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Magnetostructural Investigation of Ball-Milled Cobalt-Copper Alloy [Текст] / R. S. Iskhakov, L. A. Kuzovnikova, S. V. Komogortsev [и др.] // Phys. Met. Metallogr. - Vol. 102, Suppl. 1, Chapter 11. - р. S64-S66DOI 10.1134/S0031918X0614016X. - Библиогр.: 6. - Russian Foundation for Basic Research (project no. 04-02-16230)
Аннотация: In this work we investigate a metastable inhomogeneous Co–Cu alloy produced by mechanical alloying. We use both conventional structural method (X-ray diffraction) and magnetic measurements of M(T) and M(H) dependences to obtain additional information about the process of mechanical alloying.

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Держатели документа:
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036 Russia
Institute of Chemistry and Chemical Technology, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036 Russia

Доп.точки доступа:
Iskhakov, R. S.; Исхаков, Рауф Садыкович; Kuzovnikova, L. A.; Кузовникова, Людмила Александровна; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Denisova, E. A.; Денисова, Елена Александровна; Balaev, A. D.; Балаев, Александр Дмитриевич; Mal'tsev, V. K.; Мальцев, Вадим Константинович; Bondarenko, G. N.; Бондаренко, Галина Николаевна
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Realizing persistent zero area compressibility over a wide pressure range in Cu2GeO4 by microscopic orthogonal-braiding strategy / X. Zhang, Yo. Liu, M. S. Molokeev [et al.] // Angew. Chem. - 2024. - Vol. 136, Is. 7. - Ст. e202318401, DOI 10.1002/ange.202318401. - Cited References: 24. - The authors would like to acknowledge Zhuohong Yin for useful discussions and experimental time for the 4W2 beamline in the Beijing synchrotron radiation facility (BSRF). This work was supported by the National Scientific Foundations of China (Grants T2222017, 12274425, 22133004, 11974360 and 51890864) and the CAS Project for Young Scientists in Basic Research (YSBR-024). M.S. Molokeev would like to acknowledge support fromthe Ministry of Science and High Education of the Russian Federation (Project No. FSRZ-2023-0006) . - ISSN 0044-8249. - ISSN 1521-3757
Кл.слова (ненормированные):
Zero area compressibility -- Orthogonal-Braiding -- High pressure -- Copper-based oxides -- First-principles calculation
Аннотация: Zero area compressibility (ZAC) is an extremely rare mechanical response that exhibits an invariant two-dimensional size under hydrostatic pressure. All known ZAC materials are constructed from units in two dimensions as a whole. Here, we propose another strategy to obtain the ZAC by microscopically orthogonal-braiding one-dimensional zero compressibility strips. Accordingly, ZAC is identified in a copper-based compound with a planar [CuO4] unit, Cu2GeO4, that possesses an area compressibility as low as 1.58(26) TPa-1 over a wide pressure range from ≈0 GPa to 21.22 GPa. Based on our structural analysis, the subtle counterbalance between the shrinkage of [CuO4] and the expansion effect from the increase in the [CuO4]-[CuO4] dihedral angle attributes to the ZAC response. High-pressure Raman spectroscopy, in combination with first-principles calculations, shows that the electron transfer from in-plane bonding dx2-y2 to out-of-plane nonbonding dz2 orbitals within copper atoms causes the counterintuitive extension of the [CuO4]-[CuO4] dihedral angle under pressure. Our study provides an understanding on the pressure-induced structural evolution of copper-based oxides at an electronic level and facilitates a new avenue for the exploration of high-dimensional anomalous mechanical materials.

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Держатели документа:
Functional Crystals Lab, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, China
Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk 660036, Russia
University of the Chinese Academy of Sciences, Beijing 100049, China
Department of Physics, Far Eastern State Transport University, Khabarovsk 680021, Russia
International Research Center of Spectroscopy and Quantum Chemistry, Siberian Federal University, Krasnoyarsk 660041, Russia

Доп.точки доступа:
Zhang, Xingyu; Liu, Youquan; Molokeev, M. S.; Молокеев, Максим Сергеевич; Xu, Bohui; Jiang, Xingxing; Lin, Zheshuai
}
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    Realizing persistent zero area compressibility over a wide pressure range in Cu2GeO4 by microscopic orthogonal-braiding strategy / X. Zhang, Yo. Liu, M. S. Molokeev [et al.] // Angew. Chem. Int. Ed. - 2024. - Vol. 63, Is. 7. - Ст. e202318401, DOI 10.1002/anie.202318401. - Cited References: 24. - The authors would like to acknowledge Zhuohong Yin for useful discussions and experimental time for the 4W2 beamline in the Beijing synchrotron radiation facility (BSRF). This work was supported by the National Scientific Foundations of China (Grants T2222017, 12274425, 22133004, 11974360 and 51890864) and the CAS Project for Young Scientists in Basic Research (YSBR-024). M.S. Molokeev would like to acknowledge support fromthe Ministry of Science and High Education of the Russian Federation (Project No. FSRZ-2023-0006) . - ISSN 1433-7851. - ISSN 1521-3773
   Перевод заглавия: Реализация постоянной нулевой сжимаемости в широком диапазоне давлений в Cu2GeO4 с помощью микроскопической стратегии ортогонального плетения
Кл.слова (ненормированные):
Zero area compressibility -- Orthogonal-Braiding -- High pressure -- Copper-based oxides -- First-principles calculation
Аннотация: Zero area compressibility (ZAC) is an extremely rare mechanical response that exhibits an invariant two-dimensional size under hydrostatic pressure. All known ZAC materials are constructed from units in two dimensions as a whole. Here, we propose another strategy to obtain the ZAC by microscopically orthogonal-braiding one-dimensional zero compressibility strips. Accordingly, ZAC is identified in a copper-based compound with a planar [CuO4] unit, Cu2GeO4, that possesses an area compressibility as low as 1.58(26) TPa-1 over a wide pressure range from ~0 GPa to 21.22 GPa. Based on our structural analysis, the subtle counterbalance between the shrinkage of [CuO4] and the expansion effect from the increase in the [CuO4]-[CuO4] dihedral angle attributes to the ZAC response. High-pressure Raman spectroscopy, in combination with first-principles calculations, shows that the electron transfer from in-plane bonding dx2-y2 to out-of-plane nonbonding dz2 orbitals within copper atoms causes the counterintuitive extension of the [CuO4]-[CuO4] dihedral angle under pressure. Our study provides an understanding on the pressure-induced structural evolution of copper-based oxides at an electronic level and facilitates a new avenue for the exploration of high-dimensional anomalous mechanical materials.

