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    Иванова, Оксана Станиславовна.
    Прозрачные магнитные стеклокерамики на основе боратных и германатных стекол с наночастицами ферритов / О. С. Иванова, И. С. Эдельман // Четвертый междисциплинарный научный форум с международным участием “Новые материалы и перспективные технологии” : сборник материалов. - 2018. - Т. 1. - С. 215-220. - Библиогр.: 5
   Перевод заглавия: Transparance magnetic glass ceramics based on borate and germanate glasses with ferrite nanoparticles

Материалы конференции
Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Эдельман, Ирина Самсоновна; Edelman, I. S.; Ivanova, O. S.; "Новые материалы и перспективные технологии", междисциплинарный научный форум с международным участием(4 ; 2018 ; нояб. ; 27-30 ; Москва); Российская академия наук; Совет молодых ученых Российской академии наукРоссийское химическое общество им. Д.И. Менделеева; Институт металлургии и материаловедения им. А. А. Байкова РАН
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    Иванова, Оксана Станиславовна.
    Магнитооптические боратные и германатные стекла / О. С. Иванова, Р. Д. Иванцов, И. С. Эдельман. - [Б. м. : б. и.]. - Библиогр.: 1 назв. - Б. ц.
Перевод заглавия: Magnetooptical borate and germanate glasses
   Перевод заглавия: Magnetooptical borate and germanate glasses

Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Иванцов, Руслан Дмитриевич; Ivantsov, R. D.; Эдельман, Ирина Самсоновна; Edelman, I. S.; Ivanova, O. S.}
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    Высокотемпературная теплоёмкость бората меди / Л. Т. Денисова [и др.] // Журн. СФУ. Сер. "Химия". - 2013. - Т. 6, №. 1. - С. 60-64 ; J. Sib. Fed. Univ. Chem.
   Перевод заглавия: High-Temperature Heat Capacity of Copper Borate
Кл.слова (ненормированные):
heat capacity -- thermodynamic properties -- copper-Borate
Аннотация: This paper reports experimental data obtained on the heat capacity of copper borate within the 380 – 1020 К temperature range. The thermodynamic functions have been calculated using this data.

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Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Денисова, Л. Т.; Денисов, Виктор Михайлович; Саблина, Клара Александровна; Sablina, K. A.; Чумилина, Любовь Геннадьевна; Патрин, Геннадий Семёнович; Patrin, G.S.; Иртюго, Лилия Александровна

}
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    Weak antiferromagnet iron borate FeBO3. classical object for magnetism and the state of the art / S. G. Ovchinnikov, V. V. Rudenko, N. V. Kazak [et al.] // J. Exp. Theor. Phys. - 2020. - Vol. 131, Is. 1. - P. 177-188, DOI 10.1134/S106377612007016X. - Cited References: 74. - This work was supported by the Russian Science Foundation, project no. 18-12-00022 . - ISSN 1063-7761. - ISSN 1090-6509
Рубрики:
ELECTRONIC-STRUCTURE
   TRANSITION
   RESONANCE
   FERROMAGNETISM
   DEPENDENCE
Аннотация: The simple lattice and magnetic structure, the high Neel temperature, the narrow antiferromagnetic resonance line of FeBO3, and the narrow electron paramagnetic resonance line of its isostructural diamagnetic analogs MBO3:Fe3+(M = Ga, In, Sc, Lu) make iron borate unique for investigations and applications. Iron borate is a model crystal for numerous experimental and theoretical studies, including spin crossovers and metallization at megabar pressures and many-electron effects in optics and X-ray spectroscopy. The recent works dealing with the investigation of the properties of FeBO(3)are reviewed.

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Публикация на русском языке Слабый ферромагнетик борат железа FeBO3. Классический объект для магнетизма и современное состояние исследований [Текст] / С. Г. Овчинников, В. В. Руденко, Н. В. Казак [и др.] // Журн. эксперим. и теор. физ. - 2020. - Т. 158 Вып. 1. - С. 184-197

Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Rudenko, V. V.; Руденко, Валерий Васильевич; Kazak, N. V.; Казак, Наталья Валерьевна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Gavrichkov, V. A.; Гавричков, Владимир Александрович; Russian Science FoundationRussian Science Foundation (RSF) [18-12-00022]
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Violation of axial symmetry of optical properties in the trigonal crystal Nd:GdFe2.1Ga0.9(BO3)(4) / A. V. Malakhovskii [et al.] // Phys. Lett. A. - 2009. - Vol. 373, Is. 18-19. - P. 1683-1686, DOI 10.1016/j.physleta.2009.03.019. - Cited References: 16. - The work was supported by the Russian Foundation for Basic Researches, grant No 07-02-00704. . - ISSN 0375-9601

РУБ Physics, Multidisciplinary
Рубрики:
IRON BORATE GDFE3(BO3)(4)
Кл.слова (ненормированные):
Optical anisotropy -- Spectroscopy -- Rare earth compounds -- Transition metal compounds -- Optical anisotropy -- Rare earth compounds -- Spectroscopy -- Transition metal compounds
Аннотация: Strong dependence of birefringence and absorption spectra of d-d, f-f and charge transfer transitions on the direction of light beam in the plane perpendicular to the threefold crystallographic axis has been found out in trigonal crystal Nd:GdFe2.1Ga0.9(BO3)(4). X-ray measurements have shown that the crystal consists of inversion twins, whose formation is stimulated by the partial substitution of Fe by Ga. Observed violation of axial symmetry of the trigonal crystal optical properties is accounted for on the basis of assumption about stripe domain structure of the inversion twins. (c) 2009 Elsevier B.V. All rights reserved.

