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Effect of cation substitution in fluorine-oxygen molybdates (NH4)(2-x) A (x) MoO2F4 / E. V. Bogdanov [et al.] // Phys. Solid State. - 2011. - Vol. 53, Is. 2. - P. 303-308, DOI 10.1134/S1063783411020065. - Cited References: 11. - This study was supported by the Russian Foundation for Basic Research (project no. 09-02-00062) and the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools of the Russian Federation (project no. NSh-1011.2008.2). . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
   CRYSTALS
   (NH4)(2)WO2F4
   DIFFRACTION
   OXYFLUORIDE
   MECHANISM
   DISORDER
Аннотация: Thermophysical and structural studies of (NH4)(2 - x) A (x) MoO2F4 (A = Cs, Rb, K) solid solutions of oxyfluorides have been performed. The character of the influence of cation substitutions on the stability of the initial phase (space group Cmcm) and on the mechanism of phase transitions has been elucidated.

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Держатели документа:
[Bogdanov, E. V.
Vasil'ev, A. D.
Flerov, I. N.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Vasil'ev, A. D.
Flerov, I. N.] Siberian Fed Univ, Inst Engn Phys & Radioelect, Krasnoyarsk 660074, Russia
[Laptash, N. M.] Russian Acad Sci, Inst Chem, Far Eastern Branch, Vladivostok 690022, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk 660036, Russian Federation
Institute of Engineering Physics and Radioelectronics, Siberian Federal University, ul. Kirenskogo 28, Krasnoyarsk 660074, Russian Federation
Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences, pr. Stoletiya Vladivostoka 159, Vladivostok 690022, Russian Federation

Доп.точки доступа:
Bogdanov, E. V.; Богданов, Евгений Витальевич; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Flerov, I. N.; Флёров, Игорь Николаевич; Laptash, N. M.
}
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    Effects of composition modulation on the luminescence properties of Eu3+ doped Li1-xAgxLu(MoO4)2 solid-solution phosphors / F. Cheng [et al.] // Dalton Trans. - 2015. - Vol. 44, Is. 41. - P. 18078-18089, DOI 10.1039/c5dt02760h. - Cited References: 42. - The present work was supported by the National Natural Science Foundations of China (Grant No. 51272242, 51572023, 51511130035), Natural Science Foundations of Beijing (2132050), the Program for New Century Excellent Talents in University of Ministry of Education of China (NCET-12-0950), Beijing Nova Program (Z131103000413047), Beijing Youth Excellent Talent Program (YETP0635), the Funds of the State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences (RERU2015022), and the excellent tutor section of the Fundamental Research Funds for the Central Universities of China University of Geosciences, Beijing (2-9-2015-028). This work was also partly supported by the Russian Foundation for Basic Research (Grant No. 15-52-53080 GFEN_a). . - ISSN 1477-9226
   Перевод заглавия: Влияние модуляции состава на люминесцентные свойства твердотельного люминофора Li1-xAgxLu(MoO4)2 допированного Eu3+

РУБ Chemistry, Inorganic & Nuclear
Рубрики:
RED PHOSPHORS
   PHOTOLUMINESCENCE PROPERTIES
   ENERGY-TRANSFER
   WHITE LEDS
   IONS
   NA
   POLYMORPHISM
   TUNGSTATES
   RELAXATION
   MOLYBDATES
Аннотация: Double molybdate scheelite-type solid-solution phosphors Li1−xAgxLu1−y(MoO4)2:yEu3+ were synthesized by the solid state reaction method, and their crystal structures and luminescence properties were investigated in detail. The composition modulation and structural evolution of this series of samples were studied and the selected AgEu(MoO4)2, AgLu(MoO4)2, LiLu(MoO4)2 and LiEu(MoO4)2 phases were analyzed based on the Rietveld refinement. Depending on the variation of the Li/Ag ratio in Li1−xAgxLu1−y(MoO4)2:yEu3+ phosphors, the difference in the luminescence properties of Li1−xAgxLu1−y(MoO4)2:yEu3+ phosphors was ascribed to two factors, one reason could be assigned to the coupling effect and the nonradiative transition between the energy levels of LixAg1−xLu(MoO4)2 matrices and the activator Eu3+, another could be due to the near ultraviolet energy absorption and transmission efficiency between the charge-transfer (CT) band of O2−–Mo6+ and the 4f → 4f emissive transitions of Eu3+. The ultraviolet-visible diffuse reflection spectra (UV-vis DRS) and Raman spectra analysis were also used to verify the above mechanism.

