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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volova T. G., Golubev A. I., Nemtsev I. V., Lukyanenko A. V., Dudaev A. E., Shishatskaya E. I.
Заглавие : Correction: Volova et al. Laser processing of polymer films fabricated from PHAs differing in their monomer composition. Polymers 2021, 13, 1553
Колич.характеристики :2 с
Место публикации : Polymers. - 2024. - Vol. 16, Is. 8. - Ст.1075. - ISSN 20734360 (eISSN), DOI 10.3390/polym16081075
Примечания : Cited References: 1
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Каравайский, Андрей Юрьевич, Фомин, Сергей Викторович, Лукин, Юрий Иванович
Заглавие : Модель комплексной диэлектрической проницаемости органо-минеральных почв, учитывающая минеральный состав и содержание органического вещества
Колич.характеристики :21 с
Место публикации : Журн. радиоэлектрон. - 2024. - № 1. - Ст.6. - ISSN 16841719 (eISSN), DOI 10.30898/1684-1719.2024.1.9; J. Radio Electron.
Примечания : Библиогр.: 29
Аннотация: На основе рефракционной диэлектрической модели создана одночастотная диэлектрическая модель талых и мерзлых лесных почв корневой зоны, учитывающая влияние как минеральной, так и органической компоненты почвенной смеси. Модель разработана для частоты 435 МГц на основе диэлектрических измерений пяти почв, в которых содержание органического вещества варьировалось от 11,1 до 54,4 % и глины от 21,1 до 40,9 %. Диэлектрические измерения были проведены в диапазоне массовой влажности от сухого состояния до наименьшей влагоемкости и диапазоне температур от – 30 до 25 ℃. В исследуемом диапазоне температур коэффициент детерминации между рассчитанными с использованием предложенной модели и измеренными значениями действительной (ε') и мнимой (ε") частями комплексной диэлектрической проницаемости составляет 0,988 – 0,997 для ε' и 0,957 – 0,971 для ε". Нормированное среднеквадратическое отклонение при этом составило 6 – 5,6 % для ε' и 20,2 – 21,2 % для ε". Разработанная диэлектрическая модель может быть применена в алгоритмах дистанционного зондирования при восстановлении значения влажности лесных почв корневой зоны из данных радарного и радиометрического зондирования.The single-frequency dielectric model of thawed and frozen forest soils in the root zone based on the refractive dielectric model was created, taking into account the influence of both the mineral and organic components of the soil mixture. The dielectric model was created on at 435 MHz the basis of the laboratory dielectric measurements of five soils with organic matter content in the range from 11.1 to 54.4 % and clay content from 21.1 to 40.9 %. Dielectric measurements were carried out in the range of the gravimetric moisture from the dry state to the lowest moisture capacity and in the temperature range from –30 to 25 ℃. The coefficient of determination between the predicted and measured values for real and imaginary parts of the complex permittivity are 0.988 - 0.997 and 0.957 - 0.971, respectively. The normalized standard deviations in this case are 6 - 5.6 % and 20.2 - 21.2 % for real and imaginary parts of the complex permittivity, respectively. The developed dielectric model can be used in remote sensing algorithms of soil moisture retrieval of forest soils in the root zone from the data radar and radiometric.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tikhomirov A. A., Molokeev M. S., Velichko V. V.