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Держатели документа:
L.V. Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Akademgorodok, 660036 Krasnoyarsk, Russian Federation

Доп.точки доступа:
Malakhovskii, A. V.; Малаховский, Александр Валентинович; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Zabluda, V. N.; Заблуда, Владимир Николаевич; Leont'ev, A. A.; Temerov, V. L.; Темеров, Владислав Леонидович; Gudim, I. A.; Гудим, Ирина Анатольевна; Russian Foundation for Basic Researches [07-02-00704]
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Unusual Valence States of Manganese Ions in Gadolinium Gallium Aluminum Borate Single Crystals [Text] / A. S. Aleksandrovsky, L. N. Bezmaternykh [et al.] // Известия высших учебных заведений. Физика. - 2008. - Т. 51, № 10/2. - P115-119

Доп.точки доступа:
Aleksandrovsky, A.S.; Bezmaternykh, L.N.; Bovina, A.F.; Gudim, I.A.; Kharlamova, S.A.; Krylov, A.S.; Melnikova, S.V.; Temerov, V.Ye.
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Unusual magnetic transitions and nature of magnetic resonance spectra in oxide glasses containing gadolinium / J. . Kliava [et al.] // Phys. Rev. B. - 2005. - Vol. 71, Is. 10. - Ст. 104406, DOI 10.1103/PhysRevB.71.104406. - Cited References: 40 . - ISSN 1098-0121

РУБ Physics, Condensed Matter
Рубрики:
ELECTRON-PARAMAGNETIC-RESONANCE
   BORATE GLASSES
   IONS
   BEHAVIOR
   GD3+
   SPECTROSCOPY
   SYSTEMS
   GD-3+
   FIELD
   SHAPE
Кл.слова (ненормированные):
gadolinium -- glass -- lanthanide -- oxide -- anisotropy -- article -- chemical structure -- concentration response -- electron spin resonance -- energy -- magnetism -- molecular physics -- nanoparticle -- phase transition -- refraction index -- temperature sensitivity
Аннотация: Magnetic susceptibility, electron paramagnetic resonance (EPR), and optical properties have been studied in a glass system {20La(2)O(3)-22Al(2)O(3)-23B(2)O(3)-35(SiO2+GeO2)} with a part of La2O3 substituted by Gd2O3 in different concentrations. Positive Weiss constants have been found in the more heavily doped glasses and ascribed to clustering of Gd3+ ions. Two magnetic phase transitions at 55 and 12 K were detected and ascribed, respectively, to ferromagnetic and antiferromagnetic clusters containing Gd ions. The overall shape of the EPR spectra shows the presence of clustering at the higher Gd contents. At low temperatures the cluster-related resonance signal is altered in shape, indicating an onset of magnetic anisotropy field. This signal is convincingly fitted to superparamagnetic resonance arising from ferromagnetic nanoparticles. The clustering, depending on the Gd concentration, correlates with a significant shift to lower energies of the strong optical absorption band edge, ascribed to a charge transfer transition between Gd ions. A nonmonotonous change of refractive index with the increase of the Gd content indicates changes in the glass matrix and in Gd cluster structure.

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Держатели документа:
Univ Bordeaux 1, CNRS, UMR 5798, CPMOH, F-33405 Talence, France
Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel
RAS, SB, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
SI Vavilov State Opt Inst, St Petersburg 199034, Russia
Bar Ilan Univ, Dept Phys, IL-52900 Ramat Gan, Israel
ИФ СО РАН
CPMOH, UMR 5798, CNRS-Universite Bordeaux-I, 33405 Talence Cedex, France
Department of Chemistry, Bar-Ilan University, Ramat-Gan 52900, Israel
L. V. Kirensky Institute of Physics SB RAS, Krasnoyarsk 660036, Russian Federation
S. V. Vavilov State Optical Institute, St. Petersburg 199034, Russian Federation
Department of Physics, Bar-Ilan University, Ramat-Gan 52900, Israel