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Держатели документа:
Functional Crystals Lab, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, China
Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk 660036, Russia
University of the Chinese Academy of Sciences, Beijing 100049, China
Department of Physics, Far Eastern State Transport University, Khabarovsk 680021, Russia
International Research Center of Spectroscopy and Quantum Chemistry, Siberian Federal University, Krasnoyarsk 660041, Russia

Доп.точки доступа:
Zhang, Xingyu; Liu, Youquan; Molokeev, M. S.; Молокеев, Максим Сергеевич; Xu, Bohui; Jiang, Xingxing; Lin, Zheshuai
}
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The effect of aluminum-oxide powders on the structure and properties of copper electrodeposited composite coatings / I. R. Volkova, L. E. Tyryshkina, M. N. Volochaev [et al.] // Prot. Met. Phys. Chem. Surf. - 2023. - Vol. 59, Is. 1. - P. 71-75, DOI 10.1134/S2070205122700022. - Cited References: 9 . - ISSN 2070-2051. - ISSN 2070-206X
Кл.слова (ненормированные):
copper electrodeposited composite coatings -- aluminum-oxide nanopowder -- alumina -- microstructure -- microhardness -- ultimate tensile strength
Аннотация: Copper electrodeposited composite coatings containing two types of aluminum-oxide powders with different dispersities (alumina Al2O3-1 and electroexplosive aluminum-oxide nanopowder Al2O3-2) are obtained during the work. The studies show that introducing the powders leads to a change in the microstructure of the composites and a change in the grain growth principles during the formation of the coatings. Refinement and ordering of the grain structure of the coatings occurs and twinning defects and texture are formed. The change in the formation of the microstructure of the composites leads to a change in some operational characteristics: an increase in the microhardness (by 10% in the composites with the addition of alumina and by more than 30% in the coatings with electroexplosive aluminum oxide) and ultimate tensile strength (by 20% in the composites with Al2O3-1 and almost 1.5-fold in the samples with Al2O3-2).

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Публикация на русском языке Влияние порошков оксида алюминия на структуру и свойства медных композиционных гальванических покрытий [Текст] / И. Р. Волкова, Л. Е. Тырышкина, М. Н. Волочаев [и др.] // Физикохим. поверхн. и защита материалов. - 2023. - Т. 59 № 1. - С. 39-44

Держатели документа:
Federal Research Center “Krasnoyarsk Science Center”, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia
Reshetnev Siberian State University of Science and Technology, 660037, Krasnoyarsk, Russia

Доп.точки доступа:
Volkova, I. R.; Tyryshkina, L. E.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Zaloga, A. N.; Shabanova, K. A.; Ovchinnikov, A. V.; Lyamkin, A. I.
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Effect of Cu on performance of self-dispersing Ni-catalyst in production of carbon nanofibers from ethylene / S. D. Afonnikova, Yu. I. Bauman, V. O. Stoyanovskii [et al.] // C – J. Carbon Res. - 2023. - Vol. 9, Is. 3 : Advanced Carbon Nanomaterials and Hybrids. - Ст. 77, DOI 10.3390/c9030077. - Cited References: 72. - This work was supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis (project AAAA-A21-121011390054-1). The physicochemical characterization of samples was supported by the Russian Science Foundation (project No. 22-13-00406, https://rscf.ru/en/project/22-13-00406/BIC SB RAS (accessed on 30 March 2023)). - Analysis of the physicochemical properties of the samples was performed using the equipment of the ‘National Center for Catalyst Research’ (Novosibirsk, BIC SB RAS) and Krasnoyarsk regional Center of the Collective Use (KSS SB RAS). The authors are grateful to A.N. Serkova for the performed SEM studies, B.A. Kolesov for the Raman spectra data, to A.B. Ayupov for analyzing samples by low-temperature adsorption/desorption of nitrogen, to Y.V. Shubin for the XRD analysis and to E.I. Belyaeva for the particle distribution analysis . - ISSN 2311-5629
Кл.слова (ненормированные):
nickel-copper alloys -- carbon erosion -- catalytic pyrolysis -- carbon nanofibers -- segmented structure
Аннотация: The development of effective catalysts for the pyrolysis of light hydrocarbons with the production of carbon nanomaterials represents a relevant direction. In the present work, the influence of copper addition on performance of a self-dispersed Ni-catalyst and structural features of the obtained carbon nanofibers (CNFs) was studied. The precursors of Ni and Ni-Cu catalysts were prepared by activation of metal powders in a planetary mill. During contact with the C2H4/H2 reaction mixture, a rapid disintegration of the catalysts with the formation of active particles catalyzing the growth of CNFs has occurred. The kinetics of CNF accumulation during ethylene decomposition on Ni- and Ni-Cu catalysts was studied. The effect of temperature on catalytic performance was explored and it was shown that introduction of copper promotes 1.5–2-fold increase in CNFs yield in the range of 525–600 °C; the maximum CNFs yield (100 g/gcat and above, for 30-min reaction) is reached on Ni-Cu-catalyst at 575–600 °C. A comparative analysis of the morphology and structure of CNF was carried out using electron microscopy methods. The growth mechanism of carbon filaments in the shape of “railway crossties” on large nickel crystals (d > 250 nm) was proposed. It was found that the addition of copper leads to a decrease in the bulk density of the carbon product from 40–60 to 25–30 g/L (at T = 550–600 °C). According to the low-temperature nitrogen adsorption data, specific surface area (SSA) of CNF samples (at T ˂ 600 °C) lies in the range of 110–140 m2/g, regardless of the catalyst composition; at T = 600 °C the introduction of copper contributed to an increase in the specific surface of CNF by 100 m2/g.

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Держатели документа:
Boreskov Institute of Catalysis SB RAS, 5 Lavrentyev Ave., Novosibirsk 630090, Russia
Kirensky Institute of Physics, Akademgorodok, 50/38, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Afonnikova, S. D.; Bauman, Yury I.; Stoyanovskii, Vladimir O.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Mishakov, Ilya V.; Vedyagin, Aleksey A.
}
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Synthesis and optical properties of nickel-doped copper metaborate crystals / A. D. Molchanova, E. M. Moshkina, M. S. Molokeev [et al.] // Opt. Spectrosc. - 2023. - Vol. 131, Is. 8. - P. 717-722, DOI 10.1134/S0030400X23060127. - Cited References: 18. - The study was performed with the support of Russian Science Foundation, RSF grant no. 19-12-00413 . - ISSN 0030-400X. - ISSN 1562-6911
Кл.слова (ненормированные):
3d-ions -- crystal growth -- optical spectroscopy -- magnetic ordering -- cuprates
Аннотация: This work presents information on the growth and spectroscopic study of single crystals of copper metaborate doped with nickel Cu1–xNixB2O4 (x = 0.05, 0.1). In the absorption spectra of both crystals, satellites related to Cu centers distorted by impurity Ni atoms were observed near the lines of zero phonon transitions. Polarization studies in the isotropic ab-plane of the tetragonal crystal Cu1–xNixB2O4 show the presence of linear magnetic dichroism in the magnetically ordered state, which was previously observed both in manganese-doped and undoped copper metaborates CuB2O4. The temperature of magnetic phase transitions into the collinear antiferromagnetic and into helicoidal structures, TN = 19.1 K and T * = 8.6 K, respectively, were determined from the temperature dependence of the dichroic signal.

