk 454080, Russia.
Siberian Fed Univ, Svobodny Prospect 79, Krasnoyarsk 660041, Russia.
Tech Univ Dresden, Chair Inorgan Chem 1, Bergstr 66, D-01062 Dresden, Germany.

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Yushina, Irina; Slyusareva, Evgenia; Krylova, S. N.; Крылова, Светлана Николаевна; Vtyurin, A. N.; Втюрин, Александр Николаевич; Kaskel, Stefan; Senkovska, Irena; RFBR (Russian Foundation for Basic Research)Russian Foundation for Basic Research (RFBR) [21-52-12018]; DFG (Deutsche Forschungsgemeinschaft)German Research Foundation (DFG) [448809307]
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