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Structural, optical, and electronic properties of Cu-doped TiNxOy grown by ammonothermal atomic layer deposition / F. A. Baron, Y. L. Mikhlin, M. S. Molokeev [et al.] // ACS Appl. Mater. Interfaces. - 2021. - Vol. 13, Is. 27. - P. 32531-32541, DOI 10.1021/acsami.1c08036. - Cited References: 69. - This research was funded by the RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science (project code 20-42-240013) and by the grant of the Government of the Russian Federation for Creation of World Tier Laboratories (contract no. 075-15-2019-1886) . - ISSN 1944-8244. - ISSN 1944-8252

РУБ Nanoscience & Nanotechnology + Materials Science, Multidisciplinary
Рубрики:
OXYNITRIDE THIN-FILMS
TITANIUM-NITRIDE
CONFORMAL TIN
Кл.слова (ненормированные):
atomic layer deposition -- titanium oxynitride -- copper doping -- surface segregation -- thin film
Аннотация: Copper-doped titanium oxynitride (TiNxOy) thin films were grown by atomic layer deposition (ALD) using the TiCl4 precursor, NH3, and O2 at 420 °C. Forming gas was used to reduce the background oxygen concentration and to transfer the copper atoms in an ALD chamber prior to the growth initiation of Cu-doped TiNxOy. Such forming gas-mediated Cu-doping of TiNxOy films had a pronounced effect on their resistivity, which dropped from 484 ± 8 to 202 ± 4 μΩ cm, and also on the resistance temperature coefficient (TCR), which decreased from 1000 to 150 ppm °C–1. We explored physical mechanisms causing this reduction by performing comparative analysis of atomic force microscopy, X-ray photoemission spectroscopy, X-ray diffraction, optical spectra, low-temperature transport, and Hall measurement data for the samples grown with and without forming gas doping. The difference in the oxygen concentration between the films did not exceed 6%. Copper segregated to the TiNxOy surface where its concentration reached 0.72%, but its penetration depth was less than 10 nm. Pronounced effects of the copper doping by forming gas included the TiNxOy film crystallite average size decrease from 57–59 to 32–34 nm, considerably finer surface granularity, electron concentration increase from 2.2(3) × 1022 to 3.5(1) × 1022 cm–3, and the electron mobility improvement from 0.56(4) to 0.92(2) cm2 V–1 s–1. The DC resistivity versus temperature R(T) measurements from 4.2 to 300 K showed a Cu-induced phase transition from a disordered to semimetallic state. The resistivity of Cu-doped TiNxOy films decreased with the temperature increase at low temperatures and reached the minimum near T = 50 K revealing signatures of the quantum interference effects similar to 2D Cu thin films, and then, semimetallic behavior was observed at higher temperatures. In TiNxOy films grown without forming gas, the resistivity decreased with the temperature increase as R(T) = – 1.88T0.6 + 604 μΩ cm with no semimetallic behavior observed. The medium range resistivity and low TCR of Cu-doped TiNxOy make this material an attractive choice for improved matching resistors in RF analog circuits and Si complementary metal–oxide–semiconductor integrated circuits.

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Держатели документа:
KSC SB RAS, Inst Chem & Chem Technol, Fed Res Ctr, Krasnoyarsk 660036, Russia.
KSC SB RAS, Kirensky Inst Phys, Fed Res Ctr, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Reshetnev Siberian State Univ Sci & Technol, Krasnoyarsk 660037, Russia.

Доп.точки доступа:
Baron, F. A.; Барон, Филипп Алексеевич; Mikhlin, Yurii L.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Rautskiy, M. V.; Рауцкий, Михаил Владимирович; Tarasov, I. A.; Тарасов, Иван Анатольевич; Volochaev, M. N.; Волочаев, Михаил Николаевич; Shanidze, L. V.; Шанидзе, Лев Викторович; Lukyanenko, A. V.; Лукьяненко, Анна Витальевна; Smolyarova, T. E.; Смолярова, Татьяна Евгеньевна; Konovalov, Stepan O.; Zelenov, Fyodor, V; Tarasov, A. S.; Тарасов, Антон Сергеевич; Volkov, N. V.; Волков, Никита Валентинович; RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science [20-42-240013]; Government of the Russian Federation for Creation of World Tier Laboratories [075-15-2019-1886]
}
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Features of MagMAX thin film deposition techniques / S. A. Lyashchenko, I. A. Yakovlev, A. S. Tarasov [et al.] // International workshop on the properties of functional MAX-materials (2nd FunMax) : book of abstracts / org. com. M. Farle [et al.]. - 2021. - P. 14