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Публикация на русском языке Синтез и оптические свойства кристаллов метабората меди, легированного никелем [Текст] / А. Д. Молчанова, Е. М. Мошкина, М. С. Молокеев [и др.] // Оптика и спектроскопия. - 2022. - Т. 130 Вып. 1. - С. 111-115

Держатели документа:
Institute of Spectroscopy, Russian Academy of Sciences, 108840, Moscow, Troitsk, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia
Scientific and Innovation Department, Kemerovo State University, 650000, Kemerovo, Russia

Доп.точки доступа:
Molchanova, A. D.; Moshkina, E. M.; Мошкина, Евгения Михайловна; Molokeev, M. S.; Молокеев, Максим Сергеевич; Tropina, E. V.; Bovina, A. F.; Бовина, Ася Федоровна; Boldyrev, K. N.
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Copper ferrite nanoparticles synthesized using anion-exchange Resin: Influence of synthesis parameters on the cubic phase stability / S. Saikova, A. Pavlikov, D. Karpov [et al.] // Materials. - 2023. - Vol. 16, Is. 6. - Ст. 2318, DOI 10.3390/ma16062318. - Cited References: 67. - The Russian team acknowledges the support of the Russian Science Foundation (Project 22-73-10047) . - ISSN 1996-1944
Кл.слова (ненормированные):
copper ferrite -- magnetic properties -- anion-exchange resin precipitation -- magnetic nanoparticles
Аннотация: Copper ferrite is of great interest to researchers as a material with unique magnetic, optical, catalytic, and structural properties. In particular, the magnetic properties of this material are structurally sensitive and can be tuned by changing the distribution of Cu and Fe cations in octahedral and tetrahedral positions by controlling the synthesis parameters. In this study, we propose a new, simple, and convenient method for the synthesis of copper ferrite nanoparticles using a strongly basic anion-exchange resin in the OH form. The effect and possible mechanism of polysaccharide addition on the elemental composition, yield, and particle size of CuFe2O4 are investigated and discussed. It is shown that anion-exchange resin precipitation leads to a mixture of unstable cubic (c-CuFe2O4) phases at standard temperature and stable tetragonal (t-CuFe2O4) phases. The effect of reaction conditions on the stability of c-CuFe2O4 is studied by temperature-dependent XRD measurements and discussed in terms of cation distribution, cooperative Jahn–Teller distortion, and Cu2+ and oxygen vacancies in the copper ferrite lattice. The observed differences in the values of the saturation magnetization and coercivity of the prepared samples are explained in terms of variations in the particle size and structural properties of copper ferrite.

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Держатели документа:
School of Non-Ferrous Metals and Material Science, Siberian Federal University, 660041 Krasnoyarsk, Russia
Institute of Chemistry and Chemical Technology, Federal Research Center “Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences”, Akademgorodok, 660036 Krasnoyarsk, Russia
Kirensky Institute of Physics, Federal Research Center “Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences”, Akademgorodok, 660036 Krasnoyarsk, Russia
Department of Physics and Astronomy, Uppsala University, P.O. Box 516, SE-751 20 Uppsala, Sweden

Доп.точки доступа:
Saikova, Svetlana; Pavlikov, Aleksandr; Karpov, Denis; Samoilo, Aleksandr; Kirik, Sergey; Volochaev, M. N.; Волочаев, Михаил Николаевич; Trofimova, Tatyana; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Kuklin, Artem
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    Анализ распределения меди в кристаллах LiNBO3:Cu с поверхностным легированием / Р. И. Анисимов, А. А. Колмаков, А. С. Темерева [и др.] // XI Международная конференция по фотонике и информационной оптике : сборник научных трудов. - Москва, 2022. - С. 451-452. - Библиогр.: . - ISBN 978-5-7262-2842-6
   Перевод заглавия: Analysis of copper distribution in LiNBO3:Cu crystals with surface doping
Рубрики:

Аннотация: Представлены результаты исследований распределения примеси по глубине в структурах, сформированных термической диффузией меди в пластинах X-среза ниобата лития.

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Держатели документа:
Томский государственный университет систем управления и радиоэлектроники
Институт физики им. Л.В. Киренского СО РАН
Сибирский федеральный университет

Доп.точки доступа:
Анисимов, Р. И.; Колмаков, А. А.; Темерева, А. С.; Шараева, А. Е.; Шандаров, С. М.; Тимофеев, Иван Владимирович; Timofeev, I. V.; Пятнов, Максим Владимирович; Pyatnov, M. V.; Международная конференция по фотонике и информационной оптике(11 ; 2022 ; 26-28 янв. ; Москва); Российская академия наук; Национальный исследовательский ядерный университет "МИФИ"
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The effect of copper and iron adsorption on the catalytic performance of alumina nanofiber / nanodiamond composite in sensing applications / N. O. Ronzhin, E. D. Posokhina, E. V. Mikhlina [et al.] // J. Phys. Chem. Solids. - 2022. - Vol. 167. - Ст. 110785, DOI 10.1016/j.jpcs.2022.110785. - Cited References: 68. - This work is supported by the Russian Foundation for Basic Research, Project 18–29–19078. The authors would like to express their special thanks to Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS» for providing the equipment to ensure the accomplishment of this project . - ISSN 0022-3697
Кл.слова (ненормированные):
Nanodiamonds -- Alumina nanofibers -- Indicator system -- Copper ions -- Iron ions -- Phenol detection
Аннотация: Phenolic compounds are common environmental pollutants, which are used in many industries and contaminate water environment due to industrial wastewater discharge. Presently, there is an increasing demand for the development and improvement of inexpensive, easy-to-use analytical tools for in-situ detection of phenolic compounds. In this work, we investigate the effect of adsorption of Cu2+ and Fe2+ ions on the catalytic activity of a composite material based on alumina nanofibers (ANF) and detonation nanodiamonds (DND) in the co-oxidation of phenols with 4-aminoantipyrine in the presence of hydrogen peroxide. We have found more than two-fold increase of the catalytic activity for ANF + DND + Cu composite, while the activity of ANF + DND + Fe composite is found to decrease by several times in comparison with the original ANF + DND material. The results of FTIR analysis indicate that the adsorption of iron ions occurs with the formation of hydroxide surface groups and hydrogen bonds, which apparently block their catalytic activity in the Fenton redox cycle. The higher catalytic performance of AND + DND composite functionalized with copper ions makes it possible to detect two times lower concentrations of analytes (phenol and 4-chlorophenol) in comparison with the original composite. It is shown that the AND + DND + Cu composite provides a linear yield of the co-oxidation reaction product in a wide range of analyte concentrations (0.25–100 μM for phenol and 0.5–25 μM for 4-chlorophenol). Model experiments demonstrate the applicability of copper-functionalized composite as a reusable sensor for the determination of phenol in aqueous samples.

