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Synthesis and structural properties of cubic G0-Rb2KMoO3F3 oxyfluoride / V. V. Atuchin [et al.] // Ceram. Int. - 2012. - Vol. 38, Is. 3. - P. 2455-2459, DOI 10.1016/j.ceramint.2011.11.013. - Cited References: 23. - This study was partly supported by RFBR (Grant 09-02-00062) and SB RAS (Grant 34). . - ISSN 0272-8842

РУБ Materials Science, Ceramics
Рубрики:
PHASE-TRANSITIONS
   FERROELECTRIC K3WO3F3
   (NH4)(3)MOO3F3
   TEMPERATURE
   PEROVSKITE
   ELPASOLITE
   CRYSTALS
   BEHAVIOR
   High temperature
   Melt solidification
   Micromorphologies
   Melt solidification
   Microstructure-final
   Oxyfluorides
   Space Groups
   Oxyfluorides
   X ray methods
Кл.слова (ненормированные):
Powders: solid state reaction -- Microstructure-final -- X-ray methods -- Alkali oxides -- Halides
Аннотация: High-temperature G0 polymorph of Rb2KMoO3F3 has been prepared by melt solidification. Micromorphology and chemical properties of the final product were evaluated by scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The elpasolite-related crystal structure of G0-Rb2KMoO3F3 has been refined by Rietveld method at T = 298 K (space group Fm-3m, a = 8.92446(8) Å, V = 710.76(1) Å3; RB = 3.55%). Ferroelectric G1-Rb2KMoO3F3 polymorph, earlier reported at T˂328 K, is not found at T = 298 K.

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Держатели документа:
[Atuchin, V. V.] SB RAS, Inst Semicond Phys, Lab Opt Mat & Struct, Novosibirsk 630090 90, Russia
[Gavrilova, T. A.] SB RAS, Inst Semicond Phys, Lab Nanolithog & Nanodiagnost, Novosibirsk 630090 90, Russia
[Isaenko, L. I.
Zhurkov, S. A.] SB RAS, Inst Geol & Mineral, Lab Crystal Growth, Novosibirsk 530090 90, Russia
[Kesler, V. G.] SB RAS, Inst Semicond Phys, Lab Phys Principles Integrated Microelect, Novosibirsk 630090 90, Russia
[Molokeev, M. S.] SB RAS, Inst Phys, Lab Crystal Phys, Krasnoyarsk 660036 36, Russia

Доп.точки доступа:
Atuchin, V. V.; Gavrilova, T. A.; Isaenko, L. I.; Kesler, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Zhurkov, S. A.
}
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Crystal structure and electronic states of Co and Gd ions in a Gd0.4Sr0.6CoO2.85 single crystal / M. S. Platunov [et al.] // JETP Letters. - 2016. - Vol. 103, Is. 3. - P. 196-200, DOI 10.1134/S0021364016030139. - Cited References:20. - This work was supported in part by the Russian Foundation for Basic Research (project nos. 13-02-00958, 13-02-00358, 14-02-31051, and 16-32-60049), by the Council of the President of the Russian Federation for Support of Young Scientists and Leading Scientific Schools (project no. SP-938.2015.5), and by the program "UMNIK." The X-ray diffraction and thermochemical studies were supported by the Siberian Branch, Russian Academy of Sciences (project no. V.45.3.1). . - ISSN 0021-3640. - ISSN 1090-6487

РУБ Physics, Multidisciplinary
Рубрики:
X-RAY-ABSORPTION
   PROFILE REFINEMENT
   PEROVSKITE
   CHARGE
   SPIN
Аннотация: X-ray diffraction and X-ray absorption near edge structure (XANES) spectra have been measured at the Со K-edge and Gd L3-edge in GdCoO3 and Gd0.4Sr0.6CoO2.85 cobaltites. The effect of Sr substitution on the crystal structure and electronic and magnetic states of Co3+ ions in a Gd0.4Sr0.6CoO2.85 single crystal has been analyzed. The XANES measurements at the Co K-edge have not showed a noticeable shift of the absorption edge with an increase in the concentration of Sr. This indicates that the effective valence of cobalt does not change. An increase in the intensity of absorption at the Gd L3-edge is due to an increase in the degree of hybridization of the Gd(5d) and O(2p) states. The effect of hole doping on the magnetic properties results in the appearance of the ferromagnetic component and in a significant increase in the magnetic moment.