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Держатели документа:
School of Materials Sciences and Technology, China University of Geosciences, Beijing, China
School of Materials Sciences and Engineering, University of Science and Technology Beijing, Beijing, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, Russian Federation
Beijing National Laboratory for Molecular Sciences, State Key Laboratory of Rare Earth Materials Chemistry and Applications, College of Chemistry and Molecular Engineering, Peking University, Beijing, China

Доп.точки доступа:
Cheng, F.; Xia, Zhiguo; Molokeev, M. S.; Молокеев, Максим Сергеевич; Jing, X.
}
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    Electronic structure of β-RbSm(MoO4)2 and chemical bonding in molybdates / V. V. Atuchin [et al.] // Dalton Trans. - 2015. - Vol. 44, Is. 4. - P. 1805-1815, DOI 10.1039/c4dt03203a. - Cited References: 121. - VVA and ASA gratefully acknowledge the Ministry of Education and Science of the Russian Federation for financial support. ZL acknowledges the support by National Natural Science Foundation of China (11174297 and 11474292), the National Basic Research Project of China (2011CB922204), and Foundation of the Director of Technical Institute of Physics and Chemistry, CAS. The work was partially supported by RAS Project 24-29 and RFBR Grant 13-02-00825. . - ISSN 1477-9226. - ISSN 1477-9234
   Перевод заглавия: Электронная структура бета-RbSm(MoO4)2 и химическая связь в молибдатах

РУБ Chemistry, Inorganic & Nuclear
Рубрики:
RAY PHOTOELECTRON-SPECTROSCOPY
   CRYSTAL-STRUCTURE
   X-RAY
   NEUTRON-DIFFRACTION
   MAGNETIC-PROPERTIES
   PHASE-FORMATION
   CORE LEVELS
   2ND-HARMONIC GENERATION
   LUMINESCENCE PROPERTIES
   VIBRATIONAL PROPERTIES
Аннотация: Microcrystals of orthorhombic rubidium samarium molybdate, beta-RbSm(MoO4)(2), have been fabricated by solid state synthesis at T = 450 degrees C, 70 h, and at T = 600 degrees C, 150 h. The crystal structure has been refined by the Rietveld method in space group Pbcn with cell parameters a = 5.0984(2), b = 18.9742(6) and c = 8.0449(3) angstrom (R-B = 1.72%). Thermal properties of beta-RbSm(MoO4)(2) were traced by DSC over the temperature range of T = 20-965 degrees C, and the earlier reported β ↔ α phase transition at T similar to 860-910 degrees C was not verified. The electronic structure of beta-RbSm(MoO4) 2 was studied by employing theoretical calculations and X-ray photoelectron spectroscopy. It has been established that the O 2p-like states contribute mainly to the upper part of the valence band and occupy the valence band maximum, whereas the Mo 4d-like states contribute mainly to the lower part of the valence band. Chemical bonding effects have been analysed from the element core level binding energy data. In addition, it was found that the luminescence spectrum of beta-RbSm(MoO4)(2) is rather peculiar among the Sm3+ containing materials. The optical refractive index dispersion in beta-RbSm(MoO4)(2) was also predicted by the first-principles calculations.

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Держатели документа:
RAS, Inst Semicond Phys, Lab Opt Mat & Struct, SB, Novosibirsk 630090, Russia
Tomsk State Univ, Funct Elect Lab, Tomsk 634050, Russia
Novosibirsk State Univ, Lab Semicond & Dielectr Mat, Novosibirsk 630090, Russia
RAS, Kirensky Inst Phys, Lab Coherent Opt, SB, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Krasnoyarsk 660041, Russia
RAS, Baikal Inst Nat Management, Lab Oxide Syst, SB, Ulan Ude 670047, Russia
Gen Res Inst Nonferrous Met, Beijing 100088, Peoples R China
RAS, Inst Semicond Phys, Lab Nanodiagnost & Nanolithog, SB, Novosibirsk 630090 90, Russia
RAS, Inst Semicond Phys, Lab Phys Bases Integrated Microelect, SB, Novosibirsk 630090 90, Russia
RAS, Kirensky Inst Phys, Lab Crystal Phys, SB, Krasnoyarsk 660036, Russia
RAS, Kirensky Inst Phys, Lab Mol Spect, SB, Krasnoyarsk 660036, Russia
Chinese Acad Sci, Tech Inst Phys & Chem, Beijing 100190, Peoples R China