Доп.точки доступа:
Kliava, J.; Malakhovskii, A. V.; Малаховский, Александр Валентинович; Edelman, I. S.; Эдельман, Ирина Самсоновна; Potseluyko, A. M.; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Melnikova, S.V.; Мельникова, Светлана Владимировна; Zarubina, T. V.; Petrovskii, G.; Bruckental, Y.; Yeshurun, Y.
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    Ultra-narrow band blue emission of Eu2+ in halogenated (Alumino)borate systems based on high lattice symmetry / Y. Wei [et al.] // J. Am. Ceram. Soc. - 2019. - Vol. 102. - P. 2353– 2369, DOI 10.1111/jace.16127. - Cited References: 63. - This work was supported by the National Natural Science Foundation of China (Grant Nos. 51672259, 51672265, 21521092, 51750110511), Engineering Research Center of Nano-Geomaterials of Ministry of Education, China University of Geosciences (Wuhan) (No. NGM2016KF002), the Ministry of Science and Technology of Taiwan (Contract No. MOST 104-2113-M-027-007-MY3), the Key Research Program of Frontier Sciences, CAS (Grant No. YZDY-SSW-JSC018), and projects for science and technology development plan of Jilin province (20170414003GH), the Program for Jiangmen Innovative Reasearch Team (No.[2017]385),major program of basic research and applied research of Guangdong Province (2017KZDXM083) and the Russian Science Foundation (Grant No. 17-12-01047). . - ISSN 0002-7820
   Перевод заглавия: Ультра-узкое синее излучение Eu2 + в галогенированных (алюмо)боратных системах с высокой решеточной симметрией
Кл.слова (ненормированные):
blue emission -- high symmetry -- phosphors -- ultra-narrow band -- WLEDs
Аннотация: Phosphor materials with ultra‐high color purity are highly desired in backlit display and WLEDs. How to achieve high‐purity three‐primary emission in rare earth ions activated inorganic phosphors has become a hot topic. Herein, we reported ultra‐narrow band and highly efficient blue‐violet‐emitting Eu2+‐doped Ba2B5O9X (fwhm = 31 nm) and NaBa4(AlB4O9)2X3 (X = Cl, Br) (fwhm = 43 nm) phosphors with peak positions around 424‐437 nm. Especially, the color purity of Ba2B5O9Cl:Eu sample even exceeded 97%, its internal quantum efficiency could achieve 87%. The EXANES analysis revealed that the Eu mainly existed in the form of +2. According to the Rietveld structural refinement, extraordinarily narrow band emission should be attributed to the highly symmetric lattice structures with the flower‐like polyhedrons in the studied (alumino)borate matrix. Significantly, the color gamut of as‐prepared blue phosphor combined with the standard green and red phosphors was almost close to that of Rec. 2020 display standard. In addition, cation substitution strategy in NaBa4(AlxB5‐xO9)2Cl3 (x = 0‐4) and NaBa4(GayB5‐yO9)2Cl3 (y = 0‐3) samples successfully achieved spectra adjustment, and the underlying mechanism was proposed. All these results demonstrate that the as‐prepared phosphors could be superior blue‐emitting candidates for backlit display as well as WLEDs.

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Держатели документа:
Faculty of Materials Science and Chemistry, Engineering Research Center of Nano-Geomaterials of Ministry of Education, China University of Geosciences, Wuhan, China
State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
Institute of Organic and Polymeric Materials, National Taipei University of Technology, Taipei, Taiwan
National Synchrotron Radiation Research Center, Hsinchu, Taiwan
School of Applied Physics and Materials, Wuyi University, Jiangmen, Guangdong, China

Доп.точки доступа:
Wei, Y.; Qu, X.; Li, G.; Cheng, Z.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Lin, C. C.; Chan, T. -S.; Chang, C. -K.; Chuang, Y. -C.; Lin, J.
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Udod, L. V.
NMR-study of the crystalline and amorphous CuB2O4 / L. V. Udod, K. A. Sablina, Y. N. Ivanov // J. Supercond. Nov. Magn. - 2007. - Vol. 20, Is. 2. - P. 183-186, DOI 10.1007/s10948-006-0122-6. - Cited References: 9 . - ISSN 1557-1939

РУБ Physics, Applied + Physics, Condensed Matter
Рубрики:
COPPER METABORATE
BORATE GLASSES
Кл.слова (ненормированные):
Amorphous states -- Copper metaborate -- Amorphization -- Amorphous materials -- Crystalline materials -- Ground state -- Magnetic properties -- Molecular structure -- Nuclear magnetic resonance spectroscopy -- Copper compounds
Аннотация: B-11 nuclear magnetic resonance (NMR) spectroscopy was applied to study the crystalline, amorphous and crystallizing from an amorphous states of copper metaborate. The occurrence of trigonal BO3 units at the expense of converting tetragonal BO4 units was observed in amorphous CuB2O4. This fact explains the essential change of CuB2O4 magnetic properties under amorphization.

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Держатели документа:
RAS, SB, LV Kirensky Inst Phys, Krasnoyarsk 660036, Russia
ИФ СО РАН
L. V. Kirensky Institute of Physics, SB, RAS, Akademgorodok, 660036, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Sablina, K. A.; Саблина, Клара Александровна; Ivanov, Y. N.; Иванов, Юрий Николаевич; Удод, Любовь Викторовна
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10.

