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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Denisova E. A., Nemtsev I. V., Telegin S. V., Iskhakov R. S., Kuzovnikova L. A., Shepeta N. A.
Заглавие : Microstructure and magnetic properties of Co58Ni10Fe5B16Si11 and Co58Ni10Fe5B16Si11-Al2O3 bulk amorphous coatings prepared by plasma spraying
Коллективы : International Conference on High-Tech and Innovations in Research and Manufacturing
Место публикации : J. Phys.: Conf. Ser. - 2020. - Vol. 1582, Is. 1. - Ст.012078. - DOI 10.1088/1742-6596/1582/1/012078
Примечания : Cited References: 18. - This work was funded by the Russian Foundation for Basic Research, the Government of the Krasnoyarsk Territory, the Krasnoyarsk Regional Fund for the Support of Scientific and Technical Activities (project no. 18-42-240006 Nanomaterials with magnetic properties determined by the topological features of the nanostructure). The authors thank the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” for the provided equipment
Аннотация: The bulk soft magnetic glassy Co58Ni10Fe5B16Si11 alloy specimens have been prepared by plasma spray deposition. In order to increase resistivity of the material, the bulk Co58Ni10Fe5B16Si11-Al2O3 composite materials were fabricated. The investigations of structure and magnetic properties of the bulk samples were carried out by X-ray diffraction, electron microscopy and magnetic measurements. The relation of the structural features and magnetic characteristics of the bulk coating to the main parameters of the deposition regimes was determined. Optimized plasma spray deposition parameters allowed obtaining bulk glassy samples with magnetic parameters that are not inferior to the characteristics of a thermally treated rapidly quenched ribbon with the same composition. It was found that the bulk amorphous coatings can be characterized as a heterophase system. The relaxation annealing of the Co58Ni10Fe5B16Si11 bulk coating leads to a phase transition in this alloy in the precrystallization temperature range. The magnetic properties of the both kinds of coatings are correlated with changes in the microstructure. The appearance of nanocrystalline phase with TC640 K during relaxation heat treatment leads to a decrease of the coercivity and to an increase of the permeability. A comparison between the magnetic properties of the CoNiFe-BSi coating and (CoNiFe-BSi)-Al2O3, composite coating is carried out.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gordienko A. I., Derevyagina L. S., Malikov A. G., Orishich A. M., Surikova N. S., Volochaev M. N.
Заглавие : The effect of the initial microstructure of the X70 low-carbon microalloyed steel on the heat affected zone formation and the mechanical properties of laser welded joints
Место публикации : Mater. Sci. Eng. A. - 2020. - Vol. 797. - Ст.140075. - ISSN 09215093 (ISSN), DOI 10.1016/j.msea.2020.140075
Примечания : Cited References: 32. - Microstructural studies and mechanical tests of laser welds were performed within the frame of the Fundamental Research Program of the State Academies of Sciences for 2013?2020, line of research III.23.1.1. Part of the research related to the selection of optimal laser welding parameters for low carbon steels was carried out within Basic State Project No. AAAA-A17-117030610122-6. TEM studies were carried out in Center of Federal Research Center of Kirensky Institute of Physics SB RAS. The authors are grateful to I.P. Mishin. for assistance in cross-helical rolling of the steel
Аннотация: In this paper, the heat affected zone (HAZ) of laser welded joints of the X70 steel were studied by the transmission electron microscopy method. The effect of the initial microstructure (coarse-grained hot-rolled and fine-grained after cross-helical rolling) on the HAZ formation and the mechanical characteristics of the welded joints were shown. It was found that the microstructure in the inter-critical HAZ of the steel after cross-helical rolling was more dispersed, homogeneous, and uniform compared to that of the coarse-grained hot-rolled one due to the initial fine-grained ferrite-bainitic-pearlite microstructure and the absence of pronounced ferrite-pearlite banding in the base metal. The character of the microhardness value distribution in the HAZ of the steel after cross-helical rolling was smooth with the gradual decrease from 370 down to 185 HV as shifted towards the base metal. In the HAZ of the coarse-grained hot-rolled steel, the heterogeneous microhardness value (up to 640–670 НV) distribution was revealed. The reason was the upper degenerate bainite microstructure with high residual stresses, characterized by laths up to 2.0–2.5 μm long and a high martensitic-austenitic constituent fraction (10–16%) of a slender shape along the boundaries of bainite laths. The conclusion was drawn that one of the ways to reduce the brittleness of the laser welded joints could be using the initially fine-grained steels possessing the homogeneous (mainly bainitic) microstructure.