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Публикация на русском языке Кристаллическая структура и электронные состояния ионов Co и Gd в монокристалле Gd0.4Sr0.6CoO2.85 [Текст] / М. С. Платунов [и др.] // Письма в Журн. эксперим. и теор. физ. : Наука, 2016. - Т. 103 Вып. 3-4. - С. 214-219

Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.
Russian Acad Sci, Inst Chem & Chem Technol, Siberian Branch, Krasnoyarsk 660036, Russia.
Natl Res Ctr Kurchatov Inst, Pl Akad Kurchatova 1, Moscow 123182, Russia.
Natl Res Nucl Univ MEPhI, Kashirskoe Sh 31, Moscow 115409, Russia.

Доп.точки доступа:
Platunov, M. S.; Платунов, Михаил Сергеевич; Dudnikov, V. A.; Дудников, Вячеслав Анатольевич; Orlov, Yu. S.; Орлов, Юрий Сергеевич; Kazak, N. V.; Казак, Наталья Валерьевна; Solovyov, L. A.; Соловьев, Леонид Александрович; Zubavichus, Y. V.; Veligzhanin, A. A.; Dorovatovskii, P. V.; Vereshchagin, S. N.; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Russian Foundation for Basic Research [13-02-00958, 13-02-00358, 14-02-31051, 16-32-60049]; Council of the President of the Russian Federation for Support of Young Scientists and Leading Scientific Schools [SP-938.2015.5]; program "UMNIK"; Siberian Branch, Russian Academy of Sciences [V.45.3.1]
}
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Zinenko, V. I.
Lattice dynamics of BiFeO3: The untypical behavior of the ferroelectric instability under hydrostatic pressure / V. I. Zinenko, M. S. Pavlovskii // JETP Letters. - 2008. - Vol. 87, Is. 6. - P. 288-291, DOI 10.1134/S0021364008060052. - Cited References: 15 . - ISSN 0021-3640

РУБ Physics, Multidisciplinary
Рубрики:
AB-INITIO CALCULATIONS
PEROVSKITE
Аннотация: Within a nonempirical model of an ionic crystal with the inclusion of the dipole and quadrupole ion polarizations, the lattice vibrational frequencies, high-frequency dielectric constant, Born dynamic charges, and the elasticity moduli of the BiFeO3 crystal have been calculated and their dependencies on the hydrostatic pressure in the cubic, rhombic, and rhombohedral phases have been determined. The results indicate the presence of the ferroelectric instability, which depends weakly on the pressure in all of the phases investigated. The dependence of the crystal lattice dynamics on the applied pressure for the cubic phases of BiAlO3, BaTiO3, and PbTiO3 has been calculated for comparison.

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Держатели документа:
[Zinenko, V. I.
Pavlovskii, M. S.] Russian Acad Sci, Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk 660036, Russian Federation

Доп.точки доступа:
Pavlovskii, M. S.; Павловский, Максим Сергеевич; Зиненко, Виктор Иванович
}
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Na-23 NMR study of the local order in the Na1/2Bi1/2TiO3 structure in a weak magnetic field / I. P. Aleksandrova [et al.] // Phys. Solid State. - 2008. - Vol. 50, Is. 3. - P. 496-501, DOI 10.1134/S1063783408030177. - Cited References: 14 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
PEROVSKITE
Аннотация: The orientation dependences of the second-order quadrupole shifts of the central component in the Na-23 NMR spectrum were studied in the temperature range 293-760 K. The profile of the spectral distribution is calculated using various models of the Na1/2Bi1/2TiO3 structure. The calculations agree with the experimental data for the monoclinic structure of a polar cluster with two Na displacement components: a displacement along the [111](P) direction and a small displacement statistically or dynamically disordered over six equally probable [100](P)-type directions. Tetragonal-phase nuclei and monoclinic clusters with a very small displacement component along the [111](P) direction are found to coexist and have close energies over the temperature range 580-610 K. The results obtained provide new information concerning the character of the diffuse phase transition at 610 K.