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Доп.точки доступа:
Farle, M. \org. com.\; Ovchinnikov, S. G. \org. com.\; Овчинников, Сергей Геннадьевич; Tarasov, A. S. \org. com.\; Тарасов, Антон Сергеевич; Smolyarova, T. E. \org. com.\; Смолярова, Татьяна Евгеньевна; Lyashchenko, S. A.; Лященко, Сергей Александрович; Yakovlev, I. A.; Яковлев, Иван Александрович; Tarasov, A. S.; Shevtsov, D. V.; Шевцов, Дмитрий Валентинович; Varnakov, S. N.; Варнаков, Сергей Николаевич; Ovchinnikov, S. G.; Farle, M.; Фарле, Михаель; International workshop on functional MAX-materials(2 ; 2021 ; Sept. 14-17 ; Krasnoyarsk (on-line)); Kirensky Institute of Physics; Siberian Federal Univercity
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Solovev, P. N.
Numerical study of structural and magnetic properties of thin films obliquely deposited on rippled substrates / P. N. Solovev, A. V. Izotov, B. A. Belyaev // J. Phys.: Condens. Matter. - 2021. - Vol. 33, Is. 49. - Ст. 495802, DOI 10.1088/1361-648X/ac26fc. - Cited References: 35. - The reported study was funded by RFBR, the Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund and JSC 'NPP Radiosviaz', Project Number 20-42-242901 . - ISSN 0953-8984. - ISSN 1361-648X

РУБ Physics, Condensed Matter
Рубрики:
SIMULATION
ANISOTROPY
GROWTH
Кл.слова (ненормированные):
oblique deposition -- micromagnetic simulation -- thin film growth simulation -- rippled substrate -- magnetic anisotropy -- magnetization reversal
Аннотация: Structural modulation in thin films plays a substantial role in the formation of their magnetic properties. By producing topographic patterns in thin films, it is possible to engineer their magnetic response. Here, we report on the numerical study of the relationship between structural and static magnetic properties of thin films obliquely deposited on substrates with the sinusoidal surface. 3D Monte Carlo film growth simulations show that, under certain deposition conditions, an inhomogeneous columnar morphology can form in the films caused by the shadowing effect and the rippled substrate. Calculations of the demagnetizing tensors for these films demonstrate that their columnar structure is the source of the shape-induced uniaxial magnetic anisotropy that varies nonmonotonically with the deposition angle. Micromagnetic simulations of the generated films confirm the uniaxial character of the shape-induced anisotropy, and also show that magnetization reversal occurs via an incoherent rotation of magnetic moments.

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Держатели документа:
Fed Res Ctr KSC SB RAS, Kirensky Inst Phys, 50-38 Akademgorodok, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, 79 Svobodny Pr, Krasnoyarsk 660041, Russia.

Доп.точки доступа:
Izotov, A. V.; Изотов, Андрей Викторович; Belyaev, B. A.; Беляев, Борис Афанасьевич; Соловьев, Платон Николаевич; RFBRRussian Foundation for Basic Research (RFBR); Government of Krasnoyarsk Territory; Krasnoyarsk Regional Fund; JSC 'NPP Radiosviaz' [20-42-242901]
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Magnetostructural study of nanostructured and amorphous bulk alloys (Co–P)100–xCux / L. A. Kuzovnikova, E. A. Denisova, I. V. Nemtsev [et al.] // J. Struct. Chem. - 2021. - Vol. 62, Is. 5. - P. 802-809, DOI 10.1134/S0022476621050164. - Cited References: 19. - The study was supported by RFBR, the Government of the Krasnoyarsk Region, and the Krasnoyarsk Regional Science Foundation within project No. 20-43-240003 . - ISSN 0022-4766
Кл.слова (ненормированные):
cobalt–copper composite material -- chemical deposition -- magnetic properties -- amorphous bulk alloys -- dynamic compaction
Аннотация: The work reports a magnetostructural study of bulk nanostructured composite materials Co–P/Cu prepared by dynamic compaction (DC) and uniaxial cold pressing (CP). The initial particles with amorphous and crystalline structure are synthesized by chemical deposition. Magnetic characteristics of composites (saturation magnetization, Bloch constant, local anisotropy field, ferro-magnetic resonance line width, coercive force) are studied. The phase compositions of initial composite particles and compacts prepared by two methods (DC and CP) are determined from the anisotropy field and the Bloch constant values using magnetic phase analysis. It is shown that the use of composite particles in dynamic compaction allows obtaining homogeneous nanostructured bulk materials while preserving magnetic characteristics of initial powders.