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Podorozhnyak, Sergey A., Chzhant, Anatoly, V, Maltsevt, Vadim K., Krayuhin, Ivan N., Patrin G. S., Sakash, Irina Yu
Заглавие : Structural changes of Co caused a change of the solution pH during chemical deposition
Место публикации : J. Sib. Fed. Univ. Math. Phys. - 2020. - Vol. 13, Is. 4. - P.451-458. - ISSN 1997-1397, DOI 10.17516/1997-1397-2020-13-4-451-458; Журн. СФУ. Матем. и физика. - ISSN 2313-6022(eISSN)
Примечания : Cited References: 10
Предметные рубрики: COBALT
MICROSTRUCTURE
Аннотация: The phase transformations of the Co lattice are discussed, which determine the anomalous changes in the magnetic properties of chemically deposited Co-P films obtained at various pH values. The coercivity of the H-c films obtained at low pH values exceeds 1 kOe and decreases to several units Oe in the films obtained at high pH values. It is shown that the observed changes in the magnetic properties of Co-P films are caused by the transition of the cobalt crystal lattice to the nanocrystalline state.Обсуждаются фазовые превращения решетки Co, которые определяют аномальные изменения магнитных свойств химически осажденных пленок Co-P, полученных при различных значениях pH. Коэрцитивная сила пленок, полученных при низких значениях pH, превышает 1 кЭ и снижается до нескольких единиц Э в пленках, полученных при высоких значениях pH. Показано, что наблюдаемые изменения магнитных свойств пленок Co-P вызваны переходом кристаллической решетки кобальта в нанокристаллическое состояние.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Timofeeva E. E., Panchenko E. Yu., Eftifeeva A. S., Yanushonite E. I., Zherdeva M. V., Chumlyakov Yu. I., Volochaev M. N.
Заглавие : The effect of high-temperature and high-stress martensite aging on martensitic transformation and microstructure of Ti-51.5 at % Ni single crystals
Коллективы : International Conference on Physical Mesomechanics. Materials with Multilevel Hierarchical Structure and Intelligent Manufacturing Technology 2020
Место публикации : AIP Conf. Proc. - 2020. - Vol. 2310. - Ст.020336. - DOI 10.1063/5.0034595
Примечания : Cited References: 9. - The study was supported by the Russian Science Foundation (grant No. 18-19-00298)
Аннотация: In this work, the thermomechanical stability of heterophase [001]-oriented Ti–51.5 at % Ni single crystals was investigated. Experiments include a high-temperature and high-stress martensite ageing and also loading/unloading cycling at superelasticity (SE) during forward and reverse B2-B19′ martensitic transformations (MT). It was found that Ti–51.5 at % Ni single crystals containing large Ti3Ni4 particles (d ∼ 600 nm after ageing at 850 K for 1 h) is not resistant to stress-assisted martensite ageing and cycling. Stress-assisted martensite ageing at 423 K, 1.7–2 GPa, for 2–4 h leads to the deformation of large Ti3Ni4 particles, the appearance of dislocations at the particle-matrix boundaries, an increase in MT temperatures (by 10 K), and a strong diffusion of the MT (the intervals of forward and reverse MT Δσ1 and Δσ2 increase in 2 times). During loading/unloading cycling at 423 K and 1.0–2.0 GPa single crystals with large particles were destroyed after 20–25 cycles. It is possible to increase the thermomechanical stability due to the additional precipitation of nanosized Ti3Ni4 particles (d‹30 nm by ageing at 673 K, 1 h), which appear in the B2 matrix between large particles. In such crystals with a bimodal structure no changes in the microstructure and functional properties were observed after stress-assisted martensite ageing and loading/unloading cycling.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Derevyagina L. S., Gordienko A. I., Surikova N. S., Volochaev M. N.