Заглавие : Photo-biological effectiveness of PAR for radish plant communities irradiated using an LED source with an adjustable spectrum
Колич.характеристики :8 с
Место публикации : Light Eng. - 2024. - Vol. 32, Is. 2. - P.70–77. - ISSN 02362945 (ISSN), DOI 10.33383/2023-063. - ISSN 25419935 (eISSN)
Примечания : Cited References: 15. - The study was carried out with financial support within the framework of State Assignment 121101300066-7 of the Ministry of Education and Science and the Strategic Academic Leadership Program "Priority-2030" for the Siberian Federal University
Аннотация: The aim of the current study was to find the most effective spectral modes of irradiation of short-season plants (for example, radish) using a fluorescent LED irradiator with a variable spectrum. The research methodology was based on the species-specific response of plants to the spectral composition of light. Photo-biological experiments were carried out to find effective spectral composition of PAR for cultivating radish communities under stable and variable irradiation modes of electrical lighting. It was shown that under stable irradiation modes, the highest productivity of economically useful radish biomass had been achieved at spectral composition with a maximum of 60 % radiation in the (600–700) nm region in a variable spectral irradiation mode. The variable spectral irradiation mode turned out to be the most effective when the spectral composition with the dominance of red rays was changed to the spectral composition with the dominance of blue rays. There were no significant differences between the best production parameters for stable and variable modes of irradiation of radish plants, which indicates the expediency of choosing the stable spectral mode of irradiation of radish plants as a short-season crop under electrical illumination. The results obtained can be used to select spectral irradiation modes for short-season plants grown under electrical lighting in northern regions and in isolated rooms in various climatic zones using "City-farm" technologies.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Komogortsev S. V., Iskhakov R. S., Vazhenina I. G., Nemtsev I. V., Li O. A.
Заглавие : Ferromagnetic resonance and magnetic anisotropy of 3d-metal wires with composition gradients
Колич.характеристики :5 с
Место публикации : Bull. Russ. Acad. Sci.: Phys. - 2024. - Vol. 88, Is. 4. - P.531-535. - ISSN 10628738 (ISSN), DOI 10.1134/S1062873823706244. - ISSN 19349432 (eISSN)
Примечания : Cited References: 13
Аннотация: Results are presented from investigating the ferromagnetic resonance spectra of arrays of Co‒Ni and Co‒Fe‒Ni wires with different composition gradients, deposited into polycarbonate track-etched membranes. The effect interfaces and concentration gradients have on the effective fields of the investigated wires is examined. An anomalous angular dependence of the fields of ferromagnetic resonance is observed for the wire arrays at a pore density of ~18% in the membrane.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Endzhievskaya I. G., Endzhievskiy A. S., Galkin M. A., Molokeev M. S.
Заглавие : Machine learning methods in assessing the effect of mixture composition on the physical and mechanical characteristics of road concrete
Колич.характеристики :18 с
Место публикации : J. Build. Eng. - 2023. - Vol. 76. - Ст.107248. - ISSN 23527102 (eISSN), DOI 10.1016/j.jobe.2023.107248
Примечания : Cited References: 17. - The work was carried out within the framework of the Strategic Academic Leadership Program "Priority-2030" for the Siberian Federal University. The research in field of Machine Learning application was supported by the Tyumen Oblast Government, as part of the West-Siberian Interregional Science and Education Center’s project No. 89-DON (3)
Аннотация: Current manuscript presents a study on the use of 48 experimental data points containing parameters of concrete production technological process and its properties, such as strength, density, and bending strength. It was revealed that temporal characteristics, specifically - compressive strength at the age of 3, 7, 28 days, R3, R7, and R28, are significantly correlated with each other, indicating that only one characteristic, such as R28 or Rfl 28, is sufficient for prediction. The absence of multiple correlations between parameters and properties suggests that linear regression analysis may not be accurate. Therefore, the use of Machine Learning is optimal; specifically Random Forest method is preferable due to ease of use and minimum hyperparameters for tuning. Low prediction errors (?1–11%) for 30% of the test data, as determined by the cross-validation method, confirm a relationship between the experimental parameters and the concrete properties. The most important parameters for achieving high values of compressive and bending strengths, R28 and Rfl 28, were identified, namely: air-entraining additives, granite crushed stone consisting of a mixture of fractions 5–20 mm, crushed stone derived from gravel of high strength grains of large fractions 10–20 mm. To obtain explanatory model, another Machine Learning method, that was used, called Decision Tree. The model showed that a high amount of crushed stone 10–20 mm from gravel, more than 212 (kg per 1 m3 of concrete mix), leads to a higher number of strong grains with smooth, rounded surface, thereby, reducing the bending strength of concrete. However, a large concentration of crushed stone mix fractions of 5–20 mm from granite, more than 537 (kg per 1 m3 of concrete mix), leads to the maximum roughness, which makes a significant contribution to the increased strength of concrete due to the adhesion of the matrix and aggregates to each other.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zhila, Natalia O., Sapozhnikova, Kristina Yu., Berezovskaya, Arina V., Kiselev, Evgeniy G., Shishatskaya, Ekaterina I., Vasiliev A. D., Thomas, Sabu, Volova, Tatiana G.