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Публикация на русском языке Исследование наноструктурированных и аморфных объемных сплавов (Со–Р)100-хСuх магнитоструктурными методами [Текст] / Л. А. Кузовникова, Е. А. Денисова, И. В. Немцев [и др.] // Журн. структ. химии. - 2021. - Т. 62 № 5. - С. 861-869

Держатели документа:
Krasnoyarsk Transport Institute, Branch of the Federal State Budget Institution of Higher Education “Irkutsk State Transport University IrGUPS”, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics, Federal Research Center, Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
Federal Research Center Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Kuzovnikova, L. A.; Кузовникова, Людмила Александровна; Denisova, E. A.; Денисова, Елена Александровна; Nemtsev, I. V.; Немцев, Иван Васильевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Kuzovnikov, A. A.; Maltsev, V. K.; Мальцев, Вадим Константинович; Shepeta, N. A.
}
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    Induced magnetic anisotropy of Co-P thin films obtained by electroless deposition / A. V. Chzhan, S. A. Podorozhnyak, S. M. Zharkov [et al.] // J. Magn. Magn. Mater. - 2021. - Vol. 537. - Ст. 168129, DOI 10.1016/j.jmmm.2021.168129. - Cited References: 28. - The work is partially supported by the RFBR Foundation (10-02-00161-a project). The study has been carried out within the framework of the state task of the Ministry of science and higher education of the Russian Federation (topic No. FSRZ-2020-0011) . - ISSN 0304-8853
   Перевод заглавия: Индуцированная магнитная анизотропия тонких пленок Co-P, полученных химическим осаждением
Кл.слова (ненормированные):
Cobalt -- Cobalt compounds -- Coercive force -- Drops -- Electroless plating -- Magnetic anisotropy -- Magnetic fields -- Cover glass -- Deposition of films -- Diffraction peaks -- Electroless -- Hydrogen indices -- Induced magnetic anisotropy -- Magnetic anisotropy constant -- pH range -- Thin-films
Аннотация: Co1−x-Px films (x = 0.02–0.05) deposited on cover glass by electroless plating from aqueous solutions in a continuous magnetic field with the strength of 2.5 kOe are presented. It has been found that in the pH range from 7.2 to 9.3, two special areas can be distinguished, they are characterized by the deposition of films with qualitatively different parameters in them. So, the change of the pH of working solutions from 7.2 to 8.7 causes the increase in the value of the induced magnetic anisotropy constant KU from 2.5 × 105 erg/cm3 to 6 × 105 erg/cm3. If the value of the hydrogen index is still increasing, an uneven drop to 5 × 104 erg/cm3 is observed. In the same way, the coercivity HC changes; at first it grows from 700 Oe to 1.5 kOe, and then it drops to Oe units. The concentration of phosphorus in the range of 7.2 to 8.7 increases linearly from 2 to 3 wt%, and in the range of 8.7 to 9.3, it increases from 3 to 5 wt%. The x-ray diffraction data show that the samples obtained at pH<8.7 are characterized by the presence of the hcp phase of Co (α-Co). The observed reflections of films obtained at pH > 8.7 indicate the fcc-Co (β-Co) with the diffraction peak blurring: the greater the pH value of the samples obtained, the more the diffraction peak blurring. It is shown that the induced magnetic anisotropy in high-coercivity films relates to the modification of the Co lattice. The lattice passes from a distorted fcc to an hcp structure during the growth of crystallites in a magnetic field. The induced magnetic anisotropy appears in films that were obtained in the high pH field due to the ordering of magnetic ions pairs.

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Держатели документа:
Siberian Federal University, Krasnoyarsk, Russian Federation
Krasnoyarsk State Agrarian University, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Nikolaev Institute of Inorganic Chemistry SB RAS, ave. Lavrentyev 3, Novosibirsk, Russian Federation

Доп.точки доступа:
Chzhan, A. V.; Podorozhnyak, S. A.; Zharkov, S. M.; Жарков, Сергей Михайлович; Gromilov, S. A.; Patrin, G. S.; Патрин, Геннадий Семёнович
}
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    Iron-cobalt coatings produced using an eco-friendly route / E. A. Denisova, L. A. Chekanova, S. V. Komogortsev [et al.] // J. Supercond. Nov. Magn. - 2021. - Vol. 34, Is. 10. - P. 2681-2688, DOI 10.1007/s10948-021-05964-1. - Cited References: 35. - This work was funded by the Russian Foundation for Basic Research, Krasnoyarsk Territory, and Krasnoyarsk Regional Fund of Science, project number 20-43-240003 . - ISSN 1557-1939. - ISSN 1557-1947
   Перевод заглавия: Железо-кобальтовые покрытия, полученные экологически чистым путем