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Держатели документа:
Institute of Biophysics SB RAS, Akademgorodok 50/50, Krasnoyarsk, 660036, Russian Federation
Institute of Computational Modelling SB RAS, Akademgorodok 50/44, Krasnoyarsk, 660036, Russian Federation
Kirensky Institute of Physics SB RAS, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
Federal Research Center KSC SB RAS, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodny 79, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Ronzhin, N. O.; Posokhina, E. D.; Mikhlina, E. V.; Shestakov, N. P.; Шестаков, Николай Петрович; Nemtsev, I. V.; Немцев, Иван Васильевич; Bondar, V. S.; Ryzhkov, I. I.
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10.

Flux pinning docking interfaces in satellites using superconducting foams as trapped field magnets / M. R. Koblischka, A. Koblischka-Veneva, D. Gokhfeld [et al.] // IEEE Trans. Appl. Supercond. - 2022. - Vol. 32, Is. 4. - Ст. 4900105, DOI 10.1109/TASC.2022.3147734. - Cited References: 44. - This work was supported in part by SUPERFOAM international project funded by ANR and DFG under Grants ANR-17-CE05-0030 and DFG-ANR Ko2323-10. . - ISSN 1051-8223. - ISSN 1558-2515

РУБ Engineering, Electrical & Electronic + Physics, Applied
Рубрики:
BULK
RECONFIGURATION
MAGNETIZATION
Кл.слова (ненормированные):
Superconducting magnets -- Satellites -- Yttrium barium copper oxide -- Magnetomechanical effects -- Magnetic fields -- Superconducting coils -- Magnetometers -- Flux-pinning docking interface -- Foams -- Trapped field magnets -- YBCO
Аннотация: Flux-Pinning Docking Interfaces (FPDI) in satellite systems were developed using bulk superconductors and permanent magnets in previous works. However, such FPDIs have limited magnetic field strength, consist of heavy-weight material, and can only be used with a single purpose, i.e., as chasing or docking satellite. Replacing the magnetic material in the FPDI by a trapped field (TF)-magnet would enable the interface to operate for both purposes, i.e., generating a (stronger) magnetic field and trapping it. We show the requirements for such a system and discuss the possible gains when using a TF-FPDI in satellites. To reduce the system weight, the use of superconducting foams as superconducting material is discussed in detail. Furthermore, the use of superconducting foams, the size of which can be easily upscaled, may also comprise the function of the damping material, so even more weight could be saved for the payload.

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Держатели документа:
Saarland Univ, Dept Expt Phys, D-66041 Saarbrucken, Germany.
Shibaura Inst Technol, Tokyo 1358548, Japan.
Fed Res Ctr KSC SB RAS, Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
Tokyo Univ Sci, Dept Phys, Tokyo 1628601, Japan.
Univ Lorraine, GREEN, F-54000 Nancy, France.

Доп.точки доступа:
Koblischka, Michael R.; Koblischka-Veneva, Anjela; Gokhfeld, D. M.; Гохфельд, Денис Михайлович; Naik, S. Pavan Kumar; Nouailhetas, Quentin; Berger, Kevin; Douine, Bruno; ANRFrench National Research Agency (ANR); DFGGerman Research Foundation (DFG)European Commission [ANR-17-CE05-0030, DFG-ANR Ko2323-10]
}
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11.

    Solid-state reaction in Cu/a-Si nanolayers: A comparative study of STA and electron diffraction data / E. T. Moiseenko, V. V. Yumashev, R. R. Altunin [и др.] // Materials. - 2022. - Vol. 15, Is. 23. - Ст. 8457, DOI 10.3390/ma15238457. - Cited References: 45. - This work was supported by the Russian Science Foundation under grant # 22-13-00313 . - ISSN 1996-1944
   Перевод заглавия: Твердофазная реакция в нанослоях Cu/a-Si: сравнительное исследование данных, полученных методами СТА и дифракции электронов
Кл.слова (ненормированные):
copper silicide -- thin films -- nanolayer -- solid-state reaction -- phase formation -- kinetics -- activation energy -- enthalpy -- DSC -- electron diffraction
Аннотация: The kinetics of the solid-state reaction between nanolayers of polycrystalline copper and amorphous silicon (a-Si) has been studied in a Cu/a-Si thin-film system by the methods of electron diffraction and simultaneous thermal analysis (STA), including the methods of differential scanning calorimetry (DSC) and thermogravimetry (TG). It has been established that, in the solid-state reaction, two phases are formed in a sequence: Cu + Si → η″-Cu3Si → γ-Cu5Si. It has been shown that the estimated values of the kinetic parameters of the formation processes for the phases η″-Cu3Si and γ-Cu5Si, obtained using electron diffraction, are in good agreement with those obtained by DSC. The formation enthalpy of the phases η″-Cu3Si and γ-Cu5Si has been estimated to be: ΔHη″-Cu3Si = −12.4 ± 0.2 kJ/mol; ΔHγ-Cu5Si = −8.4 ± 0.4 kJ/mol. As a result of the model description of the thermo-analytical data, it has been found that the process of solid-state transformations in the Cu/a-Si thin-film system under study is best described by a four-stage kinetic model R3 → R3 → (Cn-X) → (Cn-X). The kinetic parameters of formation of the η″-Cu3Si phase are the following: Ea = 199.9 kJ/mol, log(A, s−1) = 20.5, n = 1.7; and for the γ-Cu5Si phase: Ea = 149.7 kJ/mol, log(A, s−1) = 10.4, n = 1.3, with the kinetic parameters of formation of the γ-Cu5Si phase being determined for the first time.

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Держатели документа:
Laboratory of Electron Microscopy, Siberian Federal University, 79 Svobodny Ave., 660041 Krasnoyarsk, Russia
Institute of Chemistry and Chemical Technology, Federal Research Center KSC SB RAS, Akademgorodok 50/24, 660036 Krasnoyarsk, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50/38, 660036 Krasnoyarsk, Russia

Доп.точки доступа:
Moiseenko, E. T.; Yumashev, V. V.; Altunin, R. R.; Zeer, G. M.; Nikolaeva, N. S.; Belousov, O. V.; Zharkov, S. M.; Жарков, Сергей Михайлович
}
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12.