Заглавие : Biosynthesis and properties of sulfur-containing polyhydroxyalkanoates (PHAs) produced by wild-type strain Cupriavidus necator B-10646
Место публикации : Polymers. - 2023. - Vol. 15, Is. 4. - Ст.1005. - ISSN 20734360 (eISSN), DOI 10.3390/polym15041005
Примечания : Cited References: 53. - The study was funded by State Assignment of the Ministry of Science and Higher Education of the Russian Federation (project No. 0287-2021-0025)
Аннотация: The study addresses the growth of the wild-type strain Cupriavidus necator B-10646 and the synthesis of sulfur-containing polyhydroxyalkanoates (PHA) by this strain on media containing fructose and three different precursors (3-mercaptopropionic acid, 3′,3′-dithiodipropionic acid and 3′,3′-thiodipropionic acid). By varying the concentration and number of doses of the precursors added into the bacterial culture, it was possible to find conditions that ensure the formation of 3-mercaptopropionate (3MP) monomers from the precursors and their incorporation into the C-chain of poly(3-hydroxybutyrate). A series of P(3HB-co-3MP) copolymer samples with different content of 3MP monomers (from 2.04 to 39.0 mol.%) were synthesized and the physicochemical properties were studied. The effect of 3MP monomers is manifested in a certain decrease in the molecular weight of the samples and an increase in polydispersity. Temperature changes are manifested in the appearance of two peaks in the melting region with different intervals regardless of the 3MP content. The studied P(3HB-co-3MP) samples, regardless of the content of 3MP monomers, are characterized by equalization of the ratio of the amorphous and crystalline phases and have a close degree of crystallinity with a minimum of 42%, = and a maximum of 54%.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sukhanova E.V., Sagatov N., Oreshonkov A. S., Gavryushkin P.N., Popov Z.I.
Заглавие : Novel Janus 2D structures of XMoY (X, Y = O, S, Se, Te) composition for solar hydrogen production
Место публикации : Int. J. Hydrog. Energy. - 2023. - Vol. 48, Is. 38. - P.14226-14237. - ISSN 03603199 (ISSN), DOI 10.1016/j.ijhydene.2022.12.286. - ISSN 18793487 (eISSN)
Примечания : Cited References: 97. - The authors acknowledge financial support from Russian Science Foundation (№ 21-73-20183). The authors are grateful to the Joint Supercomputer Center of the Russian Academy of Sciences and to the Information Technology Centre of Novosibirsk State University for providing access to the cluster computational resources
Аннотация: The successful fabrication of H-phase Janus transition metal dichalcogenides (TMDs) has received considerable interest due to its great potential in photocatalytic applications. Here, new A′-XMoY (X/Y = O, S, Se, Te) Janus-type structures belonging to the family of TMDs were theoretically investigated for the first time in terms of photocatalytic water splitting via DFT calculations. For all compounds, the Raman spectra were calculated. The SMoO, SeMoO, SMoSe, SMoTe and SeMoTe compounds are dynamically stable and are semiconductors. Among all considered structures SMoTe is the most promising candidate for solar hydrogen production because valence and conduction bands perfectly engulf the redox potentials of water at both neutral and acidic media, opposite to SMoSe, SMoO, SeMoO suitable only in the acidic media, and SeMoTe – in the neutral media. Moreover, A′-SMoTe demonstrates the outstanding values of the solar-to-hydrogen (STH) conversion efficiencies of 54.0 and 67.1 for neutral and acidic media.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Frolov K. V., Smirnova E. S., Sidorova E. V., Alekseeva O. A., Sorokin T. A., Artemov V. V., Chmelenin D. N., Gudim I. A.