Заглавие : Effect of helical rolling on the bainitic microstructure and impact toughness of the low-carbon microalloyed steel
Место публикации : Mater. Sci. Eng. A. - 2021. - Vol. 816. - Ст.141275. - ISSN 09215093 (ISSN), DOI 10.1016/j.msea.2021.141275
Примечания : Cited References: 43
Аннотация: Ferrite-bainite microstructures and impact toughness of the X65 low-carbon microalloyed steel were investigated after helical rolling at 1000, 920, 850, and 810 °C followed by continuous cooling in air. After helical rolling at 1000 °C, granular bainite with large areas of the massive-shape martensite-austenite constituent (d = 1.5 μm) and a high fraction of twinned martensite (d › 2.0 μm) were observed in the steel. This caused a decrease in impact energy at low test temperatures (for example, 70 J at –70°С). Lowering the helical rolling temperature contributed to a reduction of dimensions of both ferrite-bainite and martensite-austenite constituent areas, as well as the replacement of the latter by a slender type one and an improvement in fracture toughness at the low temperatures. The highest impact energy level (210 J at –70 °C) was achieved after helical rolling at 850 °C due to the formation of a homogeneous microstructure, which included dispersed ferrite grains, granular bainite and small fractions of the slender type martensite-austenite constituent (d = 0.1–0.7 μm). In this case, areas of twinned martensite were absent.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volova T., Kiselev E., Nemtsev I. V., Lukyanenko A. V., Sukovatyi A., Kuzmin A., Ryltseva G., Shishatskaya E.
Заглавие : Properties of degradable polyhydroxyalkanoates with different monomer compositions
Место публикации : Int. J. Biol. Macromol. - 2021. - Vol. 182. - P.98-114. - ISSN 01418130 (ISSN), DOI 10.1016/j.ijbiomac.2021.04.008
Примечания : Cited References: 109. - The part of the reported study on polymer synthesis and examination was funded by RFBR and KKRF [Grant No. 19-43-240012 “Biological and physical principles of production of new generation biomaterials”]. The work on production and investigation of polymer films was carried out as part of the State Assignment of the Ministry of Education and Science of the Russian Federation [Grant No. FSRZ-2020-0006]
Аннотация: Purpose: To synthesize and investigate polyhydroxyalkanoates (PHAs) with different monomer composition and percentages and polymer films prepared from them. Results: Various PHAs: homopolymer poly-3-hydroxybutyrate P(3HB) and 2-, 3-, and 4-component copolymers comprising various combinations of 3-hydroxybutyrate (3HB), 3-hydroxyvalerate (3HV), 4-hydroxybutyrate (4HB), and 3-hydroxyhexanoate (3HHx) monomers were synthesized under specialized conditions. Relationships were found between the monomer composition of PHAs and their molecular-weight and thermal properties and degree of crystallinity. All copolymers had decreased weight average molecular weights, Mw (to 390–600 kDa), and increased values of polydispersity (3.2–4.6) compared to the P(3HB). PHA copolymers showed different thermal behavior: an insignificant decrease in Tmelt and the presence of the second peak in the melting region and changes in parameters of crystallization and glass transition. At the same time, they retained thermostability, and the difference between Tmelt and Tdegr was at least 100–120 °C. Incorporation of 4HB, 3HV, and 3HHx monomer units into the 3-hydroxybutyrate chain caused changes in the amorphous to crystalline ratio and decreased the degree of crystallinity (Cx) to 20–40%. According to the degree to which the monomers reduced crystallinity, they were ranked as follows: 4HB – 3HHx – 3HV. A unique set of films was produced; their surface properties and physical/mechanical properties were studied as dependent on PHA composition; monomers other than 3-hydroxybutyrate were found to enhance hydrophilicity, surface development, and elasticity of polymer films. Conclusion: An innovative set of PHA copolymers was synthesized and solution-cast films were prepared from them; the copolymers and films were investigated as dependent on polymer chemical composition. Results obtained in the present study contribute to the solution of a critical issue of producing degradable polymer materials.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Izotov A. V., Belyaev B. A., Solovev P. N., Boev N. M.
