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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vtyurin A. N., Bulou A., Krylov A. S., Shmygol I. V., Aleksandrov K. S.
Заглавие : Raman scattering study of the upper phase transition in CsScF4
Место публикации : Journal of Raman Spectroscopy. - 2000. - Vol. 31, Is. 3. - P.151-155. - ISSN 0377-0486, DOI 10.1002/(SICI)1097-4555(200003)31:3151::AID-JRS5103.0.CO;2-T
Ключевые слова (''Своб.индексиров.''): article--crystal--heating--high temperature--melting point--neutron scattering--phase transition--photon--raman spectrometry--temperature dependence
Аннотация: Effects of the phase transition between the high-temperature tetragonal phases of the CsScF4 crystal were studied by Raman scattering. The appearance of new lines including a soft mode was observed below the phase transition point, in complete accordance with the new crystal symmetry. The behavior of the soft mode, which corresponds to in-phase rotations of ScF6 rigid groups around the z-axis (and out-of-phase within perovskite-like layers), resembles that observed earlier in RbAlF4, which suggests a similar mechanism of this transition in both crystals. Copyright (C) 2000 John Wiley and Sons, Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Averyanov E. M., Adomenas P. V., Zhuikov V. A., Zyryanov V. Ya.
Заглавие : Orientational melting of low chains of molecules and nature of the nematic-smectic A-phase transition
Место публикации : JETP Letters. - 1986. - Vol. 43, Is. 2. - P.117-120. - ISSN 0021-3640
Примечания : Cited References: 13
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : PETRAKOVSKII G. A., SOSNIN V. M., RUDENKO V. V., RYBNIKOVA S. M.
Заглавие : AFMR LINEWIDTH STUDY OF FEBO3 CRYSTALS GROWN FROM SOLUTION-MELTING
Место публикации : Fiz. Tverd. Tela: MEZHDUNARODNAYA KNIGA, 1984. - Vol. 26, Is. 12. - P3720-3722. - ISSN 0367-3294
Примечания : Cited References: 6
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gerasimov V. S., Ershov A. E., Gavrilyuk A. P., Karpov S. V., Agren H., Polyutov S. P.
Заглавие : Suppression of surface plasmon resonance in Au nanoparticles upon transition to the liquid state
Место публикации : Opt. Express: Optical Society of America, 2016. - Vol. 24, Is. 23. - P.26851-26856. - ISSN 10944087 (ISSN), DOI 10.1364/OE.24.026851
Примечания : Cited References: 24. - This work was performed within the State contract of the RF Ministry of Education and Science for Siberian Federal University for scientific research in 2014–2016 (Reference number 1792) and SB RAS Program No II.2P (0358-2015-0010). The numerical calculations were performed using the MVS-1000 M cluster at the Institute of Computational Modeling, Siberian Branch, Russian Academy of Sciences.
Ключевые слова (''Своб.индексиров.''): electron scattering--gold--lattice constants--liquids--melting--metal nanoparticles--nanoparticles--surface plasmon resonance--electron phonon couplings--experimental spectra--experimental values--gold nanoparticles--nonlinear optical response--plasmonic nanoparticle--relaxation constants--surface plasmon frequency--plasmons
Аннотация: Significant suppression of resonant properties of single gold nanoparticles at the surface plasmon frequency during heating and subsequent transition to the liquid state has been demonstrated experimentally and explained for the first time. The results for plasmonic absorption of the nanoparticles have been analyzed by means of Mie theory using experimental values of the optical constants for the liquid and solid metal. The good qualitative agreement between calculated and experimental spectra support the idea that the process of melting is accompanied by an abrupt increase of the relaxation constants, which depends, beside electronphonon coupling, on electron scattering at a rising number of lattice defects in a particle upon growth of its temperature, and subsequent melting as a major cause for the observed plasmonic suppression. It is emphasized that observed effect is fully reversible and may underlie nonlinear optical responses of nanocolloids and composite materials containing plasmonic nanoparticles and their aggregates in conditions of local heating and in general, manifest itself in a wide range of plasmonics phenomena associated with strong heating of nanoparticles. © 2016 Optical Society of America.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ershov A. E., Gerasimov R.E., Rasskazov I. L., Zakomirnyi V. I., Gavrilyuk A.P., Karpov S. V., Polyutov S. P.
Заглавие : Surface plasmon resonance of Au nanoparticles in the vicinity of the melting temperature
Коллективы : International Conference on Coherent and Nonlinear Optics, International Conference on Lasers, Applications, and Technologies
Место публикации : The International Conference on Coherent and Nonlinear Optics; The Lasers, Applications, and Technologies ICONO/LAT 2016. - 2016. - Ст.IThL13. - P.77-78
Аннотация: We have demonstrated experimentally the significant suppression of resonant properties of single Au nanoparticles at the surface plasmon frequency during heating and subsequent transition to the liquid state.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gerasimov V. S., Ershov A. E., Rasskazov I. L., Zakomirnyi V. I., Gavrilyuk A. P., Karpov S. V., Polyutov S. P.