Заглавие : Structure and properties of multiferroic ferroborates of mixed composition SmFe3-xAlx(BO3)4 and Eu1-yLayFe3(BO3)4
Коллективы : Samarkand International Symposium on Magnetism, Samarkand State University
Место публикации : Book of abstacts of Samarkand International Symposium on Magnetism (SISM-2023)/ int. adv. com. S. G. Ovchinnikov [et al.]. - 2023. - Ст.3PO-L8-3. - P.195. - ISBN 978-5-00202-320-2
Примечания : Cited References: 6. - РНФ 23-22-00286
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Titova V. R., Gudim I. A.
Заглавие : Influence of melt-solution composition on the properties of NdSc3(BO3)4 single crystals
Коллективы : "Термодинамика и материаловедение", симпозиум с международным участием, Российское химическое общество им. Д.И. Менделеева, Научный совет РАН по физической химии, Институт неорганической химии им. А.В. Николаева Сибирского отделения РАН, Институт химии твердого тела УрО РАН, Институт химии силикатов им. И. В. Гребенщикова РАН
Место публикации : XV Cимпозиум с международным участием "Термодинамика и материаловедение": тез. докладов. - Новосибирск, 2023. - P.238. - ISBN 978-5-901688-27-4, DOI 10.26902/THERM_2023_228
Примечания : Библиогр.: 1. - РНФ № 22-12-20019 ; Красноярский региональный фонд науки
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10.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Komogortsev S. V., Vazhenina I. G., Iskhakov R. S., Nemtsev I. V.
Заглавие : Ferromagnetic resonance and magnetic anisotropy of 3-d metal rods with gradients of composition
Коллективы : International Baltic Conference on Magnetism, Балтийский федеральный университет им. И. Канта
Место публикации : V International Baltic Conference on Magnetism. IBCM: Book of abstracts. - 2023. - P.135
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Komogortsev S. V., Satsuk S. A., Nemtsev I. V., Iskhakov R. S., Semenov S. V.
Заглавие : Magnetic properties of three-dimensional metal rods with composition gradients produced by electroless deposition
Место публикации : IEEE Magn. Lett. - 2022. - Vol. 13. - Ст.6103405. - ISSN 1949307X (ISSN), DOI 10.1109/LMAG.2022.3163015
Примечания : Cited References: 30. - This work was supported in part by the Russian Foundation for Basic Research (RFBR), Krasnoyarsk Territory and in part by the Krasnoyarsk Regional Fund of Science under Grant 20-43-240003. The authors thank the Center of Collective Use of the Federal Research Center Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences for the equipment. Sergey V. Komogortsev thank the RFBR, Krasnoyarsk Region and the Krasnoyarsk Regional Science Foundation (Project 20-42-240001) for the support in the contribution of numerical simulation. The authors also thank V. S. Plotnikov and V. V. Tkachev for electron microscopy images
Аннотация: A comparative study of the magnetic properties of arrays of Co–Ni rods with different composition gradients (smooth or step-like) along the rod axes was carried out. Ordered arrays of Co–Ni nanorods with diameters up to 400 nm and 8 µm length were prepared by electroless plating into a porous nuclear-track-etched polycarbonate membrane. The gradient in Co and Ni composition was confirmed by energy-dispersive X-ray analysis. The variation of Co–Ni contents along the long axis of the rods correlates with the gradient of the magnetization within the rod. Magnetization reversal was studied by analyzing the angular dependence of coercivity and using micromagnetic simulations. For both types of gradient rods, reversal occurs by curling. The local magnetic anisotropy field of rods with a step-type gradient is significantly higher than that for rods with a smooth gradient.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chekanova L. A., Shepeta N. A., Denisova E. A., Iskhakov R. S., Kuzovnikova L. A., Nemtsev I. V.