Заглавие : Grain-size dependence of magnetic microstructure and high-frequency susceptibility of nanocrystalline thin films: A micromagnetic simulation study
Место публикации : J. Magn. Magn. Mater. - 2021. - Vol. 529. - Ст.167856. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2021.167856
Примечания : Cited References: 73. - The reported study was funded by RFBR, the Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund and JSC «NPP «Radiosviaz», project number 20-42-242901
Аннотация: The size of crystallites is one of the most important factors that determine the key characteristics of nanocrystalline thin magnetic films that make them very promising media for various applications. In this paper, using micromagnetic simulation, we study in detail the influence of the grain size on the magnetic microstructure of the films and its relation with high-frequency dynamics of magnetization. When the grain size exceeds some critical value Dcr, a sharp broadening and shift of the ferromagnetic resonance line are observed at certain frequencies of the alternating magnetic field. Using a two-magnon scattering model, it is shown that these effects are caused by the scattering of spin waves on the inhomogeneous stochastic magnetic structure—magnetization ripple. An expression for the determination of the critical size Dcr is obtained. The micromagnetic simulation results agree with the main conclusions of the static and dynamic theories of magnetization ripple and also confirmed by experimental data reported by other authors.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sazonov A. M., Silyanov S. A., Bayukov O. A., Knyazev Yu. V., Zvyagina Y. A., Tishin P. A.
Заглавие : Composition and Ligand Microstructure of Arsenopyrite from Gold Ore Deposits of the Yenisei Ridge (Eastern Siberia, Russia)
Место публикации : Minerals. - 2019. - Vol. 9, Is. 12. - Ст.737. - ISSN 2075-163X, DOI 10.3390/min9120737
Примечания : Cited References: 62. - The work was supported by the Russian Foundation for Basic Research (project number 19-35-90017) and the Government of the Russian Federation (project 14.Y26.31.0012).
Аннотация: The Mössbauer spectroscopy method was used to study the ligand microstructure of natural arsenopyrite (31 specimens) from the ores of the major gold deposits of the Yenisei Ridge (Eastern Siberia, Russia). Arsenopyrite and native gold are paragenetic minerals in the ore; meanwhile, arsenopyrite is frequently a gold carrier. We detected iron positions with variable distribution of sulfur and arsenic anions at the vertexes of the coordination octahedron {6S}, {5S1As}, {4S2As}, {3S3As}, {2S4As}, {1S5As}, {6As} in the mineral structure. Iron atoms with reduced local symmetry in tetrahedral cavities, as well as iron in the high-spin condition with a high local symmetry of the first coordination sphere, were identified. The configuration {3S3As} typical for the stoichiometric arsenopyrite is the most occupied. The occupation degree of other configurations is not subordinated to the statistic distribution and varies within a wide range. The presence of configurations {6S}, {3S3As}, {6As} and their variable occupation degree indicate that natural arsenopyrites are solid pyrite {6S}, arsenopyrite {3S3As}, and loellingite {6As} solutions, with the thermodynamic preference to the formation of configurations in the arsenopyrite–pyrite–loellingite order. It is assumed that in the variations as part of the coordination octahedron, the iron output to the tetrahedral positions and the presence of high-spin Fe cations depend on the physical and chemical conditions of the mineral formation. It was identified that the increased gold concentrations are typical for arsenopyrites with an elevated content of sulfur or arsenic and correlate with the increase of the occupation degree of configurations {5S1As}, {4S2As}, {1S5As}, reduction of the share of {3S3As}, and the amount of iron in tetrahedral cavities.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Денисова, Елена Александровна, Комогорцев, Сергей Викторович, Исхаков, Рауф Садыкович, Немцев, Иван Васильевич, Кузовникова, Людмила Александровна, Телегин С. В., Юркин, Глеб Юрьевич, Шепета, Наталья Александровна
Заглавие : Объемные аморфные композиционные покрытия Co58Ni10Fe5B16Si11-Al2O3 , Co58Ni10Fe5B16Si11-ZrO2: микроструктура и магнитные свойства
Коллективы : Байкальская международная конференция "Магнитные материалы. Новые технологии", "Магнитные материалы. Новые технологии", Байкальская международная конференция, "Magnetic materials. New tecnologies", Baikal International Conference, Иркутский государственный университет
Место публикации : Магнитные материалы. Новые технологии: тез. докл. VIII Байкал. междунар. конф. BICMM-2018/ чл. прогр. ком. R. S. Iskhakov [et al.]. - Иркутск, 2018. - С. 107-108. - ISBN 978-5-00133-051-6
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zeer G. M., Zelenkova E. G., Nikolaeva N. S., Zharkov S. M., Abkaryan A. K., Mikheev A. A.