Transperant nanomagnetic materials based on borate glasses co-doped with iron, manganese and rare-earth elements / I. Edelman [et al.] // XI International Conference on Nanostructured Materials. - 2012. - P.

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zabluda, V. N.; Заблуда, Владимир Николаевич; Hennet, L.; Thiaudiere, D.; Saboungi, M.-L.; Zubavichus, Y. V.; Veligzhanin, A. A.; Zaikovskiy, V. I.; Stepanov, S.; Curély, J.; Kliava, J.; International Conference on Nanostructured Materials (11 ; 2012 ; August ; 26 – 31 ; Rhodes, Greece)
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11.

Terahertz spectroscopy of multiferroic EuFe3(BO3)4 / K. N. Boldyrev [et al.] // Phys. Lett. A. - 2012. - Vol. 376, Is. 37. - P. 2562-2564, DOI 10.1016/j.physleta.2012.06.028. - Cited References: 19. - This work was partially supported by the Russian Foundation for Basic Research under Grants No. 10-02-01071-a and No. 09-02-00171-a, by the Ministry of Education and Science under Grant HIII-4828.2012.2, and by the Russian Academy of Sciences under the programs for basic research. . - ISSN 0375-9601

РУБ Physics, Multidisciplinary
Рубрики:
SINGLE-CRYSTAL
GDFE3(BO3)4
Кл.слова (ненормированные):
Terahertz spectroscopy -- Multiferroics -- Europium iron borate
Аннотация: The terahertz spectra of a rare-earth iron borate with the huntite structure are obtained for the first time. We study the low-temperature (4.0–90 K) α-polarized transmittance spectra of the EuFe3(BO3)4 single crystal in the region 0.9–6.0 THz. Pronounced shifts of phonon frequencies and appearance of new phonon modes at the temperature T S = 58 K of the R 32 → P 3 1 21 structural phase transition are observed. Additional shifts of phonon frequencies occur at the temperature T N = 34 K of the magnetic ordering of the Fe subsystem, thus evidencing the spin–phonon coupling in this multiferroic material.

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Держатели документа:
[Boldyrev, K. N.
Klimin, S. A.
Popova, M. N.] RAS, Inst Spect, Troitsk 142190, Moscow Region, Russia
[Stanislavchuk, T. N.] New Jersey Inst Technol, Dept Phys, Newark, NJ 07102 USA
[Bezmaternykh, L. N.] RAS, Siberian Branch, Kirensky Inst Phys, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Boldyrev, K. N.; Stanislavchuk, T. N.; Klimin, S. A.; Popova, M. N.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич
}
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12.

    Synthesis, structure and properties of K2(1-x)Rb2xAl2B2O7 and Cs1.39Tl0.61Al2B2O7 borates as the basis for preparing new oxide materials / V. G. Grossman [et al.] // Lett. Mater. - 2019. - Vol. 9, Is. 1. - P. 86-90 ; Письма о материалах, DOI 10.22226/2410-3535-2019-1-86-90. - Cited References:22. - The research was carried out within the state assignment of FASO of Russia (Theme No 0339-2016-0007). . - ISSN 2218-5046. - ISSN 2410-3535
   Перевод заглавия: Синтез, структура и свойства боратов K2(1-x)Rb2xAl2B2O7 и Cs1.39Tl0.61Al2B2O7 как основа получения новых оксидных материалов