Multicomponent flux growth and composition control of Cu2MnBO5:Ga ludwigites / E. Moshkina, A. Krylov, D. Kokh [et al.] // CrystEngComm. - 2022. - Vol. 24, Is. 19. - P. 3565-3575, DOI 10.1039/d2ce00258b. - Cited References: 26. - This study was supported by the Russian Science Foundation (Grant No. 21-72-00130). The Raman, X-ray, and EDX data were obtained using the analytical equipment of the Krasnoyarsk Regional Center of Research Equipment of the Federal Research Center “Krasnoyarsk Science Center SB RAS” . - ISSN 1466-8033
Кл.слова (ненормированные):
Bismuth compounds -- Boron compounds -- Copper compounds -- Crystal symmetry -- Energy dispersive spectroscopy -- Gallium -- Manganese oxide -- Positive ions -- Sodium compounds
Аннотация: To reach the concentration phase boundary between antiferromagnetic Cu2GaBO5 and ferrimagnetic Cu2MnBO5 ludwigites, solid solutions Cu2Mn1−xGaxBO5 (x = 0.05, 0.1, 0.15, 0.175) were grown by the flux technique using a multi-component solvent based on Bi2Mo3O12 with the addition of Na2B4O7 which significantly influenced the crystal formation and cation composition of the studied compounds. The content of the flux system was corrected taking into account the earlier established relationship of the partition coefficients of Mn2O3 and Ga2O3. The influence of the solvent components on the ludwigite crystallization was analyzed. The maximum size of the grown crystal was 1 × 1 × 4 mm3. The structure and cation composition of the grown compounds were studied using X-ray (X-ray diffraction, EDX (energy-dispersive X-ray spectroscopy)) and vibrational (Raman) spectroscopy techniques. The phase boundary of Cu2MnBO5–Cu2GaBO5 was found to be in the concentration range of x = 0.15–0.175, corresponding to a change in the monoclinic axis direction and a leap in the lattice parameters. The symmetry evolution of metal–oxygen octahedra for four nonequivalent cation positions was analyzed, and the unique crystal structure of Cu2MnBO5 demonstrated high rigidity relative to the introduction of Ga3+ cations. The polarized Raman spectra of monoclinic ludwigites were obtained and studied for the first time. A comparison of the spectra of the studied samples in both phases and orthorhombic ludwigites was made. A number of spectral features due to the monoclinic distortions in the crystal were found. In agreement with the Raman experiment, the concentration phase boundary was close to 0.15.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian State University of Science and Technologies, Krasnoyarsk, 660037, Russian Federation
Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Far Eastern State Transport University, Khabarovsk, 680021, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
St Petersburg University, St Petersburg, 199034, Russian Federation

Доп.точки доступа:
Moshkina, E. M.; Мошкина, Евгения Михайловна; Krylov, A. S.; Крылов, Александр Сергеевич; Kokh, D.; Shabanova, K.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bovina, A. F.; Бовина, Ася Федоровна; Plyaskin, M.; Пляскин, Михаил Е.; Rostovtsev, N.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич
}
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13.

Synthesis and optical properties of nickel-doped copper metaborate crystals / A. D. Molchanova, E. M. Moshkina, M. S. Molokeev [et al.] // Opt. Spectrosc. - 2022. - Vol. 130, Is. 1. - P. 105-109, DOI 10.21883/EOS.2022.01.52994.41-21. - Cited References: 18. - The study was performed with the support of Russian Science Foundation, RSF grant № 19-12-00413 . - ISSN 0030-400X. - ISSN 1562-6911
Кл.слова (ненормированные):
3d-ions -- crystal growth -- optical spectroscopy -- magnetic ordering -- cuprates
Аннотация: This work presents information on the growth and spectroscopic study of single crystals of copper metaborate doped with nickel Cu1–xNixB2O4 (x = 0.05, 0.1). In the absorption spectra of both crystals, satellites related to Cu centers distorted by impurity Ni atoms were observed near the lines of zero phonon transitions. Polarization studies in the isotropic ab-plane of the tetragonal crystal Cu1–xNixB2O4 show the presence of linear magnetic dichroism in the magnetically ordered state, which was previously observed both in manganese-doped and undoped copper metaborates CuB2O4. The temperature of magnetic phase transitions into the collinear antiferromagnetic and into helicoidal structures, TN = 19.1 K and T* = 8.6 K, respectively, were determined from the temperature dependence of the dichroic signal.

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Держатели документа:
Institute of Spectroscopy, Russian Academy of Sciences, Troitsk, Moscow, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, Krasnoyarsk, Russia
Siberian Federal University, Krasnoyarsk, Russia
Scientific and innovative management, Kemerovo State University, Kemerovo, Russia

Доп.точки доступа:
Molchanova, A. D.; Moshkina, E. M.; Мошкина, Евгения Михайловна; Molokeev, M. S.; Молокеев, Максим Сергеевич; Tropina, E. V.; Bovina, A. F.; Бовина, Ася Федоровна; Boldyrev, K. N.
}
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14.

Low cost embedded copper mesh Based on cracked template for highly durability transparent EMI shielding films / A. S. Voronin, Y. V. Fadeev, M. O. Makeev [et al.] // Materials. - 2022. - Vol. 15, Is. 4. - Ст. 1449, DOI 10.3390/ma15041449. - Cited References: 55. - This research work was supported by the Ministry of Science and Higher Education of the Russian Federation within the framework of state tasks No. 0287-2021-0026 and No. 0705-2020-0032 . - ISSN 1996-1944

РУБ Chemistry, Physical + Materials Science, Multidisciplinary + Metallurgy & Metallurgical Engineering + Physics, Applied + Physics, Condensed Matter
Рубрики:
PERFORMANCE
   REALIZATION
   ELECTRODE
   NANOMESH
   PATTERN
Кл.слова (ненормированные):
transparent electromagnetic interference (EMI) shielding films -- cracked template -- electroplating -- photocurable resin -- embedded mesh -- durability
Аннотация: Embedded copper mesh coatings with low sheet resistance and high transparency were formed using a low-cost Cu seed mesh obtained with a magnetron sputtering on a cracked template, and subsequent operations electroplating and embedding in a photocurable resin layer. The influence of the mesh size on the optoelectric characteristics and the electromagnetic shielding efficiency in a wide frequency range is considered. In optimizing the coating properties, a shielding efficiency of 49.38 dB at a frequency of 1 GHz, with integral optical transparency in the visible range of 84.3%, was obtained. Embedded Cu meshes have been shown to be highly bending stable and have excellent adhesion strength. The combination of properties and economic costs for the formation of coatings indicates their high prospects for practical use in shielding transparent objects, such as windows and computer monitors.