РУБ Physics, Applied + Physics, Condensed Matter
Рубрики:
MAGNETIC-PROPERTIES
   FECO FILMS
   THIN-FILMS
   CO-FE
   ELECTRODEPOSITION
Кл.слова (ненормированные):
High-induction Fe-Co coating -- Electroless deposition -- Structure -- Magnetic properties -- Eco-friendly synthesis
Аннотация: A facile, low-cost, and green route for synthesis of high-induction Fe-Co coatings was developed. Within this approach, three natural reducing agents have been used for deposition of the metal coatings by electroless plating on dielectric and metallic substrates: arabinogalactan, starch, and sucrose. The Fe-Co alloy coatings with Co content from 0 to 94 at.% are nanocrystalline bcc solid solution with carbon additive no more than 2 at%, and pure Co coatings are of hcp structure. The magnetic properties of bcc-based iron-cobalt alloys have been investigated as a function of the atomic composition. A high-saturation magnetization of about 240 emu/g was obtained for Fe70Co30 alloy films deposited onto copper substrate. The local magnetic anisotropy of FeCo alloys increases with a decrease in iron content for all reducing agents. High magnetization close to those in the bulk Fe-Co alloys implies the prospective applications of synthesized Fe-Co coatings as magnetic shield and magnetic sensors.

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Держатели документа:
Fed Res Ctr KSC SB RAS, Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Res Ctr KSC SB RAS, Sci Ctr, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Denisova, E. A.; Денисова, Елена Александровна; Chekanova, L. A.; Чеканова, Лидия Александровна; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Nemtsev, I. V.; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Dolgopolova, M. V.
}
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    Core-shell and Bi-segmented cobalt-nickel nanorods prepared by electroless deposition / E. A. Denisova, L. A. Chekanova, S. V. Komogortsev [et al.] // IEEE International Magnetics Virtual Conference (INTERMAG'21) : Digest book. - 2021. - P. 1342. - Cited References: 2. - This work was funded by the RFBR, the Government of the Krasnoyarsk Territory, the KRFS (project no. 20-43-240003)
   Перевод заглавия: Бисегментированные и ядро-оболочка наностержни Co-Ni , полученные методом химического осаждения

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Доп.точки доступа:
Denisova, E. A.; Денисова, Елена Александровна; Chekanova, L. A.; Чеканова, Лидия Александровна; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Rautskii, M. V.; Рауцкий, Михаил Владимирович; Nemtsev, I. V.; Немцев, Иван Васильевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Tkachev, V. V.; Plotnikov, V. S.; Dolgopolova, M. V.; IEEE International Magnetics Conference(2021 ; Apr. 26-30 ; Lion, France (Virtual))
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    Получение углеродных пленок на сапфире с помощью химического осаждения из газовой фазы и их исcледование / И. А. Харченко, М. М. Симунин, А. В. Лукьяненко, И. И. Рыжков // Решетневские чтения : материалы XXV междунар. науч.-практ. конф. : в 2-х ч. - 2021. - Ч. 1. - С. 674-676. - Библиогр.: 5. - Работа выполнена при финансовой поддержке РФФИ, проект № 18-29-19078 мк. Физико–химический анализ материалов был выполнен в Красноярском региональном центре коллективного пользования ФИЦ КНЦ СО РАН
   Перевод заглавия: Production of carbon films on sapphire using chemical deposition??from the gas phase and their study
Аннотация: Проведено экспериментальное исследование процесса формирование углеродных слоев на сапфировой подложке методом CVD. Представлены результаты, полученные с помощью атомно-силовой микроскопии.