Доп.точки доступа:
Atuchin, V. V.; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Chimitova, O. D.; Diao, C. P.; Gavrilova, T. A.; Kesler, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Krylov, A. S.; Крылов, Александр Сергеевич; Bazarov, B. G.; Bazarova, J. G.; Lin, Z. S.; Ministry of Education and Science of the Russian Federation; National Natural Science Foundation of China [11174297, 11474292]; National Basic Research Project of China [2011CB922204]; Foundation of the Director of Technical Institute of Physics and Chemistry, CAS; RAS [24-29]; RFBR [13-02-00825]
}
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    Formation, structural parametres of double molybdates RbLn(MoO4)2 / O. D. Chimitova [et al.] // 3 Междунар. науч.-технич. конф. "Функциональные и конструкционные матер." : Тезисы докладов. - 2013. - P. 52. - This study was partially supported by SB RAS (Grant 28.13), Grant RFBR № 11-08-00681-а
   Перевод заглавия: Формирование, структурные параметры двойных молибдатов RbLn(MoO4)2

Доп.точки доступа:
Chimitova, O. D.; Atuchin, V. V.; Bazarov, B. G.; Базаров Б.Г.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, Zh.G.; Базарова Ж.Г.; "Функциональные и конструкционные материалы", международная научно-техническая конференция, посвященная 95-летию НАН Украины (3 ; 2013 ; нояб. ; 11-14 ; Донецк, Украина)
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    High ionic conductivity of K5-xTlx(Mg0.5Hf1.5)(MoO4)6 (0 ≤ х ≤ 5) solid solutions / V. G. Grossman, M. S. Molokeev, J. G. Bazarova, B. G. Bazarov // Solid State Sci. - 2022. - Vol. 134. - Ст. 107027, DOI 10.1016/j.solidstatesciences.2022.107027. - Cited References: 39. - The work was supported by Basic Project of BINM SB RAS №0273-2021-0008. Structural analysis of materials in this study was partly supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation . X-ray powder diffraction and thermal analysis were obtained using the equipment of the Collective Use Center BINM SB RAS . - ISSN 1293-2558
   Перевод заглавия: Высокая ионная проводимость твердых растворов K5-xTlx(Mg0.5Hf1.5)(MoO4)6 (0 ≤ х ≤ 5)
Кл.слова (ненормированные):
Synthesis -- Thallium -- Potassium -- Molybdates -- DSC -- Conducting material
Аннотация: Novel K5-xTlx(Mg0.5Hf1.5)(MoO4)6 (0 ≤ х ≤ 5) oxides were successfully synthesized by solid state reaction. The results indicate the formation of a continuous series of solid solutions with the NASICON-like structure (sp. gr. R3¯c) in the composition range 0 < x < 5. The unit-cell parameters of the solid solutions increase linearly with composition, as a consequence of thallium substitution for potassium. The cation conductivity of Tl5Mg0.5Hf1.5(MoO4)6 has been shown to exceed the conductivity of the parent potassium magnesium hafnium molybdate. The highest total conductivity of 2.49 × 10−3 S/cm was found at 831 K for Tl5Mg0.5Hf1.5(MoO4)6.

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Держатели документа:
Baikal Institute of Nature Management, SB RAS, Sakhyanovoy St., 6, Ulan-Ude, 670047, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC, Siberian Branch, Academy of Sciences, 50 / 38 Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, 82 Svobodniy Av., Krasnoyarsk, 660041, Russian Federation
Department of Physics, Far Eastern State Transport University, Serysheva str. 47, Khabarovsk, 680021, Russian Federation

Доп.точки доступа:
Grossman, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, J. G.; Bazarov, B. G.
}
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    New triple molybdate K5ScHf(MoO4)6: Synthesis, properties, structure and phase equilibria in the M2MoO4–Sc2(MoO4)3–Hf(MoO4)2 (M = Li, K) systems / V. G. Grossman, J. G. Bazarova, M. S. Molokeev, B. G. Bazarov // J. Solid State Chem. - 2020. - Vol. 283. - Ст. 121143, DOI 10.1016/j.jssc.2019.121143. - Cited References: 53. - This study was carried out within the state assignment of FASO of Russia (Theme No 0339-2016-0007) as well was supported by RFBR Grants 18-08-00799 and 18-03-00557 . - ISSN 0022-4596
   Перевод заглавия: Новый тройной молибдат K5ScHf(MoO4)6: синтез, свойства, структура и фазовые равновесия в системах M2MoO4-Sc2(MoO4)3-Hf(MoO4)2 (M = Li, K)
Кл.слова (ненормированные):
Synthesis -- Molybdates -- X-ray diffraction -- DSC -- Electric properties
Аннотация: Subsolidus phase relations in the M2MoO4–Sc2(MoO4)3–Hf(MoO4)2 (M = Li, K) systems have been studied by the method of “intersecting cuts”. No new triple molybdates have been identified in the Li2MoO4–Sc2(MoO4)3–Hf(MoO4)2 system and a new triple molybdate K5ScHf(MoO4)6 is formed in the K2MoO4–Sc2(MoO4)3–Hf(MoO4)2 system. The structure of K5ScHf(MoO4)6, have been determined in space group Rc through Rietveld analysis of X-ray powder diffraction data. The melting point of molybdate is 999 K. The compound has high ion conductivity (about 10−3 S cm−1).