Заглавие : Microstructure and phase composition of the two-phase ceramic synthesized from titanium oxide and zinc oxide
Место публикации : Sci. Sinter. - 2018. - Vol. 50, Is. 2. - P.173-181. - ISSN 0350820X (ISSN), DOI 10.2298/SOS1802173Z
Примечания : Cited References: 22
Ключевые слова (''Своб.индексиров.''): nanopowders--titanium oxide--zinc oxide--solid phase reaction--ceramic
Аннотация: We have made investigations of the phase formation and microstructure on the ceramics obtained from a starting nanopowder mixture with the weight ratio ZnO : TiO2 = 4 : 1. Ceramic is obtained at different sintering temperatures, namely, 948, 1223 and 1473 К. Using the characterization methods of electron microscopy, energy dispersive microanalysis and X-ray diffraction phase analysis it has been shown that the ceramics structure is consisted of two dispersed phases of Zn2TiO4 and ZnO with the grain sizes being in range 0,5-1 μm. It has been found also that, at ceramic`s sintering temperature of 1223 К, the solid phase interactions are completed with the structure ZnO : Zn2TiO4 ≈ 1 : 1,5 phase ratio.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bocharov G. S., Eletskii A. V., Zilova O. S., Terentyev E. V., Fedorovich S. D., Chudina O. V., Churilov G. N.
Заглавие : Mechanism of surface reinforcement of steels by nanocarbon materials using laser heating
Коллективы : Russian Science Foundation [16-19-10027]
Место публикации : Phys. Metals Metallogr. - 2018. - Vol. 119, Is. 2. - P.197-201. - ISSN 0031-918X, DOI 10.1134/S0031918X18010052. - ISSN 1555-6190(eISSN)
Примечания : Cited References:11. - This work was supported by the Russian Science Foundation, project no. 16-19-10027.
Ключевые слова (''Своб.индексиров.''): laser treatment--nanocarbon materials--technically pure iron--microhardness--microstructure--wear resistance--friction coefficient
Аннотация: The mechanism of the surface reinforcement and wear resistance of steel products are studied as a result of creating the strengthening layers with the nanocarbon using the laser heating. Laser surface treatment using soot remaining after fullerene extraction leads to a more than fivefold increase in the microhardness (up to 1086 HV) and a decrease in the friction coefficient by 20–30%. The conclusion that the reinforcement mechanism involves the formation of eutectic, cementite, martensite, the cellular substructure, and grain refinement is carried out based on metallographic studies of the strengthened layers of technically pure iron with a thickness of 20–70 μm.
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12.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Денисова, Елена Александровна, Чеканова, Лидия Александровна, Комогорцев, Сергей Викторович, Исхаков, Рауф Садыкович, Немцев, Иван Васильевич, Шепета, Наталья Александровна, Кузовникова, Людмила Александровна
Заглавие : Микроструктура и магнитные свойства нитей на основе 3-d металлов с градиентом концентрации элементов
Коллективы : Байкальская международная конференция "Магнитные материалы. Новые технологии", "Магнитные материалы. Новые технологии", Байкальская международная конференция, "Magnetic materials. New tecnologies", Baikal International Conference, Иркутский государственный университет
Место публикации : Магнитные материалы. Новые технологии: тез. докл. VIII Байкал. междунар. конф. BICMM-2018/ чл. прогр. ком. R. S. Iskhakov [et al.]. - Иркутск, 2018. - С. 115. - ISBN 978-5-00133-051-6
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Лепешев, Анатолий Александрович, Павлов А. В., Дрокин, Николай Александрович
Заглавие : Импедансная спектроскопия (ВеО+TiO2)-керамики с добавкой наночастиц TiO2 : статья
Место публикации : Журнал СФУ. Техн. и технол. - 2019. - Т. 12, № 3. - С. 366-380. - ISSN 1999-494X, DOI 10.17516/1999-494X-0144; J. Sib. Fed. Univ. Eng. Technol.