РУБ Materials Science, Multidisciplinary
Рубрики:
OPTICAL-PROPERTIES
   CRYSTAL-STRUCTURE
   K2Al2B2O7
   GROWTH
Кл.слова (ненормированные):
borate -- solid-phase synthesis -- optical properties -- борат -- твердофазный синтез -- оптические свойства
Аннотация: With the development of technology, the need for highly efficient functional materials is steadily increasing. Currently, borates attract the attention of researchers, as they are promising nonlinear materials. Potassium rubidium aluminum borate based on potassium aluminum borate (trigonal syngony, space group P321, Z = 3) was obtained by solid-phase synthesis. The individuality and purity of the borates were confirmed by X-ray diffraction. Analysis of differential scanning calorimetry and thermogravimetric method for K2(1‑x)Rb2xAl2B2O7 (x = 0.1– 0.8) was performed in the temperature range of 25–1075°С. Potassium rubidium borates decompose in the temperature range of 900 –1000°C. Differential scanning calorimetry, dielectric loss tangent, and second-harmonic generation data revealed phase transitions for K0.6Rb1.4Al2B2O7. A significant SHG effect was found at room temperature for K0.6Rb1.4Al2B2O7 (Q = 70). Then the SHG effect increases to Q = 85 at a temperature of 645°C and remains constant with a further increase in temperature. The new triple borate Cs1.39Tl0.61Al2B2O7 was synthesized by the solid-phase synthesis, and its crystallographic parameters were obtained by the Rietveld method. This borate crystallizes in the monoclinic space group P21 / c with the unit cell parameters: Z = 2, a = 6.6669(3) Å, b = 7.2991(3) Å , c = 9.3589(4) Å , β =116.6795(18)°, V = 406.94(3) Å 3. The structure can be considered to be built up from the nearly planar [Al2B2O10] rings, which are composed of two AlO4 tetrahedra and two BO3 triangles, connected, alternately to each other by corner-sharing.
С развитием технологии потребность в высокоэффективных функциональных материалах растет. В настоящее время бораты привлекают внимание исследователей, поскольку они являются перспективными нелинейными материалами. Твердофазным синтезом получены бораты K2(1-x)Rb2xAl2B2O7 (x = 0.1–0.8) на основе калий-алюминиевого бората (тригональная сингония, пространственная группа P321, Z = 3). Индивидуальность и чистота боратов подтверждена рентгеновской дифракцией. Анализ дифференциально-сканирующей калориметрией и термогравиметрическим методом для K2(1-x)Rb2xAl2B2O7 (x = 0.1–0.8) был проведен в интервале температур 25–1075 ºС. Калий-рубидиевые бораты разлагаются в интервале температур 900–1000 °C. Дифференциальной сканирующей калориметрией, диэлектрическими измерениями и методом генерации второй оптической гармоники выявлены фазовые переходы для K0.6Rb1.4Al2B2O7. Значительный ГВГ-эффект был обнаружен при комнатной температуре для K0.6Rb1.4Al2B2O7 (Q = 70). Эффект генерации второй гармоники возрастает до Q = 85 при температуре 645 °C и остается постоянным при дальнейшем увеличении температуры. Новый тройной борат Cs1.39Tl0.61Al2B2O7 был синтезирован методом твердофазного синтеза, а его кристаллографические параметры были получены с помощью метода Ритвельда. Этот борат кристаллизуется в моноклинной пространственной группе P21/c с параметрами элементарной ячейки: Z = 2, a = 6.6669 (3) Å, b = 7.2991 (3) Å, c = 9.3589 (4) Å, β = 116.6795 (18)º, V = 406.94 (3) Å3. Структуру можно представить в виде почти плоских колец [Al2B2O10], которые состоят из двух тетраэдров AlO4 и двух BO3 треугольников, соединенных попеременно друг с другом посредством вершин.

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RAS, Baikal Inst Nat Management, Siberian Branch, 6 Sakhyanova St, Ulan Ude 670047, Russia.
Lomonosov Moscow State Univ, GSP 1,1-3 Leninskie Gory, Moscow 119991, Russia.
RAS, Siberian Branch, Kirensky Inst Phys, Fed Res Ctr KSC, 50-38 Akademgorodok, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, 82 Svobodniy Av, Krasnoyarsk 660041, Russia.

Доп.точки доступа:
Grossman, V. G.; Гроссман В. Г.; Bazarov, B. G.; Базаров Б. Г.; Stefanovich, S. Y.; Стефанович С. Ю.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, J. G.; Базарова Ж. Г.; [0339-2016-0007]

}
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13.

Synthesis, structure and magnetic properties of monoclinic lanthanum-chromium borate LaCr3(BO3)4 / E. A. Volkova, M. S. Platunov, A. M. Antipin [et al.] // J. Alloys Compd. - 2024. - Vol. 994. - Ст. 174683, DOI 10.1016/j.jallcom.2024.174683. - Cited References: 38. - Single crystal X-ray analysis was carried out within the State assignment NRC "Kurchatov institute" (research contribution of A.M.A.). The research contribution of M.S.P. was partially supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental assignment for Synchrotron radiation facility "SKIF", Boreskov Institute of Catalysis (project FWUR-2024–0040) . - ISSN 0925-8388. - ISSN 1873-4669
Кл.слова (ненормированные):
Borates -- Flux growth -- Crystal structure -- Differential scanning calorimetry -- Powder X-ray diffraction -- IR spectroscopy -- Antiferromagnet
Аннотация: Single crystals of LaCr3(BO3)4 were synthesized through spontaneous nucleation from a K2Mo3O10 flux melt. The crystal structure was determined using single-crystal X-ray diffraction (XRD) at temperatures of 293 K and 85 K. LaCr-borate crystallizes in the monoclinic C2/c space group with unit cell parameters a = 7.47980(5) Å, b = 9.55180(7) Å, c = 11.48330(8) Å, β= 104.0060(6)°, V = 796.04(1) Å3 (for C1, T = 293 K), and a = 7.47380(5) Å, b = 9.55520(7) Å, c = 11.47100(8) Å, β = 103.9330(6)°, V = 795.08(1) Å3 (for C2, T = 85 K), each with Z = 4. The temperature dependence of the unit cell parameters, including the monoclinic angle (β) and the unit cell volume (V), was investigated over the range of 85–293 K. No structural phase transitions were observed in the low-temperature region down to 85 K. Differential scanning calorimetry (DSC) measurements revealed no high-temperature phase transitions between 50 and 1350°C. Infrared (IR) spectroscopy confirmed the monoclinic structure of LaCr3(BO3)4 crystals, revealing characteristic absorption bands, including the lowest frequency mode associated with the translational vibrations of the La3+ ion.

