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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Menzyanova N. G., Pyatina S. A., Shabanov A. V., Nemtsev I. V., Stolyarov D. P., Dryganov D. B., Sakhnov E. V., Shishatskaya E. I.
Заглавие : The morphology and phenotype of monocyte-macrophages when cultured on bionanofilms substrates with different surface relief profiles
Место публикации : Biomolecules. - 2020. - Vol. 10, Is. 1. - Ст.65. - ISSN 2218273X (ISSN), DOI 10.3390/biom10010065
Примечания : Cited References: 40. - This research was funded by the Russian Science Foundation, Project No 17-15-01352
Аннотация: The effect of surface relief profiles of alkanoate-based bionanofilms to the monocyte-macrophages (MN-MPhs) from peripheral blood of patients with atherosclerosis was studied in vitro. Patients were subjected to coronary stenting. Cell morphology and phenotype (expression of CD antigens, levels of production of marker cytokines) in vitro were analyzed before and after the installation of stents. It was shown, that the mean square roughness (Rq) of the bionanofilms determined the variability of cell morphology, CD antigens spectraand activity of production interleukins-6 and-10. Also, it was revealed, that the “activity” of the surface topography of biopolymer substrates depends on the functional state of MNs, isolated in different time points: Before and after stenting the ratios of cell morphotypes and production of cytokines in MN-MPhs differed significantly.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Petrov D. A., Ivantsov R. D., Zharkov S. M., Yurkin G. Yu., Molokeev M. S., Knyazev Yu. V., Lin C.-R., Tseng Y.-T.
Заглавие : Core-shell iron oxide-carbon nanoparticles modified with Ag. synthesis, morphology, magnetic properties
Коллективы : Российская академия наук, Уральское отделение РАН, Институт физики металлов им. М. Н. Михеева Уральского отделения РАН, Уральский федеральный университет им. первого Президента России Б.Н. Ельцина, Российский фонд фундаментальных исследований, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : Euro-asian symposium "Trends in magnetism" (EASTMAG-2019): Book of abstracts/ чл. конс. ком.: S. G. Ovchinnikov, N. V. Volkov [et al.] ; чл. прогр. ком. D. M. Dzebisashvili [et al.]. - 2019. - Vol. 2. - Ст.J.P18. - P.220-221. - ISBN 978-5-9500855-7-4 (Шифр В33/E12-125657784)
Примечания : Cited References: 2. - The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science to the research project No. 18-42-243021 and by Joint Research Project of Russian Foundation for Basic Research and Ministry of Science and Technology, Taiwan MOST No. 19-52-52002
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chilom, Claudia G., Zorilă, Bogdan, Bacalum M., Bălăşoiu, Maria, Yaroslavtsev R. N., Stolyar S. V., Tyutyunnicov, Sergey
Заглавие : Ferrihydrite nanoparticles interaction with model lipid membranes.
Место публикации : Chem. Phys. Lipids. - 2020. - Vol. 226. - Ст.104851. - ISSN 0009-3084, DOI 10.1016/j.chemphyslip.2019.104851. - ISSN 1873-2941 (eISSN)
Примечания : Cited References: 70. - The work was accomplished with the financial support of the 2019 RO-JINR Project Investigation of biogenic and chemically synthesized systems in interaction with biostructures for applied research, Theme 02-1-1107-2011/2019 and of the Romanian National Authority for Scientific Research, CNDI-UEFISCDI, Project numbers: PN 18 09 02 02/2018 and PN 19 06 02 03/2019. The authors are very much indebted to Professor Dr. Aurel Popescu, for very helpful suggestions and permanent encouragement.
Аннотация: In recent years was observed an increased interest towards the use of metal nanoparticles for various biomedical applications, such as therapeutics, delivery systems or imaging. As biological membranes are the first structures with which the nanoparticles interact, it is necessary to understand better the mechanisms governing these interactions. In the present paper we aim to characterize the effect of three different ferrihydrite nanoparticles (simple or doped with cooper or cobalt) on the fluidity of model lipid membranes. First we evaluated the physicochemical properties of the nanoparticles: size and composition. Secondly, their effect on lipid membranes was also evaluated using Laurdan, TMA-DPH and DPH fluorescence. Our results can help better understand the mechanisms involved in nanoparticles and membrane interactions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tarasov I. A., Smolyarova T. E., Nemtsev I. V., Yakovlev I. A., Volochaev M. N., Solovyov L. A., Varnakov S. N., Ovchinnikov S. G.