Примечания : Библиогр.: 23
Аннотация: Настоящее исследование направлено на получение электропроводной двухкомпонентной керамики на основе ВеО с добавками микро- и нанокристаллического порошка TiO2. Керамика состава (BeO+TiO2) находит применение в радиоэлектронной технике в качестве эффективных поглотителей СВЧ-излучения и в других областях современной электроники. Природа возникновения электрической проводимости и поглощения СВЧ-поля в (ВеО+TiO2)керамике окончательно не установлена. Методом импедансной спектроскопии впервые исследованы электрические и диэлектрические характеристики данной керамики в диапазоне частот от 100 Hz до 100 МHz в зависимости от присутствия в составе керамики ВеО микро- и наноразмерной фазы TiO2. Установлено, что статическое сопротивление керамики с добавкой нанопорошка оксида титана существенно уменьшается по сравнению с сопротивлением исходной керамики с микропорошком TiO2. Показано, что действительная и мнимая компоненты диэлектрической проницаемости исследуемых керамик возрастают до аномально больших величин при понижении частоты действующего электрического поля, а в области высоких частот f ≥ 10 8 Hz начинается процесс диэлектрической релаксации, приводящий к росту тангенса угла диэлектрических потерь. Определены диэлектрические характеристики данных образцов керамик в условиях блокирования сквозной проводимости.The present study is aimed at obtaining electrically conductive two-component ceramics based on BeO with the addition of micro and nanocrystalline TiO2 powder. The ceramics of the composition (BeO+TiO2) is used in radio-electronic equipment as effective absorbers of microwave radiation and in other areas of modern electronics. The nature of the appearance of electrical conductivity and absorption of the microwave field in (BeO+TiO2) ceramics has not been completely established. The impedance spectroscopy method for the first time investigated the electrical and dielectric characteristics of this ceramics in the frequency range from 100 Hz to 100 MHz, depending on the presence of micro and nano-sized TiO2 phases in the composition of the BeO ceramics. It was established that the static resistance of ceramics with the addition of titanium oxide nanopowder is significantly reduced compared with the resistance of the original ceramics with TiO2 micropowder. It is shown that the real and imaginary components of the dielectric constant of the studied ceramics increase to abnormally large values when the frequency of the effective electric field decreases, and in the high frequency range f ≥ 10 8 Hz, the process of dielectric relaxation begins, leading to an increase in the dielectric loss tangent. The dielectric characteristics of these ceramic samples under conditions of blocking through conduction are determined.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Derevyagina L. S., Gordienko A. I., Orishich A. G., Malikov N. S., Surikova M. N., Volochaev M. N.
Заглавие : Microstructure of intercritical heat affected zone and toughness of microalloyed steel laser welds
Место публикации : Mater. Sci. Eng. A. - 2020. - Vol. 770. - Ст.138522. - ISSN 09215093 (ISSN), DOI 10.1016/j.msea.2019.138522
Примечания : Cited References: 28
Аннотация: Microstructure of laser welds of the X70 low-carbon pipe steel was studied. High cooling rates after laser welding and non-uniform distribution of carbon in the ferrite-pearlite base metal caused formation of regions with increased microhardness (up to 650 НV) in inter-critical heat affected zone (ICHAZ). These regions consisted of finely dispersed degenerate upper bainite and martensite-austenite constituents of a slender shape and small fraction of a massive shape along the boundaries of bainite laths, as well as twinned martensite. High concentration of martensite-austenite constituents (10–16%) and residual stresses in ICHAZ, as well as a dendritic martensitic structure with carbide interlayers along the boundaries of martensite laths in fusion zone were the main reasons of sharp decrease in charpy impact energy of the welded samples. High microhardness of the laser welds was decreased down to 320 HV and their brittleness was improved by annealing. Also, in ICHAZ, degenerate upper bainite and the regions of martensite-austenite constituents decayed forming tempered sorbite and Fe2C and Fe3C carbides, respectively. Charpy impact energy of the welds doubled after annealing compared to the welds without annealing, and ductile-brittle transition temperature decreased down to –60°С.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Platunov M. S., Kazak N. V., Dudnikov V. A., Temerov V. L., Gudim I. A., Knyazev Yu. V., Gavrilkin S. Yu., Dyadkin, Vadim, Dovgaliuk, Iurii, Chernyshov, Dmitry, Hen, Amir, Wilhelm, Fabrice, Rogalev, Andrei, Ovchinnikov S. G.