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Держатели документа:
Russian Acad Sci, Dept Mol Elect, Fed Res Ctr, Krasnoyarsk Sci Ctr,Siberian Branch,FRC,KSC,SB,RA, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Sch Engn & Construct, Krasnoyarsk 660041, Russia.
Bauman Moscow State Syst Univ, Lab EMI Shielding Mat, Moscow 105005, Russia.
Russian Acad Sci, Lab Reinforced Plast, NN Semenov Fed Res Ctr Chem Phys, Moscow 119991, Russia.
Siberian Fed Univ, Sch Nonferrous Met & Mat Sci, Krasnoyarsk 660041, Russia.
Reshetnev Siberian Univ Sci & Technol, Dept Aircraft, Krasnoyarsk 660037, Russia.
Siberian Fed Univ, Sch Engn Phys & Radio Elect, Krasnoyarsk 660041, Russia.
Russian Acad Sci, Lab Radiospectroscopy & Spintron, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia.
Reshetnev Siberian Univ Sci & Technol, Sci & Training Ctr Space Res, Krasnoyarsk 660037, Russia.
Reshetnev Siberian Univ Sci & Technol, High Technol Inst, Krasnoyarsk 660037, Russia.
Tomsk Polytech Univ, Lab Radiat & Plasma Technol, Tomsk 634050, Russia.
Russian Acad Sci, Lab Radiophoton, Siberian Branch, VE Zuev Inst Atmospher Opt, Tomsk 634055, Russia.
Russian Acad Sci, Lab Photon Mol Syst, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia.
LLC Res & Prod Co Spectehnauka, Krasnoyarsk 660043, Russia.

Доп.точки доступа:
Voronin, Anton S.; Fadeev, Yurii V.; Makeev, Mstislav O.; Mikhalev, Pavel A.; Osipkov, Alexey S.; Provatorov, Alexander S.; Ryzhenko, Dmitriy S.; Yurkov, Gleb Y.; Simunin, Mikhail M.; Karpova, Darina V.; Lukyanenko, A. V.; Лукьяненко, Анна Витальевна; Kokh, Dieter; Bainov, Dashi D.; Tambasov, I. A.; Тамбасов, Игорь Анатольевич; Nedelin, Sergey V.; Zolotovsky, Nikita A.; Khartov, Stanislav V.; Ministry of Science and Higher Education of the Russian Federation [0705-2020-0032]; [0287-2021-0026]
}
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15.

    Электрофизические характеристики полимерного композита на основе сверхвысокомолекулярного полиэтилена с наночастицами CuO / Л. Ю. Федоров, Н. А. Дрокин, И. В. Карпов, А. В. Ушаков // Журн. СФУ. Техн. и технол. - 2022. - Т. 15, № 7. - С. 802-811 ; J. Sib. Fed. Univ. Eng. Technol., DOI 10.17516/1999-494X-0437. - Библиогр.: 19. - Исследование выполнено за счет гранта Российского научного фонда (проект № 20-19-00021) . - ISSN 1999-494X. - ISSN 2313-6057
   Перевод заглавия: Electrophysical characteristics of a polymer composite based on ultrahigh molecular weight polyethylene with CuO nanoparticles
Кл.слова (ненормированные):
вакуумный дуговой разряд -- нанокомпозиты -- оксид меди -- импеданс -- диэлектрические свой -- vacuum arc discharge -- nanocomposites -- copper oxide -- impedance -- dielectric properties
Аннотация: Методом импедансной спектроскопии исследованы электрофизические свойства композитного материала на основе сверхвысокомолекулярного полиэтилена с ограниченной массовой концентрацией 0,5 мас.% оксида меди CuO в диапазоне частот от 102 до 108 Гц. Предполагается, что введение в состав полимера малых концентраций наночастиц способствует более равномерному их осаждению на поверхностях полимерных гранул. Это позволяет в процессе тестирования таких образцов выявить наиболее вероятные механизмы их поляризации и протекания электрического тока в относительно однородном ансамбле наночастиц в полимерной матрице. Установлено, что внедряемые в полимерную матрицу наночастицы незначительно влияют на процессы электрической поляризации, но приводят к появлению частотно-зависимой проводимости в широком диапазоне частот. Этот процесс сопровождается существенным возрастанием диэлектрических потерь. Электрофизические характеристики полученных композитов обсуждаются с учётом переноса электрических зарядов (ионов или электронов) как по внутренней, так и по поверхностной структуре наночастиц CuO.
The electrophysical properties of a composite material based on ultrahigh molecular weight polyethylene with a limited mass concentration of 0.5 wt% copper oxide CuO in the frequency range from 102 to 108 Hz were studied by impedance spectroscopy. It is assumed that the introduction of low concentrations of nanoparticles into the polymer composition contributes to their more uniform deposition on the surfaces of polymer granules. This makes it possible to reveal the most probable mechanisms of their polarization and the flow of electric current in a relatively homogeneous ensemble of nanoparticles in a polymer matrix during testing of such samples. It has been established that nanoparticles introduced into the polymer matrix have little effect on the processes of electric polarization, but lead to the appearance of frequency-dependent conductivity in a wide frequency range. This process is accompanied by a significant increase in dielectric losses. The electrophysical characteristics of the resulting composites are discussed taking into account the transfer of electric charges (ions or electrons) both along the internal and surface structures of CuO nanoparticles.

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Держатели документа:
Сибирский федеральный университет, Российская Федерация, Красноярск
Федеральный исследовательский центр «Красноярский научный центр СО РАН», Российская Федерация, Красноярск
Институт физики им. Л. В. Киренского ФИЦ КНЦ СО РАН, Российская Федерация, Красноярск

Доп.точки доступа:
Федоров, Л. Ю.; Дрокин, Николай Александрович; Drokin, N. A.; Карпов, И. В.; Ушаков, А. В.

}
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16.

Crystal structure and thermodynamic properties of germanate CuEu2Ge2O8 / L. T. Denisova, M. S. Molokeev, L. A. Irtyugo [et al.] // Phys. Solid State. - 2022. - Vol. 64, Is. 12. - P. 2045-2048, DOI 10.21883/PSS.2022.12.54406.460. - Cited References: 18. - The work has been partially funded within the framework of the state science assignment of Federal State Independent Institution for Higher Education ”Siberian Federal University“, project number FSRZ-2020-0013 . - ISSN 1063-7834. - ISSN 1090-6460
Кл.слова (ненормированные):
copper-europium germanate -- solid-phase synthesis -- crystal structure -- thermodynamic properties
Аннотация: Copper-europium germanate CuEu2Ge2O8 was obtained from the initial CuO, Eu2O3 and GeO2 oxides using solid-phase synthesis by annealing in air in the temperature range of 1223-1273 K. Its crystal structure was determined (space group Cm). The influence of temperature on high-temperature heat capacity of the synthesized germanate was studied by the differential scanning calorimetry method. It was found that the dependence of heat capacity on temperature has an extreme value related to a phase transition. The thermodynamic properties were calculated based on the experimental data about heat capacity.

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Публикация на русском языке Кристаллическая структура и термодинамические свойства германата CuEu2Ge2O8 [Текст] / Л. Т. Денисова, М. С. Молокеев, Л. А. Иртюго [и др.] // Физ. тверд. тела. - 2022. - Т. 64 Вып. 12. - С. 2090-2093

Держатели документа:
Siberian Federal University, Krasnoyarsk, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, Krasnoyarsk, Russia

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Irtyugo, L. A.; Belousova, N. V.; Denisov, V. M.
}
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17.