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Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Харченко, И. А.; Симунин, Михаил Максимович; Лукьяненко, Анна Витальевна; Lukyanenko, A. V.; Рыжков, И. И.; "Решетневские чтения", международная научно-практическая конференция(25 ; 2021 ; нояб. ; 10-12 ; Красноярск); Сибирский государственный университет науки и технологий им. акад. М. Ф. Решетнева; Информационные спутниковые системы им. М.Ф. Решетнева, ОАО; "Красноярский машиностроительный завод", ОАО; Федеральный исследовательский центр "Красноярский научный центр Сибирского отделения Российской академии наук"
}
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Phase stability of nanolaminated epitaxial (Cr1-xFex)2AlC MAX phase thin films on MgO(111) and Al2O3(0001) for use as conductive coatings / H. Pazniak, M. Stevens, M. Dahlqvist [et al.] // ACS Appl. Nano Mat. - 2021. - Vol. 4, Is. 12. - P. 13761-13770, DOI 10.1021/acsanm.1c03166. - Cited References: 51. - This work has been supported by the Deutsche Forschungsgemeinschaft (DFG) within CRC/TRR 270, project B02 (Project-ID 405553726). The calculations were carried out using supercomputer resources provided by the Swedish National Infrastructure for Computing (SNIC) at the National Supercomputer Centre (NSC) and the High Performance Computing Center North (HPC2N) partially funded by the Swedish Research Council through grant agreement no. 2018-05973. J.R. acknowledges funding from the Knut and Alice Wallenberg Foundation. Support by the Interdisciplinary Center for Analytics on the Nanoscale (ICAN) of the University of Duisburg-Essen (DFG RIsources reference: RI_00313), a DFG-funded core facility (Project nos. 233512597 and 324659309), is gratefully acknowledged. M.F. acknowledges co-funding by the government of the Russian Federation (agreement no. 075-15-2019-1886) . - ISSN 2574-0970
Кл.слова (ненормированные):
MAX phase -- thin film -- DFT calculations -- pulsed laser deposition -- TEM/EDX -- electrical resistivity
Аннотация: In this study, we model the chemical stability in the (Cr1-xFex)2AlC MAX phase system using density functional theory, predicting its phase stability for 0 ‹ x ‹ 0.2. Following the calculations, we have successfully synthesized nanolaminated (Cr1-xFex)2AlC MAX phase thin films with target Fe contents of x = 0.1 and x = 0.2 by pulsed laser deposition using elemental targets on MgO(111) and Al2O3(0001) substrates at 600 °C. Structural investigations by X-ray diffraction and transmission electron microscopy reveal MAX phase epitaxial films on both substrates with a coexisting (Fe,Cr)5Al8 intermetallic secondary phase. Experiments suggest an actual maximum Fe solubility of 3.4 at %, corresponding to (Cr0.932Fe0.068)2AlC, which is the highest Fe doping level achieved so far in volume materials and thin films. Residual Fe is continuously distributed in the (Fe,Cr)5Al8 intermetallic secondary phase. The incorporation of Fe results in the slight reduction of the c lattice parameter, while the a lattice parameter remains unchanged. The nanolaminated (Cr0.932Fe0.068)2AlC thin films show a metallic behavior and can serve as promising candidates for highly conductive coatings.

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Faculty of Physics, Center for Nanointegration (CENIDE), University of Duisburg-Essen, Duisburg, 47057, Germany
Materials Design, Department of Physics, Chemistry, and Biology (IFM), Linkoping University, Linkoping, SE-581 83, Sweden
Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons (ER-C), Forschungszentrum Julich, Julich, 52425, Germany
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Pazniak, H.; Stevens, M.; Dahlqvist, M.; Zingsem, B.; Kibkalo, L.; Felek, M.; Varnakov, S. N.; Варнаков, Сергей Николаевич; Farle, M.; Фарле, Михаель; Rosen, J.; Wiedwald, U.
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10.

Core-shell and bi-segmented cobalt-nickel nanorods prepared by electroless deposition / E. A. Denisova, L. A. Chekanova, S. V. Komogortsev [et al.] // IEEE Trans. Magn. - 2022. - Vol. 58, Is. 2. - Ст. 2300805, DOI 10.1109/TMAG.2021.3098747. - Cited References: 27. - This work was funded by RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20-43-240003. The authors thank the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center“ Krasnoyarsk Science Center SB RAS” for the provided equipment . - ISSN 0018-9464
Кл.слова (ненормированные):
bi-segmented Co-Ni rods -- core-shell rods -- magnetic properties -- electroless deposition
Аннотация: A porous polymer loaded with segmented nanorods of magnetic metal is very promising for the design of novel microwave devices. Arrays of bi-segmented Ni/Co and core-shell Ni@Co rods were prepared by electroless deposition into porous of polycarbonate track etched membrane. An intrinsic effective magnetic field of the magnetic composite nanorods aligned in the nonmagnetic template was studied by magnetization curves and ferromagnetic resonance. The effect of the interface boundaries for two types of bi-segmented rods with coaxial and along-axis Co/Ni segmentation to effective field was established.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation.
Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation.
Far Eastern Federal University, Vladivostok, 690950, Russian Federation.

Доп.точки доступа:
Denisova, E. A.; Денисова, Елена Александровна; Chekanova, L. A.; Чеканова, Лидия Александровна; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Rautsky, M. V.; Рауцкий, Михаил Владимирович; Nemtsev, I. V.; Немцев, Иван Васильевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Plotnikov, V. S.; Tkachev, V. V.; Li, O. A.; Dolgopolova, M. V.
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