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Держатели документа:
[Aleksandrova, I. P.
Sukhovskii, A. A.
Ivanov, Yu. N.
Yablonskaya, Yu. E.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Vakhrushev, S. B.] Russian Acad Sci, AF Ioffe Physicotech Inst, St Petersburg 194021, Russia
ИФ СО РАН

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Ivanov, Y. N.; Иванов, Юрий Николаевич; Yablonskaya, Y. E.; Vakhrushev, S. B.
}
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Low-temperature magnetic behavior of the rare-earth cobaltites GdCoO3 and SmCoO3 / N. B. Ivanova [et al.] // Phys. Solid State. - 2007. - Vol. 49, Is. 11. - P. 2126-2131, DOI 10.1134/S1063783407110182. - Cited References: 32. - This study was supported by the Branch of General Physics and Astronomy of the Russian Academy of Sciences within the framework of the program “Strong Electron Correlations” and the Russian Science Support Foundation . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
METAL-INSULATOR-TRANSITION
   RCOO3 R
   SPIN-STATE
   OXIDE
   SM
   ND
   PEROVSKITE
   GLASSES
   PR
   EU
Аннотация: The temperature and magnetic field dependences of the static magnetization of the polycrystalline rare-earth cobaltites GdCoO3 and SmCoO3 have been measured. It is shown that, below room temperature, the magnetization of both compounds derives primarily from the rare-earth ion paramagnetism. The GdCoO3 and SmCoO3 compounds have been found to differ substantially in magnetic behavior, which can be traced to differences in their electronic shell structures. The magnetic behavior of GdCoO3 is close to that of an array of free Gd3+ ions, whereas in SmCoO3 the deviation from the free-ion properties is very large because of the Sm3+ ground state being crystal-field split. Van Vleck magnetic susceptibility measurements of SmCoO3 suggest that the splitting is similar to 10 K.

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Публикация на русском языке Сравнение одноэлектронного и многоэлектронного механизмов концентрационной зависимости зонной структуры ВТСП-купратов [Текст] / В. А. Гавричков [и др.] // Физ. тверд. тела. - 2007. - Т. 49 Вып. 11. - С. 1958-1963

Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
Univ Guadalajara, Dept Fis, CUCEI, Guadalajara 44430, Jalisco, Mexico
ИФ СО РАН
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation
Departamento de Fisica, C.U.C.E.I., Universidad de Guadalajara, Guadalajara, Jalisco 44430, Mexico

Доп.точки доступа:
Ivanova, N. B.; Иванова, Наталья Борисовна; Kazak, N. V.; Казак, Наталья Валерьевна; Michel, C. R.; Balaev, A. D.; Балаев, Александр Дмитриевич; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич
}
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Lattice dynamics and ferroelectric instability in ordered and disordered PbSc1/2Ta1/2O3 and PbSc1/2Nb1/2O3 solid solutions / V. I. Zinenko [et al.] // J. Exp. Theor. Phys. - 2007. - Vol. 105, Is. 3. - P. 617-625, DOI 10.1134/S1063776107090191. - Cited References: 23 . - ISSN 1063-7761

РУБ Physics, Multidisciplinary
Рубрики:
RELAXOR FERROELECTRICS
   PHASE-TRANSITION
   LOCAL-STRUCTURE
   PB(SC1/2NB1/2)O-3
   PEROVSKITE
   CRYSTALS
Кл.слова (ненормированные):
Dipole moment -- Lattice vibrations -- Negative ions -- Phonons -- Positive ions -- Solid solutions -- Dynamic Born charges -- Ferroelectric instabilities -- Frequency spectra -- Gordon-Kim models -- Oxygen anions -- Phonon spectra -- Ferroelectricity
Аннотация: The dynamic Born charges and the frequency spectra of lattice oscillations in the crystals of ordered and disordered PbSc1/2Ta1/2O3 (PST) and PbSc1/2Nb1/2O3 (PSN) solid solutions have been calculated within the framework of the generalized Gordon-Kim model with allowance for the dipole and quadrupole polarizabilities. The phonon spectra of both compounds contain ferroelectric soft modes. The influence of various interactions on the magnitude of dynamic charges and ferroelectric instability in PSN and PST solid solutions has been studied and it is shown that both these charges and the ferroelectric instability are determined by the competition between long-range dipole-dipole interactions and short-range dipole-charge interactions, the determining role played by the interaction of Nb (Ta) cations and oxygen anions in the Nb-O (Ta-O) bond direction.