Заглавие : Element selective magnetism in Ho0.5Nd0.5Fe3(BO3)4 single crystal probed with hard X-ray magnetic circular dichroism
Коллективы : Russian Foundation for Basic Research [16-32-60049, 17-02-00826, 18-42-243007]; Foundation for Assistance to Small Innovative Enterprises (FASIE, UMNIK program)
Место публикации : J. Magn. Magn. Mater. - 2019. - Vol. 479. - P.312-316. - ISSN 0304-8853, DOI 10.1016/j.jmmm.2019.02.040. - ISSN 1873-4766(eISSN)
Примечания : Cited References: 40. - The study was supported in part by the grants of the Russian Foundation for Basic Research (project Nos. 16-32-60049, 17-02-00826, 18-42-243007) and the Foundation for Assistance to Small Innovative Enterprises (FASIE, UMNIK program). The magnetic measurements were carried out in the Shared Facility Centre of P.N. Lebedev Physical Institute of RAS. We are grateful to Dr. Alexey Bosak for providing assistance of the structural experiments on the ID28 beamline. We are also grateful to Dr. Evgeniy Eremin from Kirensky Institute of Physics for providing the results of magnetic measurements and for useful discussions. The authors thank the ID12 beamline staffs for help during the XMCD experiment and also gratefully acknowledge the beamtime provision (proposal HC-1804) by the ESRF.
Предметные рубрики: MICROSTRUCTURE
TRANSITIONS
ND
Ключевые слова (''Своб.индексиров.''): x-ray magnetic circular dichroism--x-ray absorption--magnetic properties
Аннотация: We present a study of a Ho0.5Nd0.5Fe3(BO3)4 single crystal aiming at understanding the roles of each magnetic sublattices in magnetic transitions at low temperatures. The crystal structure is determined to have the R32 symmetry in whole studied temperature range but the crystal appears to be racemic. Element selective magnetic properties studied with X-ray magnetic circular dichroism at the L2,3-edges of Ho and Nd, and at the Fe K-edge at T = 3 K under magnetic fields of ±17 T are compared with the results of macroscopic magnetization measurements in pure and substituted crystals. All three magnetic sublattices are shown to be strongly coupled and to undergo a spin-reorientation transition when magnetic field is applied along the trigonal c-axis. On the contrary, when magnetic field is applied in the ab-plane only the holmium atoms exhibit a sizeable magnetization jump. This result allows us to conclude that the spin-flop transitions observed in macroscopic magnetization curves and associated anomalies of electric polarization are due to the Ho3+ magnetic moment reorientation.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volkova I. R., Tyryshkina L. E., Volochaev M. N., Zaloga A. N., Shabanova K. A., Ovchinnikov A. V., Lyamkin A. I.
Заглавие : The effect of aluminum-oxide powders on the structure and properties of copper electrodeposited composite coatings
Место публикации : Prot. Met. Phys. Chem. Surf. - 2023. - Vol. 59, Is. 1. - P.71-75. - ISSN 20702051 (ISSN), DOI 10.1134/S2070205122700022. - ISSN 2070206X (eISSN)
Примечания : Cited References: 9
Аннотация: Copper electrodeposited composite coatings containing two types of aluminum-oxide powders with different dispersities (alumina Al2O3-1 and electroexplosive aluminum-oxide nanopowder Al2O3-2) are obtained during the work. The studies show that introducing the powders leads to a change in the microstructure of the composites and a change in the grain growth principles during the formation of the coatings. Refinement and ordering of the grain structure of the coatings occurs and twinning defects and texture are formed. The change in the formation of the microstructure of the composites leads to a change in some operational characteristics: an increase in the microhardness (by 10% in the composites with the addition of alumina and by more than 30% in the coatings with electroexplosive aluminum oxide) and ultimate tensile strength (by 20% in the composites with Al2O3-1 and almost 1.5-fold in the samples with Al2O3-2).
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kveglis, Ludmila I., Yerbolatuly, Dosym E., Noskov, Fedor M., Komogortsev S. V., Volochaev M. N.
Заглавие : Phases, microstructure and magnetic properties in a severely deformed Cr-Ni–Al alloy
Место публикации : J. Supercond. Nov. Magn. - 2023. - Vol. 36, Is. 4. - P.1249-1255. - ISSN 15571939 (ISSN), DOI 10.1007/s10948-023-06567-8. - ISSN 15571947 (eISSN)
Примечания : Cited References: 22. - The authors express their gratitude to Nurgamit Kantay (East-Kazakhstan University named after S. Amanzholov) for his help in conducting the experiment
Аннотация: The phases, microstructure, and magnetic properties in a severely deformed Cr-Ni–Al alloy have been studied. The eutectic microstructure observed in localized regions of the alloy can be interpreted as a result from the super-Arrhenius relaxation of the alloy. According to X-ray diffraction and magnetometry, the nanosized nickel inclusions in the matrix of the chromium-nickel γ-solid solution are formed. It is shown that, after severe (superplastic) deformation, a unidirectional magnetic anisotropy is induced, which may be associated with the antiferromagnetic coupling between the CrNi2 matrix and the nickel inclusions.