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Держатели документа:
Faculty of Geology, Lomonosov Moscow State University, Moscow, Russian Federation
Synchrotron radiation facility SKIF, Boreskov Institute of Catalysis SB RAS, Kol’tsovo, Russian Federation
Shubnikov Institute of Crystallography, Complex "Crystallography and Photonics", NRC "Kurchatov institute", Moscow, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Institute of Engineering Physics and Radio Electronics, Siberian Federal University, Krasnoyarsk, Russian Federation
Melnikov Research Institute of Comprehensive Exploitation of Mineral Resources of the Russian Academy of Sciences, Moscow, Russian Federation

Доп.точки доступа:
Volkova, E. A.; Platunov, M. S.; Платунов, Михаил Сергеевич; Antipin, A. M.; Alpanova, R. R.; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Pyastolova, Yu. V.; Пястолова, Юлия Валентиновна; Podobraznyh, A. D.; Kosorukov, V. L.; Koporulina, E. V.; Maltsev, V. V.
}
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14.

    Structural limits of K2Al2B2O7-family borate crystals / V. V. Atuchin [et al.] // XVI Международная конференция "Опто-, наноэлектроника, нанотехнологии и микросистемы" : Труды. - Ульяновск, 2013. - P. 102-103
   Перевод заглавия: Структурные пределы кристаллов боратов семейства K2Al2B2O7

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Доп.точки доступа:
Atuchin, V. V.; Bazarov, B. G.; Grossman, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, Zh.G.; Институт нанотехнологий микроэлектроники РАН; Ульяновский государственный университет; Российский фонд фундаментальных исследований; Академия наук Татарстана; "Opto-, nanoelectronics, nanotechnology, and microsystems", International Conference (2013 ; Jul. ; 26-30 ; Ulyanovsk, Russia); "Опто-, наноэлектроника, нанотехнологии и микросистемы", международная конференция (2013 ; июль.; 26-30 ; Ульяновск)
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15.

    Structural field of K2Al2B2O7-family [borate] crystals / V. V. Atuchin [et al.]. ; Nonlinear Optics and Applications (VII ; April 15, 2013 ; Prague) // Proc. SPIE. - 2013. - Vol. 8772. - Ст. 877210. - P. DOI 10.1117/12.2017099
   Перевод заглавия: Структурная область боратных кристаллов семейства K2Al2B2O7
Аннотация: The known crystal structures of borate compounds with general composition AI2MIII 2B2O7 (AI: Na, K, Cs, Rb) have been considered. The structures in space groups P63/m, P-31c, P321 and P21/c have been found depending on cation combination. Criterion k = (r(MIII)+r(B)+2r(O))/r(AI) has been formulated and it controls the formation of trigonal K2Al2B2O7 (KABO) type structure. The existence of noncentrosymmetric KABO-type borates is possible over the range of k = 2.7 – 2.06. This range is promising for searching new borate crystals and solid solutions with pronounced nonlinear optical properties. © (2013) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.

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Atuchin, V. V.; Bazarov, B. G.; Базаров Б.Г.; Grossman, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, Zh.G.; Базарова Ж.Г.; Nonlinear Optics and Applications (7 ; 2013 ; Apr. ; 15 ; Prague)
}
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16.

Structural field of K2Al2B2O7 family borate crystals / B. I. Kidyarov [et al.] ; , Иркутский гос. ун-т // Международная молодежная конференция по люминесценции и лазерной физике : тезисы лекций и докладов. - 2012. - P. 10-11

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Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Kidyarov, B. I.; Atuchin, V. V.; Атучин, Виктор Валерьевич; Grossman, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarov, B. G.; Базаров Б.Г.; Bazarova, Zh.G.; Базарова Ж.Г.; Научный совет по оптике и лазерной физике Российской академии наук; Научный совет по люминесценции Российской академии наук; Иркутский филиал Института лазерной физики Сибирского отделения РАН; Институт геохимии Сибирского отделения РАН; Иркутский государственный университет; Иркутский научный центр Сибирского отделения РАН; Международная молодежная конференция по люминесценции и лазерной физике(2012 ; июль ; 16-22 ; "Песчанка", турбаза, оз. Байкал, Иркутская обл.)
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17.