Заглавие : Comparison of the microstructure and magnetic properties of films and composite powders based on 3-D metal
Место публикации : J. Supercond. Novel Magn. - 2022. - Vol. 35, Is. 11. - P.3241-3247. - ISSN 15571939 (ISSN), DOI 10.1007/s10948-022-06339-w
Примечания : Cited References: 19. - This work was funded by the Russian Foundation for Basic Research, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20–43-240003
Аннотация: The comparison between the magnetic properties of materials with different curvature and spatial distribution of nanograins, such as particles (3D spatial distribution) and multilayer films (2D) was carried out. Functionally graded Co(P)/Ni(P) and Co(P)/CoNi(P) specimens have been fabricated by electroless deposition. The magnetic and structural properties are characterized by electron microscopy, X-ray diffraction, ferromagnetic resonance spectroscopy, and vibrating sample magnetometer. It was demonstrated that the interaction between the Ni(P) core and Co(P) shell of particles could form the functionally graded materials with tailored structure and coercive force. Furthermore, it was found that the magnetic parameters (the local anisotropy field, ferromagnetic resonance linewidth, and coercivity) are mainly determined by the artificially created interface boundaries for all grains’ spatial distribution. The magnetic anisotropy field and coercivity of Co(P)/Ni(P) flat films were characterized by lower values than those for spherical shell of particles with the same composition, produced by the same method.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gordienko, A., I, Malikov A. G., Volochaev M. N., Panyukhina A. D.
Заглавие : Influence of chemical composition and thermomechanical treatment of low-carbon steels on the microstructure and mechanical properties of their laser welded joints
Коллективы : [FWRW-2021-0009]; [121030900259-0]
Место публикации : Mater. Sci. Eng. A. - 2022. - Vol. 839. - Ст.142845. - ISSN 0921-5093, DOI 10.1016/j.msea.2022.142845. - ISSN 1873-4936(eISSN)
Примечания : Cited References: 38. - Microstructural studies and mechanical tests of laser welds were performed according to the Government research assignment for ISPMS SB RAS, project FWRW-2021-0009. Part of the research related to the selection of optimal laser welding parameters for low carbon steels was carried out within Basic State Project No. 121030900259-0
Предметные рубрики: AUSTENITE GRAIN-SIZE
HEAT-AFFECTED ZONE
MARTENSITE START TEMPERATURE
Аннотация: The paper reports microstructures (revealed by transmission electron microscopy) in various zones of laser welds of the X70 and X80 low-carbon steels with different initial microstructures, as well as chemical and phase compositions. In the X70 steels with 0.13% C, the microstructure refinement has been achieved through helical rolling at temperatures of 920 °C and 850 °C (designated as X70-920 and X70-850, respectively). For all studied cases, both initial steel microstructures and phase compositions have determined the formation of different microstructures with various microhardness levels in the weld metal and heat-affected zones. For the X70-850 steel with a more dispersed and homogeneous microstructure (dF = 3.3 μm), a lower microhardness level of 340 HV has been observed in the weld metal, compared with the X70-920 one (dF = 5.5 μm, 370 HV). The reason has been the formation of both bainite and martensite laths in the X70-850 weld metal, while only lath and lamellar martensite has formed in the X70-920 one. For the X80 steel (0.55% C), lowering the carbon content and additional microalloying with chromium, molybdenum and nickel have enabled to decrease the microhardness level down to 295 HV in the weld metal due to the degenerate upper bainite formation and the carbon level reduction in martensite. The dispersed and homogeneous initial microstructures of the X70-850 and X80 steels has provided the formation of granular ferrite-bainite microstructures in the intercritical heat-affected zone. They have possessed a lower proportion of residual austenite regions and small sizes of twinned martensite areas. The welded X80 steel specimen has been characterized by higher ductile properties compared to both X70 ones.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Moshkina E. M., Krylov A. S., Kokh D., Shabanova K., Molokeev M. S., Bovina A. F., Plyaskin M., Rostovtsev N., Bezmaternykh L. N.