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Div, Krasnoyarsk 660036, Russia
Russian Acad Sci, PN Lebedev Phys Inst, Moscow 119991, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation
Lebedev Physical Institute, Russian Academy of Sciences, Moscow 119991, Russian Federation

Доп.точки доступа:
Zinenko, V. I.; Зиненко, Виктор Иванович; Zamkova, N. G.; Замкова, Наталья Геннадьевна; Maksimov, E. G.; Sofronova, S. N.; Софронова, Светлана Николаевна
}
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Effect of strontium and barium doping on the magnetic state and electrical conductivity of GdCoO3 / N. B. Ivanova [et al.] // Phys. Solid State. - 2007. - Vol. 49, Is. 8. - P. 1498-1506, DOI 10.1134/S1063783407080161. - Cited References: 36 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PEROVSKITE
   ORDER
   OXIDE
   BEHAVIOR
   GLASSES
   LACOO3
   PR
   GD
   SM
   ND
Аннотация: A coordinated investigation of the magnetic and electrical properties of polycrystalline cobalt oxide compounds CdCoO3, Gd0.9Ba0.1CoO3, and Gd0.9Sr0.1CoO3 is carried out. Undoped GdCoO3 reveals a low conductivity; a magnetic moment of 7.4 mu(B) per molecule, which is less than the theoretical value for the Gd3+ ion; and an asymptotic Curie temperature of -6 K. Doping GdCoO3 with barium and strontium to substitution of 10 at. % Gd brings about an increase in the conductivity and magnetic transitions at T = 300 K for Gd0.9Ba0.1CoO3 and T = 170 K for Gd0.9Sr0.1CoO3. The magnetization anomalies imply the formation of magnetic clusters. The behavior of the electrical conductivity at high temperatures suggests a variable activation energy. At low temperatures, Mott hopping conduction sets in.

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Публикация на русском языке Влияние допирования стронцием и барием на магнитное состояние и электропроводность GdCoO[3] [Текст] / Н. Б. Иванова [и др.] // Физ. тверд. тела. - 2007. - Т. 49 Вып. 8. - С. 1427-1435

Держатели документа:
Russian Acad Sci, Siberian Div, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Univ Guadalajara, CUCEI, Dept Fis, Guadalajara 44430, Jalisco, Mexico
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation
Departmento de Fisica, C.U.C.E.I., Universidade de Guadalajara, Guadalajara, Jalisco 44430, Mexico

Доп.точки доступа:
Ivanova, N. B.; Иванова, Наталья Борисовна; Kazak, N. V.; Казак, Наталья Валерьевна; Michel, C. R.; Balaev, A. D.; Балаев, Александр Дмитриевич; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Bulina, N. V.; Булина, Наталья Васильевна; Panchenko, E. B.
}
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Zinenko, V. I.
Statistical mechanics of cation ordering in PbSc1/2Ta1/2O3 and PbSc1/2Nb1/2O3 solid solutions / V. I. Zinenko, S. N. Sofronova // Phys. Solid State. - 2005. - Vol. 47, Is. 12. - P. 2309-2314, DOI 10.1134/1.2142896. - Cited References: 17 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITION
   PEROVSKITE
   DISORDER
   FERROELECTRICS
   CRYSTALS
   MODEL
Аннотация: A model Hamiltonian for B cation ordering (Sc-Nb(Ta)) in PbSc1/2Nb1/2O3 and PbSc1/2Ta1/2O3 solid solutions is constructed. The parameters of the model Hamiltonian are determined from the ab initio calculation within the ionic crystal model with allowance made for the deformability and the dipole and quadrupole polarizabilities of the ions. The temperatures of the phase transition due to the ordering of the B cations are calculated by the Monte Carlo method in the mean-field and cluster approximations. The phase transition temperatures calculated by the Monte Carlo method (1920 K for PbSc1/2Ta1/2O3 and 1810 K for PbSc1/2Nb1/2O3) are consistent with the experimental data (1770 and 1450 K, respectively). The thermodynamic properties of the cation ordering are investigated using the Monte Carlo method. (c) 2005 Pleiades Publishing, Inc.