Заглавие : Surface plasmon resonance of aU nanoparticles in the vicinity of the melting temperature
Коллективы : International Conference on Coherent and Nonlinear Optics, International Conference on Lasers, Applications, and Technologies
Место публикации : Журнал прикладной спектроскопии. - 2016. - Т. 83, Вып. 6-16. - P.103-104. - ISSN 0514-7506
Аннотация: We have demonstrated experimentally the significant suppression of resonant propertiesof single Au nanoparticles at thesurface plasmonfrequency during heating and subsequent transition to the liquid state.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Azarapin N. O., Atuchin V. V., Maximov N. G., Aleksandrovsky A. S., Molokeev M. S., Oreshonkov A. S., Shestakov N. P., Krylov A. S., Burkhanova T. M., Mukherjee S., Andreev O. V.
Заглавие : Synthesis, structure, melting and optical properties of three complex orthorhombic sulfides BaDyCuS3, BaHoCuS3 and BaYbCuS3
Место публикации : Mater. Res. Bull. - 2021. - Vol. 140. - Ст.111314. - ISSN 00255408 (ISSN), DOI 10.1016/j.materresbull.2021.111314
Примечания : Cited References: 60. - This study was supported by the Russian Science Foundation (19-42-02003). The authors would like to thank Alexey A. Lubin for his studies on SEM. The studies were carried out on the basis of laboratory of electron and probe microscopy in REC ‘Nanotechnologies’. This work was partially supported by the DST-RSF project under the India-Russia Programme of Cooperation in Science and Technology (No. DST/ INT/RUS/RSF/P-20 dated May 16, 2019). Shaibal Mukherjee would like to thank MeitY for the YFRF under the Visvesvaraya Ph.D. Scheme for Electronics and IT. This publication is an outcome of the R&D work undertaken in the project under the Visvesvaraya Ph.D. Scheme of MeitY being implemented by Digital India Corporation (formerly Media Lab Asia). We are grateful to the Krasnoyarsk Regional Center of Research Equipment of the Federal Research Center «Krasnoyarsk Science Center SB RAS» for the provided equipment
Аннотация: Complex sulfides BaDyCuS3, BaHoCuS3 and BaYbCuS3 were synthesized in a flow of sulfiding gases (CS2, H2S) at 900°C from standard solutions of lanthanide and copper nitrates, as well as from the same standard Ba(OH)2 solution. The crystal structures of BaDyCuS3, BaHoCuS3 and BaYbCuS3 were obtained by the Rietveld refinement method. All three compounds crystallize in the Cmcm space group (KZrCuS3 structural type) as predicted by the tolerance factor analysis. Their micromorphological, thermal and spectroscopic properties are evaluated. BaDyCuS3 and BaHoCuS3 melt congruently at 1376.5 °C and 1363.8 °C. BaYbCuS3 melts incongruently at 1353.3 °C. The optical band gap is 2.45 eV for BaDyCuS3, 2.37 eV for BaHoCuS3 and 1.82 eV for BaYbCuS3. The low bandgap of BaYbCuS3 is explained by the charge transfer band of Yb at the bottom of conduction band. The vibrational parameters of BaDyCuS3, BaHoCuS3 and BaYbCuS3 crystals were determined with the use of Raman and Infrared spectroscopies.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Morozov E. V., Martyanov O.N., Volkov N. V., Falaleev O. V.
Заглавие : NMR Imaging of Heavy Crude Oil for Softening Detection under Heat Treatment
Место публикации : Journal of Materials Science and Engineering. - 2011. - Т. 1, № 4. - С. 545-551. - ISSN 2161-6213. - ISSN 2161-6221(eissn)
Ключевые слова (''Своб.индексиров.''): mongolian heavy crude oil--nmr imaging--oil softening--melting front--oil heat treatment
Аннотация: NMR Imaging results of Mongolian heavy crude oil samples subjected to heat treatment are presented in this work. Abundance of dotted inhomogeneities related with high paraffinicity of heavy oil was obtained during imaging investigation. Behavior of heavy oil subjected to heat treatment, dotted inhomogeneities changes, softening and dynamic of melting front were visualized by means of imaging techniques based on both gradient and spin echo. Softening forestalling over the melting front are demonstrated using artificial mark in the form of water drop deposited on the oil surface. In results the NMR imaging proved to be highly effective for ?investigation of impurity agglomerates in heavy oil and it is perspective for heavy oil engineering development. ?
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Morozov E. V., Voronin A. S., Kniga, S., V, Buznik V. M.