Заглавие : Multicomponent flux growth and composition control of Cu2MnBO5:Ga ludwigites
Место публикации : CrystEngComm. - 2022. - Vol. 24, Is. 19. - P.3565-3575. - ISSN 14668033 (ISSN), DOI 10.1039/d2ce00258b
Примечания : Cited References: 26. - This study was supported by the Russian Science Foundation (Grant No. 21-72-00130). The Raman, X-ray, and EDX data were obtained using the analytical equipment of the Krasnoyarsk Regional Center of Research Equipment of the Federal Research Center “Krasnoyarsk Science Center SB RAS”
Аннотация: To reach the concentration phase boundary between antiferromagnetic Cu2GaBO5 and ferrimagnetic Cu2MnBO5 ludwigites, solid solutions Cu2Mn1−xGaxBO5 (x = 0.05, 0.1, 0.15, 0.175) were grown by the flux technique using a multi-component solvent based on Bi2Mo3O12 with the addition of Na2B4O7 which significantly influenced the crystal formation and cation composition of the studied compounds. The content of the flux system was corrected taking into account the earlier established relationship of the partition coefficients of Mn2O3 and Ga2O3. The influence of the solvent components on the ludwigite crystallization was analyzed. The maximum size of the grown crystal was 1 × 1 × 4 mm3. The structure and cation composition of the grown compounds were studied using X-ray (X-ray diffraction, EDX (energy-dispersive X-ray spectroscopy)) and vibrational (Raman) spectroscopy techniques. The phase boundary of Cu2MnBO5–Cu2GaBO5 was found to be in the concentration range of x = 0.15–0.175, corresponding to a change in the monoclinic axis direction and a leap in the lattice parameters. The symmetry evolution of metal–oxygen octahedra for four nonequivalent cation positions was analyzed, and the unique crystal structure of Cu2MnBO5 demonstrated high rigidity relative to the introduction of Ga3+ cations. The polarized Raman spectra of monoclinic ludwigites were obtained and studied for the first time. A comparison of the spectra of the studied samples in both phases and orthorhombic ludwigites was made. A number of spectral features due to the monoclinic distortions in the crystal were found. In agreement with the Raman experiment, the concentration phase boundary was close to 0.15.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Lin C. -R., Chen Y. -Z., Ivanova O. S., Altunin R. R., Knyazev Yu. V., Molokeev M. S., Zharkov S. M., Shestakov N. P., Sukhachev A. L., Edelman I. S.
Заглавие : Effect of surfactants on the structure, phase composition, and magnetic properties of FexSy nanoparticles synthesized by thermal decomposition
Место публикации : Nanobiotechnol. Rep. - 2022. - Vol. 17, Is. 3. - P.336-344. - ISSN 26351676 (ISSN), DOI 10.1134/S2635167622030089
Примечания : Cited References: 27. - This study was supported by the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project no. 19-42-240005: “Features of the Electronic Structure, Magnetic Properties, and Optical Excitations in Nanocrystals of Multifunctional Magnetic Chalcogenides Fe3S4 and FeSe” and the Russian Foundation for Basic Research and the Ministry of Science and Technology of Taiwan, joint projects nos. 19-52-52002 and 109-2112-M-153-003 and 108-2923-M-153-001-MY3The electron-microscopy study was carried out at the Laboratory of Electron Microscopy of the Center for Collective Use of the Siberian Federal University within the state assignment of the Ministry of Science and Higher Education of the Russian Federation (research code FSRZ-2020-0011). The magnetic measurements were carried out on a vibrating sample magnetometer at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
Аннотация: The effect of surfactants on the structure, morphology, and magnetic properties of FexSy iron-sulfide nanoparticles synthesized by thermal decomposition is studied. Oleylamine, hexadecylamine, and octadecylamine are used as surfactants. It is established by X-ray and electron-diffraction analysis combined with Mossbauer spectroscopy that, in samples 1 and 2 prepared using oleylamine and hexadecylamine, respectively, the Fe3S4 greigite phase dominates, with an inverse spinel structure isostructural to the iron oxide Fe3O4 magnetite with minor Fe9S11 impurities. Deviations in the distribution of iron cations over the tetrahedral and octahedral sites relative to the bulk greigite crystals are observed. The nanoparticles synthesized using octadecylamine (sample 3) are found to be multiphase with a greigite fraction of ~20%. In all three cases, as showed the results of transmission electron microscopy and Fourier transform infrared spectroscopy together with thermogravimetry analysis, the magnetic nanoparticles have an organic shell chemically bonded to their magnetic core, which prevents the agglomeration of the particles. This shell is much more massive in samples 2 and 3. The magnetization values for samples 1 and 2 are similar to those of greigite nanoparticles reported in publications, while the magnetization of sample 3 is several times lower, in accordance with the greigite fraction in it. The combination of fairly high magnetization with a massive organic shell allows one to consider hexadecylamine to be a promising surfactant for the synthesis of iron-sulfide nanoparticles protected from external impact and agglomeration.