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Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Div, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Sofronova, S. N.; Софронова, Светлана Николаевна; Зиненко, Виктор Иванович
}
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Zinenko, V. I.
Statistical mechanics of cation ordering and lattice dynamics of PbZrxTi1-xO3 solid solutions / V. I. Zinenko, S. N. Sofronova // Phys. Solid State. - 2004. - Vol. 46, Is. 7. - P. 1291-1300, DOI 10.1134/1.1778455. - Cited References: 18 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PEROVSKITE
Аннотация: An effective Hamiltonian for Zr-Ti cation ordering in PbZrxTi1 - xO3 solid solutions is written out. To determine the parameters of the effective Hamiltonian, a nonempirical calculation is performed within an ionic-crystal model taking into account the deformation and dipole and quadrupole polarizabilities of ions. The thermodynamic properties of cation ordering are studied using the Monte Carlo method. The calculated phase transition temperatures (180 and 250 K for the concentrations x = 1/3 and 1/2, respectively) are much lower than the melting temperature of the compound under study. At such temperatures, the ordering kinetics is frozen and, in reality, the phase transition to the ordered phase does not occur, in agreement with experimental observations. Within the same ionic-crystal model, we calculated the high-frequency permittivity, Born dynamic charges, and the lattice vibration spectrum for a completely disordered phase and certain ordered phases. It is shown that soft vibration modes, including ferroelectric ones, exist in the lattice vibration spectrum of both the completely disordered and the ordered phases. (C) 2004 MAIK "Nauka / Interperiodica".

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Div, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Sofronova, S. N.; Софронова, Светлана Николаевна; Зиненко, Виктор Иванович
}
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10.

    Верещагин, Сергей Николаевич.
    Применение ТГ/ДСК-анализа c программированным составом газовой фазы для изучения фазового перехода порядок-беспорядок в нестехиометрическом Sr-Dy-кобальтате / С. Н. Верещагин, В. А. Дудников, Ю. С. Орлов // J. Sib. Fed. Univ. Chem. - 2018. - Vol. 11, Is. 4. - P. 507-517 ; Журн. СФУ. Химия, DOI 10.17516/1998-2836-0095. - Библиогр.: 17. - Исследование выполнено при финансовой поддержке Российского фонда фундаментальных исследований, Правительства Красноярского края, Красноярского краевого фонда науки в рамках научного проекта No 18-42-243004 и проекта фундаментальных исследований СО РАН V.45.3.3. . - ISSN 1998-2836. - ISSN 2313-6049
   Перевод заглавия: Application of TG/DSC analysis under variable gas phase composition to study order-disorder transition in nonstoichiometric Sr-Dy-cobaltate

РУБ Chemistry, Multidisciplinary
Рубрики:
PEROVSKITE
OXYGEN
Кл.слова (ненормированные):
перовскит -- порядок-беспорядок -- фазовый переход -- ТГ -- ДСК -- perovskite -- order-disorder -- phase transition -- TG -- DSC
Аннотация: Методом термического анализа (ТГ/ДСК) в условиях постоянного и программированного состава газовой фазы изучено влияние скорости закалки на полноту перехода кубического разупорядоченного нестехиометрического перовскита (I) Sr(0.8)Dy(0.2)CoO(3-d) в тетрагональную модификацию (II) с упорядоченным расположением катионов Sr/Dy и анионных вакансий, а также взаимосвязь степени превращения I в II с количеством мобильного кислорода и его энергетическими характеристиками. Показано, что фазовое превращение протекает как фазовый переход первого рода, процесс образования структуры II контролируется кинетическими факторами, а использование скоростей охлаждения 3-99 К/мин позволяет получить образцы, формально соответствующие 98-30 % превращению I в II; при этом как количество подвижного кислорода, так и энтальпия его удаления из образца нелинейно зависят от полноты перехода I в II.
For the first time a method of TG/DSC analysis under constant and variable gas phase composition was applied to reveal interconnection between quenching ramp rates and degree of phase transformation of cubic nonstoichiometric disordered perovskite (I) Sr(0.8)Dy(0.2)CoO(3-d) to tetragonal structure (II) with ordered Sr/Dy cations and anion vacancies. It was shown that the transformation is a first order phase transition and the ordering process is kinetically controlled. Based on the experimental transition enthalpy it was found that a formal conversion degree of I to II was 98-30% under cooling ramp rates 3-99 K/min. Non-linear relationship between the completeness of I-to-II transformation and mobile oxygen characteristics (content and the enthalpy of O-removal) was demonstrated.

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Держатели документа:
SB RAS, FRC Krasnoyarsk Sci Ctr, Inst Chem & Chem Technol, 50-24 Akademgorodok, Krasnoyarsk 660036, Russia.
SB RAS, FRC Krasnoyarsk Sci Ctr, Kirensky Inst Phys, 50-38 Akademgorodok, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Дудников, Вячеслав Анатольевич; Dudnikov, V. A.; Орлов, Юрий Сергеевич; Orlov, Yu. S.; Vereshchagin S. N.

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