    Synthesis and characterization of nanoscale composite particles formed by 2D layers of Cu-Fe sulfide and Mg-based hydroxide / Y. L. Mikhlin, R. V. Borisov, S. A. Vorobyev [et al.] // J. Mater. Chem. A. - 2022. - Vol. 10, Is. 17. - P. 9621-9634, DOI 10.1039/d2ta00877g. - Cited References: 84. - This research was supported by the Russian Foundation for Basic Research, Krasnoyarsk Territory Administration and Krasnoyarsk Territory Science Foundation, project 20-43-242903. Facilities of the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” were employed in the work . - ISSN 2050-7488
   Перевод заглавия: Синтез и исследование наноразмерных композитных частиц, образованных двумерными слоями сульфида Cu-Fe и гидроксида на основе Mg
Кл.слова (ненормированные):
Binary alloys -- Copper compounds -- Electron energy levels -- Electron energy loss spectroscopy -- Electron scattering -- Light absorption -- Light scattering -- Magnesium compounds -- Near infrared spectroscopy -- Paramagnetism -- Sols -- Sulfur compounds -- X-ray photoelectron spectroscopy
Аннотация: We introduce here a multifunctional material composed of alternating atomic sulfide sheets close to the composition of CuFeS2 and Mg-based hydroxide ones (valleriite), which are assembled due to their electric charges of opposite sign. Valleriite particles 50-200 nm in lateral size and 10-20 nm in thickness were synthesized via a simple hydrothermal pathway using various concentrations of precursors and dopants, and examined with XRD, TEM, EDS, X-ray photoelectron spectroscopy, reflection electron energy loss spectroscopy (REELS), Mossbauer, Raman and UV-vis-NIR spectroscopies, and magnetization, dynamic light scattering, and zeta potential measurements. The electronic, magnetic and optical characteristics are found to be critically dependent on the charge (electron density) at the narrow-gap sulfide layers containing Cu+ and Fe3+ cations, and can be tuned via the composition of the hydroxide part. Particularly, substitution of Mg2+ with Al3+ increases the negative charge of the hydroxide layers and reduces the content of Fe3+-OH centers (10-45% of total iron); the effects of Cr and Co dopants entering both layers are more complicated. Mossbauer doublets of paramagnetic Fe3+ detected at room temperature transform into several Zeeman sextets at 4.2 K; the hyperfine fields up to 500 kOe and complex magnetic behavior, but not pure paramagnetism or antiferromagnetism, were observed for valleriites with the higher positive charge of the sulfide sheets, probably due to the depopulation of the minority-spin 3d states of S-bonded Fe3+ ions. Aqueous colloids of valleriite show optical absorption at 500-750 nm, which, along with the peaks at the same energies in REELS, may arise due to quasi-static dielectric resonance involving the vacant Fe 3d band and being dependent on the composition of both layers too. These and other findings call attention to valleriites as a new rich family of 2D materials for a variety of potential applications.

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Держатели документа:
Institute of Chemistry and Chemical Technology, Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of sciences, Akademgorodok, 50/24, Krasnoyarsk, 660036, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of sciences, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodny av. 79, Krasnoyarsk, 660041, Russian Federation
Federal Research Center “Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of sciences”, Akademgorodok, 50, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Mikhlin, Y. L.; Borisov, R. V.; Vorobyev, S. A.; Tomashevich, Y. V.; Romanchenko, A. S.; Likhatski, M. N.; Karacharov, A. A.; Bayukov, O. A.; Баюков, Олег Артемьевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Krylov, A. S.; Крылов, Александр Сергеевич; Krylova, S. N.; Крылова, Светлана Николаевна; Nemtsev, I. V.; Немцев, Иван Васильевич
}
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18.

    Zero-Dimensional Organic Copper(I) Iodide Hybrid with High Anti-Water Stability for Blue-Light-Excitable Solid-State Lighting / B. Su, J. Jin, Y. Peng [et al.] // Adv. Opt. Mater. - 2022. - Vol. 10, Is. 12. - Ст. 2102619, DOI 10.1002/adom.202102619. - Cited References: 55. - This work was supported by the National Natural Science Foundation of China (Nos.: 51961145101 and 51972118), Guangzhou Science & Technology Project (202007020005), and the Local Innovative and Research Teams Project of Guangdong Pearl River Talents Program(2017BT01×137). This work was also funded by RFBR according to the research Project No.19-52-80003 . - ISSN 2195-1071
   Перевод заглавия: Нульмерный металлорганический гибрид йодида меди(I) с высокой водостойкостью для ламп, возбуждаемых синим светом
Кл.слова (ненормированные):
anti-water stability -- copper(I) iodide cluster -- light-emitting diodes -- photoluminescence -- zero-dimensional metal halides
Аннотация: The discovery of rare-earth free luminescent materials with blue-light-excitable characteristic is of great importance for solid-sate lighting applications. Herein, a Cu(I)-based 0D luminescent hybrid (1,3-dppH2)2Cu4I8∙H2O is synthesized by a facile solution method, and it shows the orange-red emission peaking at 625 nm upon 460 nm excitation. The structure-related luminescence mechanism has been elaborated by experimental and theoretical investigations. Moreover, the emission intensity remains unchanged even after continuous water treatment for 60 days due to the improved structural stability originating from intermolecular π–π interaction between organic cations. A warm white light-emitting diode (LED) device with the color rendering index of 91.4% has been fabricated by combining the 440 nm LED chip, green-emitting Lu3Al5O12:Ce3+, and (1,3-dppH2)2Cu4I8∙H2O. This work provides a new design route towards 0D cuprous halide materials and will initiate more exploration of their intrinsic luminescence mechanism.

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Держатели документа:
The State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, School of Materials Science and Engineering, South China University of Technology, Guangzhou, 510641, China
School of Physics and Optoelectronics, South China University of Technology, Guangzhou, 510641, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Department of Engineering Physics and Radioelectronic, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Research and Development Department, Kemerovo State University, Kemerovo, 650000, Russian Federation

Доп.точки доступа:
Su, B.; Jin, J.; Peng, Y.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Yang, X.; Xia, Z.
}
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19.