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16.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Sofronova S. N., Moshkina E. M., Eremin E. V., Molokeev M. S.
Заглавие : Magnetic properties of quasi-two-dimensional oxyborates (Ni,Cu,Mn)3BO5 with different composition of Cu ions
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 1, Sect.: Low dimensional magnetism. - Ст.C.O5. - P.335-336. - ISBN 978-5-94469-051-7
Примечания : Cited References: 1. - The research was funded by RFBR, Krasnoyarsk Territory Krasnoyarsk Regional Fund of Science, project number 20-42-240011
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Komogortsev S. V., Semenov S. V., Varnakov S. N., Balaev D. A.
Заглавие : Features of the phase composition and structure of hypoeutectoid steel, manifested in the behavior of magnetization near magnetic saturation
Место публикации : Phys. Solid State. - 2022. - Vol. 64, Is. 1. - P.23-30. - ISSN 10637834 (ISSN), DOI 10.21883/PSS.2022.01.52484.192. - ISSN 10906460 (eISSN)
Примечания : Cited References: 46. - The research has been conducted with financial support by the Russian Foundation for Basic Research, Government of the Krasnoyarsk Territory, Krasnoyarsk Regional Science Foundation within the framework of the scientific project No. 20-48-242905 p_Yenisei Siberia ”Determining the impact of ferromagnetic magnetization on MHD parameters of electrolyser operation“
Аннотация: Investigation of the temperature evolution of magnetization curves near magnetic saturation makes it possible to extract new information on the features of the phase composition and structure of hypoeutectoid steel. It is shown that the main contribution to the magnitude and the temperature behavior of the energy density of the local magnetic anisotropy of hypoeutectoid steel is due to the lamellar structure of pearlite. The peculiarity of the temperature behavior of the energy of the magnetic anisotropy, along with the behavior of the paraprocess, indicates the formation of Mn-substituted cementite in the studied steel sample. The observation of the crossover of power-law regularities in the approximation of magnetization to saturation indicates the formation of two-dimensional nano-inhomogeneities of the local axis of easy magnetization in the plates of alpha iron, which are part of the pearlite.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zhila N. O., Sapozhnikova K. Y., Kiselev E. G., Nemtsev I. V., Lukyanenko A. V., Shishatskaya E. I., Volova T. G.
Заглавие : Biosynthesis and properties of a P(3HB-co-3HV-co-4HV) produced by Cupriavidus necator B-10646
Место публикации : Polymers. - 2022. - Vol. 14, Is. 19. - Ст.4226. - ISSN 20734360 (ISSN), DOI 10.3390/polym14194226
Примечания : Cited References: 77. - The study was funded by State Assignment of the Ministry of Science and Higher Education of the Russian Federation (project No. 0287-2021-0025)
Аннотация: Synthesis of P(3HB-co-3HV-co-4HV) copolymers by the wild-type strain Cupriavidus necator B-10646 on fructose or sodium butyrate as the main C-substrate with the addition of γ-valerolactone as a precursor of 3HV and 4HV monomers was studied. Bacterial cells were cultivated in the modes that enabled production of a series of copolymers with molar fractions of 3HV (from 7.3 to 23.4 mol.%) and 4HV (from 1.9 to 4.7 mol.%) with bacterial biomass concentration (8.2 ± 0.2 g/L) and PHA content (80 ± 2%). Using HPLC, DTA, DSC, X-Ray, SEM, and AFM, the physicochemical properties of copolymers and films prepared from them have been investigated as dependent on proportions of monomers. Copolymers are characterized by a reduced degree of crystallinity (Cx 38–49%) molecular weight characteristics Mn (45–87 kDa), and Mw (201–248 kDa) compared with P(3HB). The properties of the films surface of various composition including the porosity and surface roughness were studied. Most of the samples showed a decrease in the average pore area and an increase in their number with a total increase in 3HV and 4HV monomers. The results allow scaling up the productive synthesis of P(3HB-co-3HV-co-4HV) copolymers using Cupriavidus necator B-10646.