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Держатели документа:
Baikal Institute of Nature Management, Siberian Branch, Russian Academy of Sciences, Sakhyanovoy St., 6, Ulan-Ude, Buryat Republic 670047, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC, Siberian Branch, RAS, 50 / 38 Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, 82 Svobodniy Av., Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Grossman, V. G.; Bazarova, J. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarov, B. G.
}
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    Optical Properties of Trigonal Single Crystals (Yb,Tm)Al3(BO3)4 Grown from Fluxes Based on the Bismuth and Lithium Molybdates [Text] / В. Л. Темеров, А. Э. Соколов [и др.] // Crystallography report. - 2008. - Vol. 53, No. 7. - P. 1157-1162DOI 10.1134/S1063774508070110
   Перевод заглавия: Оптические свойства тригональных монокристаллов (Yb,Tm)Al3(BO3)4, выращиваемых из раствор-расплавов на основе молибдатов висмута и лития

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Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Temerov, V. L.; Темеров, Владислав Леонидович; Sokolov, A. Е.; Соколов, Алексей Эдуардович; Sukhachev, A. L.; Сухачев, Александр Леонидович; Bovina, A. F.; Бовина, Ася Федоровна; Edel'man, I. S.; Эдельман, Ирина Самсоновна; Malakhovskii, A. V.; Малаховский, Александр Валентинович
}
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    Potassium and thallium conductors with a trigonal structure in the M2MoO4–Cr2(MoO4)3–Hf(MoO4)2 (M = K, Tl) systems: Synthesis, structure, and ionic conductivity / V. G. Grossman, M. S. Molokeev, B. G. Bazarov, J. G. Bazarova // J. Alloys Compd. - 2021. - Vol. 873. - Ст. 159828, DOI 10.1016/j.jallcom.2021.159828. - Cited References: 62. - The work was supported by Basic Project of BINM SB RAS № 0273-2021-0008 . Research was conducted using equipment of the CCU BINM SB RAS (Ulan-Ude, Russia). Structural analysis of materials in this study was partly supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation . - ISSN 0925-8388
   Перевод заглавия: Калиевые и таллиевые проводники с тригональной структурой в системах M2MoO4-Cr2(MoO4)3–Hf(MoO4)2 (M = K, Tl): синтез, структура и ионная проводимость
Кл.слова (ненормированные):
Synthesis -- Thallium -- Potassium -- Molybdates -- Phase diagram -- DSC -- Conducting material
Аннотация: The triple molybdates M5CrHf(MoO4)6 (M = K, Tl) and TlCrHf0.5(MoO4)3 were found upon studying the corresponding ternary molybdate systems M2MoO4–Cr2(MoO4)3–Hf(MoO4)2 (M = K, Tl) in the subsolidus region using X-ray powder diffraction. The crystal structures of M5CrHf(MoO4)6 (M = K, Tl) and TlCrHf0.5(MoO4)3 are refined by Rietveld method. M5CrHf(MoO4)6 (M = K, Tl) crystallizes in space group Rc with unit cell parameters: a = b = 10.45548 (5), c = 37.24614 (3) Å, V = 3526.14 (4) Å3, Z = 6 for K5CrHf(MoO4)6 and a = b = 10.53406 (12), c = 37.6837 (5) Å, V = 3621.39 (9) Å3, Z = 6 for Tl5CrHf(MoO4)6. TlCrHf0.5(MoO4)3 crystallizes in space group R with unit cell parameters: a = b = 12.9710 (2), c = 11.7825 (2) Å, V = 1716.78 (6) Å3, Z = 6. The thermal stability and electrical conductivity of the new compounds were investigated. Electrical conductivity measurements gave high values for the triple molybdates M5CrHf(MoO4)6 (M = K, Tl) (σ = 5.22 × 10−4 S / cm for K5CrHf(MoO4)6, σ = 1.1 × 10−2 S / cm for Tl5CrHf(MoO4)6 at 773 K) and relatively low values for the triple molybdate TlCrHf0.5(MoO4)3 (σ = 4.42 × 10−6 S / cm at 773 K).