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18.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Iskhakov R. S., Komogortsev S. V., Denisova E. A., Chekanova L. A., Kalinin Yu. E., Sitnikov A. V.
Заглавие : Magnetic microstructure in the Co41Fe39B20-SiO2, Co-SiO2, Co-CaF nanocomposite films
Коллективы : Moscow International Symposium on Magnetism, Московский государственный университет им. М.В. Ломоносова, Российский фонд фундаментальных исследований
Место публикации : Moscow Int. Symp. on Magnet. (MISM-2008): June 20-25, 2008, Moscow : book of abstract. - 2008. - Ст.22PO-8-46. - p.299
Примечания : Support by the grant RFBR 07-02-01172-а; National Science Fund (2008, PhD RAS) are acknowledged
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volova, Tatiana G., Demidenko, Aleksey V., Murueva, Anastasiya V., Dudaev, Alexey E., Nemtsev I. V., Shishatskaya, Ekaterina I.
Заглавие : Biodegradable polyhydroxyalkanoates formed by 3- and 4-hydroxybutyrate monomers to produce nanomembranes suitable for drug delivery and cell culture
Колич.характеристики :23 с
Место публикации : Technologies. - 2023. - Vol. 11, Is. 4. - Ст.106. - ISSN 22277080 (eISSN), DOI 10.3390/technologies11040106
Примечания : Cited References: 116. - his research was funded by State Assignment of the Ministry of Science and Higher Education of the Russian Federation (project No. 0287-2021-0025)
Аннотация: Biodegradable polyhydroxyalkanoates, biopolymers of microbiological origin, formed by 3- and 4-hydroxybutyrate monomers P(3HB-co-4HB), were used to obtain nanomembranes loaded with drugs as cell carriers by electrospinning. Resorbable non-woven membranes from P(3HB-co-4HB) loaded with ceftazidime, doripinem, and actovegin have been obtained. The loading of membranes with drugs differently affected the size of fibers and the structure of membranes, and in all cases increased the hydrophilicity of the surface. The release of drugs in vitro was gradual, which corresponded to the Higuchi and Korsmeyer-Peppas models. Antibiotic-loaded membranes showed antibacterial activity against S. aureus and E. coli, in which growth inhibition zones were 41.7 ± 1.1 and 38.6 ± 1.7 mm for ceftazidime and doripinem, respectively. The study of the biological activity of membranes in the NIH 3T3 mouse fibroblast culture based on the results of DAPI and FITC staining of cells, as well as the MTT test, did not reveal a negative effect despite the presence of antibiotics in them. Samples containing actovegin exhibit a stimulating effect on fibroblasts. Biodegradable polyhydroxyalkanoates formed by 3-hydroxybutyrate and 4-hydroxybutyrate monomers provide electrospinning non-woven membranes suitable for long-term delivery of drugs and cultivation of eukaryotic cells, and are promising for the treatment of wound defects complicated by infection.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Timofeeva E. E., Panchenko E. Yu., Tokhmetova A. B., Volochaev M. N., Zherdeva M. V., Tagiltsev A. I., Surikov N. Yu., Chumlyakov Yu. I.
Заглавие : The effect of heat treatment on microstructure and martensitic transformation temperatures in Ni44Fe19Ga27Co10 single crystals
Колич.характеристики :7 с
Место публикации : Phys. Scr. - 2024. - Vol. 99, Is. 1. - Ст.015958. - ISSN 00318949 (ISSN), DOI 10.1088/1402-4896/ad16b2. - ISSN 14024896 (eISSN)
Примечания : Cited References: 34. - This work was supported by the Russian Science Foundation (grant No. 21-19-00287)
Аннотация: The microstructure and temperature of martensitic transformation of Ni44Fe19Ga27Co10 single crystals after aging at temperatures from 623 K to 1173 K were studied by electron microscopy and differential scanning calorimetry. The temperature ranges of the second phase precipitation, their lattice structure and volume fraction, and also the modification of the nanodomain structure of the L21+B2 high-temperature phase were determined in dependence on aging temperature. The influence of microstructure parameters on the martensitic transformation temperatures, transformation intervals and thermal hysteresis has been discussed.
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