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19.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Komogortsev S. V., Li O. A., Iskhakov R. S., Nemtsev I. V., Semenov S. V.
Заглавие : Magnetic properties of composition graded Co-Ni rods
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 1, Sect.: Spintronics and magnetic nanostructures. - Ст.A.P4. - P.103. - ISBN 978-5-94469-051-7
Примечания : Cited References: 2. - The research was funded by RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20-43-240003
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volova T. G., Golubev A. I., Nemtsev I. V., Lukyanenko A. V., Dudaev A. E., Shishatskaya E. I.
Заглавие : Laser processing of polymer films fabricated from phas differing in their monomer composition
Место публикации : Polymers. - 2021. - Vol. 13, Is. 10. - Ст.1553. - ISSN 20734360 (ISSN), DOI 10.3390/polym13101553
Примечания : Cited References: 87. - This work was supported by the Russian Foundation for Basic Research/Regional State Autonomous Institution “Krasnoyarsk Regional Fund for the Support of Scientific and Scientific-Technical Activities” foundations under Grant number 19-43-240012 (laser treatment and films properties) and by the State Assignment of the Ministry of Science and Higher Education of the Russian Federation No. FSRZ-2020-0006 (polymer synthesis)
Аннотация: The study reports results of using a CO2-laser in continuous wave (3 W; 2 m/s) and quasi-pulsed (13.5 W; 1 m/s) modes to treat films prepared by solvent casting technique from four types of polyhydroxyalkanoates (PHAs), namely poly-3-hydroxybutyrate and three copolymers of 3-hydroxybutyrate: with 4-hydroxybutyrate, 3-hydroxyvalerate, and 3-hydroxyhexanoate (each second monomer constituting about 30 mol.%). The PHAs differed in their thermal and molecular weight properties and degree of crystallinity. Pristine films differed in porosity, hydrophilicity, and roughness parameters. The two modes of laser treatment altered these parameters and biocompatibility in diverse ways. Films of P(3HB) had water contact angle and surface energy of 92° and 30.8 mN/m, respectively, and average roughness of 144 nm. The water contact angle of copolymer films decreased to 80–56° and surface energy and roughness increased to 41–57 mN/m and 172–290 nm, respectively. Treatment in either mode resulted in different modifications of the films, depending on their composition and irradiation mode. Laser-treated P(3HB) films exhibited a decrease in water contact angle, which was more considerable after the treatment in the quasi-pulsed mode. Roughness parameters were changed by the treatment in both modes. Continuous wave line-by-line irradiation caused formation of sintered grooves on the film surface, which exhibited some change in water contact angle (76–80°) and reduced roughness parameters (to 40–45 mN/m) for most films. Treatment in the quasi-pulsed raster mode resulted in the formation of pits with no pronounced sintered regions on the film surface, a more considerably decreased water contact angle (to 67–76°), and increased roughness of most specimens. Colorimetric assay for assessing cell metabolic activity (MTT) in NIH 3T3 mouse fibroblast culture showed that the number of fibroblasts on the films treated in the continuous wave mode was somewhat lower; treatment in quasi-pulsed radiation mode caused an increase in the number of viable cells by a factor of 1.26 to 1.76, depending on PHA composition. This is an important result, offering an opportunity of targeted surface modification of PHA products aimed at preventing or facilitating cell attachment.
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