    Structural and spectroscopic properties of new noncentrosymmetric self-activated borate Rb3EuB6O12 with B5O10 units / V. V. Atuchin [et al.] // Mater. Des. - 2018. - Vol. 140. - P. 488-494, DOI 10.1016/j.matdes.2017.12.004. - Cited References: 53. - We are grateful to Guochun Zhang for the crystal structure materials on K3YB6O12 and O. Tsydenova, A. Sarapulova for the consultations. The work was supported by Projects № 0356-2015-0412 of SB RAS Program № II.2P and № 0339-2016-0007. The reported study was funded by RFBR according to research projects 16-52-48010, 17-02-00920, 17-03-00886 and 17-52-53031 and RSF project 14-22-00143. The work was supported by Act 211 Government of the Russian Federation, contract № 02.A03.21.0011, and by the Ministry of Education and Science of the Russian Federation (5.5523.2017/8.9). This research was supported by Grant no. 8.2.01.2017 of Tomsk State University Academic D.I. Mendeleev Fund Program. . - ISSN 0264-1275
   Перевод заглавия: Структурные и спектроскопические характеристики самоактивированного бората Rb3EuB6O12 со структурными единицами B5O10
Кл.слова (ненормированные):
Rubidium rare earth borate -- Solid state reaction -- Rietveld refinement -- Raman -- Infrared spectroscopy -- Luminescence
Аннотация: New noncentrosymmetric double borate Rb3EuB6O12 was designed and synthesized by the solid state reaction method, and its crystallographic parameters were obtained by Rietveld analysis. This borate crystallizes in the trigonal space group R32 with cell parameters a = 13.4604(2) Å, c = 30.7981(5) Å, Z = 15. Its structure features a three-dimensional framework composed of the [B5O10]5 − groups that are bridged by Eu-O polyhedra. The existence of B5O10 group in the structure was confirmed by vibrational spectroscopy. Rb3EuB6O12 melts incongruently at 1101 K. The second harmonic generation effect of Rb3EuB6O12 is 16 times higher than that of the α-quartz standard. In the luminescence spectrum, the domination of a single prominent narrow line from the hypersensitive 5D0 - 7F2 manifold of Eu3 + ions is observed, while the 5D0 - 7F1 manifold and ultranarrow 5D0 - 7F0 line are of comparable peak intensity. These features are explained by a specific local symmetry of the Eu3+ ion within the crystal structure of Rb3EuB6O12.

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Держатели документа:
Laboratory of Optical Materials and Structures, Institute of Semiconductor Physics, SB RAS, Novosibirsk, Russian Federation
Functional Electronics Laboratory, Tomsk State University, Tomsk, Russian Federation
Laboratory of Single Crystal Growth, South Ural State University, Chelyabinsk, Russian Federation
Baikal Institute of Nature Management, SB RAS, Ulan-Ude, Russian Federation
Buryat State University, Ulan-Ude, Russian Federation
Laboratory of Coherent Optics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Institute of Nanotechnology, Spectroscopy and Quantum Chemistry, Siberian Federal University, Krasnoyarsk, Russian Federation
Laboratory of Nanodiagnostics and Nanolithography, Institute of Semiconductor Physics, SB RAS, Novosibirsk, Russian Federation
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
Department of Photonics and Laser Technologies, Siberian Federal University, Krasnoyarsk, Russian Federation
Department of Chemistry, Lomonosov Moscow State University, Moscow, Russian Federation

Доп.точки доступа:
Atuchin, V. V.; Subanakov, A. K.; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Bazarov, B. G.; Bazarova, J. G.; Gavrilova, T. A.; Krylov, A. S.; Крылов, Александр Сергеевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Stefanovich, S. Y.
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18.

Structural and electronic transitions in gadolinium iron borate GdFe3(BO3)(4) at high pressures / A. G. Gavriliuk [et al.] // JETP Letters. - 2004. - Vol. 80, Is. 6. - P. 426-432, DOI 10.1134/1.1830662. - Cited References: 20 . - ISSN 0021-3640

РУБ Physics, Multidisciplinary
Рубрики:
TRIGONAL GDFE3(BO3)(4)
   RM(3)(BO3)(4) CRYSTALS
   OPTICAL-SPECTRA
   BAND-STRUCTURE
   FEBO3
   GROWTH
Аннотация: The optical properties and structure of gadolinium iron borate GdFe3(BO3)(4) crystals are studied at high pressures produced in diamond-anvil cells. X-ray diffraction data obtained at a pressure of 25.6 GPa reveal a first-order phase transition retaining the trigonal symmetry and increasing the unit cell volume by 8%. The equation of state is obtained and the compressibility of the crystal is estimated before and after the phase transition. The optical spectra reveal two electronic transitions at pressures similar to26 GPa and similar to43 GPa. Upon the first transition, the optical gap decreases jumpwise from 3.1 to similar to2.25 eV. Upon the second transition at P = 43 GPa, the optical gap deceases down to similar to0.7 eV, demonstrating a dielectric-semiconductor transition. By using the theoretical model developed for a FeBO3 crystal and taking into account some structural analogs of these materials, the anomalies of the high-pressure optical spectra are explained. (C) 2004 MAIK "Nauka/Interperiodica".

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Держатели документа:
Russian Acad Sci, Inst High Pressure Phys, Troitsk 142092, Moscow Region, Russia
Russian Acad Sci, Inst Crystallog, Moscow 119333, Russia
Russian Acad Sci, Siberian Div, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Max Planck Inst Chem, D-55020 Mainz, Germany
ИФ СО РАН

Доп.точки доступа:
Gavriliuk, A. G.; Kharlamova, S. A.; Lyubutin, I. S.; Troyan, I. A.; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Potseluiko, A. M.; Eremets, M. I.; Boehler, R.
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19.