Заглавие : Nuclear magnetic resonance study of ice-based composite materials reinforced with nanodisperse aluminum oxide fibers
Коллективы : Institute of Chemistry and Chemical Technology (Siberian Branch, Russian Academy of Sciences) [0287-2021-0012]; Russian Science FoundationRussian Science Foundation (RSF) [18-1300392]
Место публикации : Inorg. Mater. Appl. Res. - 2022. - Vol. 13, Is. 1. - P.217-224. - ISSN 2075-1133, DOI 10.1134/S2075113322010270. - ISSN 2075-115X(eISSN)
Примечания : Cited References: 21. - This work was performed within the scope of state contract no. 0287-2021-0012 of the Institute of Chemistry and Chemical Technology (Siberian Branch, Russian Academy of Sciences) in the part of developing the MRI methods for studying composite materials; also the work was supported by the Russian Science Foundation (project no. 18-1300392) in the part of the study of the processes of water crystallization and ice melting in ice-based composite materials
Предметные рубрики: SELF-DIFFUSION
WATER
Аннотация: Pulsed-field gradient NMR spectroscopy and magnetic resonance imaging methods were used to investigate water suspensions of nanosized fibers of aluminum oxide and ice composite materials based on these fibers. Introduction of the nanofibers was shown to have no noticeable structural effect in the suspensions in the Al2O3 concentration range of 1-10 wt %. High content of the filler was found to change the morphology and texture of the ice matrix in the composites remarkably: it becomes more homogeneous and acquires a higher degree of continuity; the melting front does not visualize internal melting zones or integrity defects in the composite. At the same time, addition of the nanofibers to the ice composites weakly influences the quantitative dynamics of the heat transfer, which is manifested in close values of the propagation speeds of the freezing/melting front in the samples at similar temperatures.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Osseni S. А., Andreev P. O., Polkovnikov A. A., Zakharov B. A., Aleksandrovsky A. S., Abulkhaev M. U., Volkova S. S., Kamaev D. N., Kovenskiy I. M., Nesterova N. V., Kudomanov M. V., Andreev O. V.
Заглавие : Properties of oxysulfide phases and phase diagram of the Nd2S3–Nd2O3 system
Место публикации : J. Solid State Chem. - 2022. - Vol. 314. - Ст.123438. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2022.123438
Примечания : Cited References: 51. - This research was funded by the Tyumen Oblast Government , as part of the West-Siberian Interregional Science and Education Center's project No. 89-DON (3)
Аннотация: We have determined the thermal characteristics and optical properties of the sulfide and oxysulfide phases in the Nd2S3 - Nd2O3 system. A congruent melting peak at temperature 1801 ± 4.9 °C with ΔH = 65.2 ± 6.7 kJ/mol was detected for the Nd2S3 compound by the DSC method. The characteristics of the α-Nd2S3 → γ-Nd2S3 polymorphic transition are t = 1183 ± 1.8°С, and ΔH = 7.5 ± 0.3 kJ/mol. The γ-Nd2S3 phase obtained upon cooling during annealing at 800 °C is retained for up to 30 h, and then the γ-Nd2S3 → α-Nd2S3 transition occurs within 20 h. The microhardness of the phases is: α-Nd2S3 H = 451 ± 4 HV; γ-Nd2S3 H = 531 ± 4 HV. It was found by the TG method that the Nd10S14O phase thermally dissociates at temperatures above 1400 °C. The mass loss is 0.5 mass % at 1580 °C and 1.0 mass % at 1620 °C, but the samples remain single-phase ones after cooling. However, two impurity phases γ-Nd2S3-X and Nd2O2S appear in the Nd10S14O samples treated at temperatures above 1620 ± 20 °C. For samples of the Nd10S14O phase annealed in an argon atmosphere at temperatures of 1050, 1400, 1580 °C, a regular decrease in the unit cell parameters and optical band gap was recorded: 1050 °C a = 15.06291(28), c = 19.97864(35), Eg = 2, 63 eV, 1400 °C a = 15.04779(36), c = 19.97160(44), Eg = 2.64 eV; 1580 °C a = 15.03532(48), c = 19.94984(60), Eg = 2.51 eV. The microhardness of Nd10S14O is H = 549 ± 10 HV. The Nd2O2S phase has H = 593 ± 4 HV, Eg = 4.28 eV. The phase diagram of the Nd2S3 - Nd2O3 system from 1000 °C to the melt was constructed. The Nd2O2S phase melts congruently at 2050 ± 30 °C. Eutectics with coordinates 23 mol. % Nd2O3 (0.3484 Nd10S14O + 0.6516 Nd2O2S), t = 1553 ± 1.8°С; ΔH = 187 ± 19 J/g; 82 mol. % Nd2O3; (0.54 Nd2O2S + 0.46 Nd2O3), t = 1970 ± 30°С were obtained. The liquidus of the Nd2S3 - Nd2O3 system was built according to DSC data and calculated using the Redlich-Kister equation. The melting enthalpy of Nd2O2S ΔH = 67 kJ/mol was calculated using the Schroeder equation.
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