    Destruction of long-range magnetic order in an external magnetic field and the associated spin dynamics in Cu2GaBO5 and Cu2AlBO5 ludwigites / A. A. Kulbakov, R. Sarkar, O. Janson [et al.] // Phys. Rev. B. - 2021. - Vol. 103, Is. 2. - Ст. 024447, DOI 10.1103/PhysRevB.103.024447. - Cited References: 46. - We thank U. Nitzsche for technical assistance. This project was funded in part by the German Research Foundation (DFG) under Grant IN 209/9-1, via Project C03 of the Collaborative Research Center SFB 1143 (project-id 247310070) at the TU Dresden, and the Würzburg-Dresden Cluster of Excellence on Complexity and Topology in Quantum Matter—ct.qmat (EXC 2147, project-id 390858490). O.J. was supported by the Leibniz Association through the Leibniz Competition . - ISSN 2469-9950
   Перевод заглавия: Разрушение дальнего магнитного порядка во внешнем магнитном поле и связанная с ним спиновая динамика в людвигитах Cu2GaBO5 и Cu2AlBO5
Кл.слова (ненормированные):
Aluminum compounds -- Antiferromagnetic materials -- Antiferromagnetism -- Band structure -- Copper compounds -- Crystal structure -- Density functional theory -- Gallium compounds -- Magnetic fields -- Neutron diffraction -- Neutron scattering -- Spin fluctuations -- Spin glass -- Temperature -- Antiferromagnetic exchange -- Antiferromagnetic orderings -- Brillouin zone boundary -- External magnetic field -- Long range magnetic order -- Long-range-ordered state -- Quantum spin systems -- Two-dimensional spin model -- Boron compounds
Аннотация: The quantum spin systems Cu2M′BO5 (M′=Al,Ga) with the ludwigite crystal structure consist of a structurally ordered Cu2+ sublattice in the form of three-leg ladders, interpenetrated by a structurally disordered sublattice with a statistically random site occupation by magnetic Cu2+ and nonmagnetic Ga3+ or Al3+ ions. A microscopic analysis based on density-functional-theory calculations for Cu2GaBO5 reveals a frustrated quasi-two-dimensional spin model featuring five inequivalent antiferromagnetic exchanges. A broad low-temperature 11B nuclear magnetic resonance points to a considerable spin disorder in the system. In zero magnetic field, antiferromagnetic order sets in below TN≈4.1 K and ∼2.4 K for the Ga and Al compounds, respectively. From neutron diffraction, we find that the magnetic propagation vector in Cu2GaBO5 is commensurate and lies on the Brillouin-zone boundary in the (H0L) plane, qm=(0.45,0,−0.7), corresponding to a complex noncollinear long-range ordered structure with a large magnetic unit cell. Muon spin relaxation is monotonic, consisting of a fast static component typical for complex noncollinear spin systems and a slow dynamic component originating from the relaxation on low-energy spin fluctuations. Gapless spin dynamics in the form of a diffuse quasielastic peak is also evidenced by inelastic neutron scattering. Most remarkably, application of a magnetic field above 1 T destroys the static long-range order, which is manifested in the gradual broadening of the magnetic Bragg peaks. We argue that such a crossover from a magnetically long-range ordered state to a spin-glass regime may result from orphan spins on the structurally disordered magnetic sublattice, which are polarized in magnetic field and thus act as a tuning knob for field-controlled magnetic disorder.

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Держатели документа:
Institut fur Festkorper- und Materialphysik, Technische Universitat Dresden, Dresden, 01069, Germany
Wurzburg-Dresden Cluster of Excellence on Complexity and Topology in Quantum Matter - Ct.qmat, TU Dresden, Dresden, 01069, Germany
Institute for Theoretical Solid State Physics, IFW Dresden, Dresden, 01069, Germany
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50, Krasnoyarsk, 660036, Russian Federation
Laboratory for Muon Spin Spectroscopy, Paul Scherrer Institute, Villigen PSI, CH-5232, Switzerland
Institute for Quantum Phenomena in Novel Materials, Helmholtz-Zentrum Berlin fur Materialen und Energie GmbH, Hahn-Meitner-Platz 1, Berlin, 14109, Germany
Max Planck Institute for Chemical Physics of Solids, Nothnitzer Str. 40, Dresden, 01187, Germany
Zavoisky Physical-Technical Institute, FRC Kazan Scientific Center of RAS, Sibirsky tract 10/7, Kazan, 420029, Russian Federation
Fakultat Chemie und Lebensmittelchemie, Technische Universitat Dresden, Dresden, 01069, Germany
Julich Center for Neutron Science at MLZ, Forschungszentrum Julich GmbH, Lichtenbergstra?e 1, Garching, 85748, Germany

Доп.точки доступа:
Kulbakov, A. A.; Sarkar, R.; Janson, O.; Dengre, S.; Weinhold, T.; Moshkina, E. M.; Мошкина, Евгения Михайловна; Portnichenko, P. Y.; Luetkens, H.; Yokaichiya, F.; Sukhanov, A. S.; Eremina, R. M.; Schlender, P.; Schneidewind, A.; Klauss, H. -H.; Inosov, D. S.
}
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20.

    Peculiarities of Intermetallic Phase Formation in the Process of a Solid State Reaction in (Al/Cu)n Multilayer Thin Films / E. T. Moiseenko, S. M. Zharkov, R. R. Altunin [et al.] // JOM. - 2021. - Vol. 73, Is. 2. - P. 580-588, DOI 10.1007/s11837-020-04522-9. - Cited References: 44. - This work was supported by the Russian Science Foundation under Grant #18-13-00080. The electron microscopy investigations were conducted in the SFU Joint Scientific Center whose infrastructure was supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation. The preparation of cross-section samples for TEM investigations was conducted in the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” . - ISSN 1047-4838
   Перевод заглавия: Особенности формирования интерметаллических фаз в процессе твердофазной реакции в многослойных тонких пленках (Al/Cu)
Кл.слова (ненормированные):
Bilayer thin films -- Copper diffusion -- In-situ transmission electron microscopies -- Intermetallic phase -- Multi-layer thin film -- Phase formation process -- Phase formation sequence -- Simultaneous thermal analysis
Аннотация: Phase formation in a solid state reaction in Al/Cu bilayer and multilayer thin films was studied by the methods of in situ transmission electron microscopy, electron diffraction, simultaneous thermal analysis and x-ray diffraction. It was established that the phase formation sequences in the (Al/Cu)n (n = 2, 15) multilayer thin films (θ-Al2Cu → γ1-Al4Cu9 → η2-AlCu) and Al/Cu bilayer thin films (θ-Al2Cu → η2-AlCu → γ1-Al4Cu9) were different. It was assumed that the phase formation process in the thin films was strongly affected by a number of copper/aluminum interfaces due to the changes of aluminum and copper diffusion current.

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Держатели документа:
Siberian Federal University, 79 Svobodny pr., Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
Institute of Chemistry and Chemical Technology, Federal Research Center KSC SB RAS, Akademgorodok 50/24, Krasnoyarsk, 660036, Russian Federation
Reshetnev Siberian State University of Science and Technology, Krasnoyarskij Rabochij 31, Krasnoyarsk, 660037, Russian Federation

Доп.точки доступа:
Moiseenko, E. T.; Zharkov, S. M.; Жарков, Сергей Михайлович; Altunin, R. R.; Belousov, O. V.; Solovyov, L. A.; Yumashev, V. V.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Zeer, G. M.
}
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