Spectroscopic study of the magnetic ordering in SmFe3(BO3)(4) / E. P. Chukalina [et al.] // Phys. Lett. A. - 2010. - Vol. 374, Is. 15-16. - P. 1790-1792, DOI 10.1016/j.physleta.2010.02.018. - Cited References: 20. - The authors thank B.Z. Malkin and S.A. Klinnin for helpful discussions and K.N. Boldyrev for participating in some low-temperatures measurements. This work was supported in part by the Russian Foundation for Basic Research (grants Nos. 10-02-01071 and 10-02-00765), and by the Russian Academy of Sciences under the Programs for Basic Research. . - ISSN 0375-9601

РУБ Physics, Multidisciplinary
Рубрики:
IRON BORATE GDFE3(BO3)(4)
SINGLE-CRYSTAL
DYFE3(BO3)(4)
Кл.слова (ненормированные):
Rare-earth iron borates -- Magnetic ordering -- Optical spectroscopy -- Magnetic ordering -- Optical spectroscopy -- Rare-earth iron borates
Аннотация: SmFe3(BO3)(4) belongs to the family of rare-earth RFe3(BO3)(4) multiferroics. We present the first measurements of the optical spectra of SmFe3(BO3)(4) (on single crystals) and report the data on the crystal-field levels and their symmetries for the ground multiplet H-6(5/2) [0 (Gamma(4)). 135 (Gamma(56)), and 220 (Gamma(4)) cm(-1)] and on the ground-state exchange splitting (13.2 cm(-1) at 1.7 K), important to interpret the magnetic, magnetoelectric, and thermodynamic properties of this compound. The observed exchange splitting of the Sm3+ Kramers doublets manifests the magnetic ordering in SmFe3(BO3)(4) at 32 +/- 1 K. From a comparison of the temperature-dependent spectra of the Sm3+ ion in SmFe3(BO3)(4) and in Nd-Gd mixed iron borate where the magnetic spin reorientation has been found earlier, we suggest the easy-plane arrangement of the Fe spins in SmFe3(BO3)(4). The samarium iron borate preserves the R32 (D-3(7)) crystal structure at all the investigated temperatures (down to 1.7 K). (C) 2010 Elsevier B.V. All rights reserved.

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Держатели документа:
[Chukalina, E. P.
Popova, M. N.] RAS, Inst Spect, Troitsk 142190, Moscow Region, Russia
[Bezmaternykh, L. N.
Gudim, I. A.] RAS, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
ИФ СО РАН
Institute of Spectroscopy, RAS, 5, Fizicheskaya str, 142190 Troitsk, Moscow region, Russian Federation
L.V. Kirensky Institute of Physics, Siberian Branch, RAS, 660036 Krasnoyarsk, Russian Federation

Доп.точки доступа:
Chukalina, E. P.; Popova, M. N.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич; Gudim, I. A.; Гудим, Ирина Анатольевна
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20.

Specific heat and ESR in borate TbAl3(BO3)4 / M. I. Paschenko [et al.] // 20th Int. Сonf. on Magnetism (ICM-2015) : book of abstracts. - 2015. - Ст. TH.C-P35. - P. 1731
Аннотация: The rare earth aluminum borates RAl3(BO3)4 have only one magnetic subsystem - a subsystem of rare earth ions. That is why same of these crystals can be a simple model systems for the study of spontaneous and magnetic field induced phase transitions. In this work, the specific heat and ESR were studied in order to determine parameters of interactions between the magnetic ions in the TbAl3(BO3)4 crystal. Investigation of temperature dependence of the specific heat allowed us to determine the magnetic ordering temperature of the rare-earth subsystem of TbAl3(BO3)4, Tc = 0.68 K. The initial splitting, Δ ≈ 1.3 K, and the effective g-factor, g = 16, of the lowest quasidoublet of Tb3+ ion were determined from the ESR experiments. In the case of antiferromagnetic ordering, in frame of the molecular field theory, the difference between the constants of effective fields of intrasublattice interaction, λ11, and intersublattice interaction λ12 can be calculated by using the expression: (λ11- λ12) = Δ/2 (geff μB) 2tanh (Δ/2Tc). In the case of ferromagnetic ordering, λ12 = 0 and λ11 is equal to the molecular field constant λ0. By fitting this expression to the experimental data we obtained (λ11- λ12) or λ0 equal to 0.03 T2 /K. Low temperature magnetic ordering and small value of the effective interaction between the magnetic moments of the terbium ions allows us to make the assumption about the dipole-dipole nature of the magnetic ordering in this material.

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Доп.точки доступа:
Paschenko, M. I.; Bedarev, V. A.; Kobets, M. I.; Dergachev, K. G.; Khatsko, E. N.; Gnatchenko, S. L.; Zvyagin, A. A.; Zajarniuk, T.; Szewczyk, A.; Gutowska, M.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич; Temerov, V. L.; Темеров, Владислав Леонидович; International Conference on Magnetism(20 ; 2015 ; Jul ; 5-10 ; Barselona, Spain)
}
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