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Держатели документа:
Baikal Institute of Nature Management, SB RAS, Sakhyanovoy St., 6, Ulan-Ude, 670047, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC, Siberian Branch, Academy of Sciences, 50/38 Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, 82 Svobodniy Av., Krasnoyarsk, 660041, Russian Federation
Department of Physics, Far Eastern State Transport University, Serysheva str. 47, Khabarovsk, 680021, Russian Federation

Доп.точки доступа:
Grossman, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarov, B. G.; Bazarova, J. G.
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    Structural parameters of double molybdates ALn(MoO4)2 / V. V. Atuchin [et al.] // XVI Международная конференция "Опто-, наноэлектроника, нанотехнологии и микросистемы" : Труды. - Ульяновск, 2013. - P. 239-240
   Перевод заглавия: Структурные параметры двойных молибдатов ALn(MoO4)2

Материалы конференции

Доп.точки доступа:
Atuchin, V. V.; Chimitova, O. D.; Bazarov, B. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, Zh.G.; Институт нанотехнологий микроэлектроники РАН; Ульяновский государственный университет; Российский фонд фундаментальных исследований; Академия наук Татарстана; "Opto-, nanoelectronics, nanotechnology, and microsystems", International Conference (2013 ; Jul. ; 26-30 ; Ulyanovsk, Russia); "Опто-, наноэлектроника, нанотехнологии и микросистемы", международная конференция (2013 ; июль.; 26-30 ; Ульяновск)
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10.

    Structural, thermal and electrical studies of thallium-scandium-hafnium(zirconium) molybdates / V. G. Grossman, M. S. Molokeev, J. G. Bazarova [et al.] // J. Solid State Chem. - 2022. - Vol. 307. - Ст. 122832, DOI 10.1016/j.jssc.2021.122832. - Cited References: 56. - The work was supported by Basic Project of BINM SB RAS N degrees 0273-2021-0008. Research was conducted using equipment of the CCU BINM SB RAS. Structural analysis of materials in this study was partly sup-ported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation . - ISSN 0022-4596. - ISSN 1095-726X
   Перевод заглавия: Структурные, термические и электрические исследования молибдатов таллия-скандия-гафния(циркония)

РУБ Chemistry, Inorganic & Nuclear + Chemistry, Physical
Рубрики:
POSITIVE ELECTRODE MATERIAL
CRYSTAL-STRUCTURE
IONIC-CONDUCTIVITY
Кл.слова (ненормированные):
Synthesis -- Scandium -- Thallium -- Molybdates -- Impedance spectroscopy -- Conducting material
Аннотация: Thallium scandium hafnium molybdate Tl5ScHf(MoO4)6 and thallium scandium zirconium molybdate Tl5ScZr(MoO4)6 crystallize in trigonal symmetry with the space group . The compounds are synthesized by sintering the finely powdered simple molybdates mixture in a muffle furnace at 723–823 K for 100 h. The crystal structures of Tl5ScHf(MoO4)6 and Tl5ScZr(MoO4)6 are obtained by Rietveld method. The following unit cell parameters are calculated for Tl5ScHf(MoO4)6: a = 10.62338 (5), c = 38.0579 (2) Å, V = 3719.64 (4) Å3, Z = 6 and for Tl5ScZr(MoO4)6: a = 10.63216 (7), c = 38.0716 (3) Å, V = 3727.14 (5) Å3, Z = 6. The conductivity of the Tl5ScHf(MoO4)6 and Tl5ScZr(MoO4)6 are measured between 293 and 860 K. The ionic conductivity of Tl5ScHf(MoO4)6 and Tl5ScZr(MoO4)6 molybdates are 8 × 10−4 S/cm and 8 × 10−3 S/cm (at 773 K); the activation energy of ionic transfer are 0.8 eV and 0.3 eV respectively.

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Держатели документа:
SB RAS, Baikal Inst Nat Management, Sakhyanovoy St 6, Ulan Ude 670047, Russia.
Acad Sci, Fed Res Ctr KSC, Kirensky Inst Phys, Siberian Branch, 50-38 Akademgorodok, Krasnoyarsk 660036, Russia.
Kemerovo State Univ, Res & Dev Dept, Kemerovo 650000, Russia.
Russian Acad Sci, Fed Sci Res Ctr Crystallog & Photon, Shubnikov Inst Crystallog, Moscow 119333, Russia.

Доп.точки доступа:
Grossman, Victoria G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Bazarova, Jibzema G.; Bazarov, Bair G.; Sorokin, Nikolay, I; Basic Project of BINM SB RAS [0273-2021-0008]; Government of the Russian Federation [075-15-2019-1886]
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