Заглавие : Tailoring the preferable orientation relationship and shape of α-FeSi2nanocrystals on Si(001): The impact of gold and the Si/Fe flux ratio, and the origin of α/Si boundaries
Место публикации : CrystEngComm. - 2020. - Vol. 22, Is. 23. - P.3943-3955. - ISSN 14668033 (ISSN), DOI 10.1039/d0ce00399a
Примечания : Cited References: 52. - The experimental part of the reported study was funded by the Russian Science Foundation, project no. 16-13-00060-Π. Theoretical analysis of the ORs of the α-FeSi2 nanocrystals grown was supported by the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science via research project No. 18-42-243013. We also acknowledge the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” for support with carrying out the microscopic investigations. I. A. Tarasov personally thanks M. A. Visotin for continuous fruitful discussion about the energetics of the formation of the α-FeSi2 nanocrystals
Аннотация: The growth of α-FeSi2 nanocrystal ensembles on gold-activated and gold-free Si(001) surfaces at different Si/Fe flux ratios via molecular beam epitaxy is reported. The study reveals that the utilisation of gold as a catalyst regulates the preferable orientation relationship (OR) of the nanocrystals to silicon and their morphology at a given Si/Fe flux ratio. α-FeSi2 free-standing crystals with continuously tuned sizes from 30 nm up to several micrometres can be grown with an α(001)//Si(001) basic OR under gold-assisted conditions and an α(111)//Si(001) OR under gold-free growth conditions on a Si(001) surface. The preferred morphology of nanocrystals with a particular OR can be altered through changes to the Si/Fe flux ratio. Herein, the microstructure and basic OR between the silicide nanocrystals and the silicon substrate, and the formation of nanocrystal facets were analysed in detail with the help of microscopic techniques and simulation methods based on the analysis of near coincidence site (NCS) distributions at silicide/silicon interfaces. On the basis of the simulations used, we managed to reveal the nature of the interfaces observed for the main types of α-FeSi2 nanocrystals grown. Three types of interfaces typical for nanoplates with an α(001)//Si(001) basic OR, which are (i) stepped, (ii) stressed, and (iii) flat, are explained based on the tendency for the NCS density to increase at the interface. The results presented reveal the potential for the bottom-up fabrication of α-FeSi2 nanocrystals with tuned physical properties as potentially important contact materials and as building blocks for future nanoelectronic devices.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Sokolov A. Е., Ivanova O. S., Svetlitsky E. S., Petrov D. A., Chen Ying-Zhen, Spivakov A. A., Lin En-Szu, Jhang Cheng-Jhih, Tseng Yaw Teng, Lin Chun-Rong
Заглавие : Magnetic nanoparticles FE3O4@C: synthesis, morphology, magnetic properties and application
Коллективы : "Новое в магнетизме и магнитных материалах", международная конференция, Научный совет по физике конденсированных сред РАН, МИРЭА - Российский технологический университет, Московский государственный университет им. М.В. Ломоносова, Магнитное общество России
Место публикации : Новое в магнетизме и магнитных материалах: сборник трудов XXIV международной конференции/ прогр. ком.: Р. С. Исхаков, С. Г. Овчинников [и др.]. - 2021. - Секция 10: Малые магнитные частицы. - Ст.10-35-38
Примечания : Библиогр.: 8
Аннотация: Работа посвящена исследованию магнитных наночастиц Fe3O4@C, синтезированных методом термического разложения с использованием трех различных маршрутов синтеза: (1) двухстадийный процесс, когда предварительно синтезированные наночастицы Fe3O4 покрываются углеродом, (2) наночастицы в одностадийном процессе получения покрываются углеродом, и (3) эти наночастицы ядро-оболочка покрывались дополнительной углеродной оболочкой. Изучены морфология и особенности магнитных и магнитооптических свойств полученных гибридных наночастиц. Исследованы адсорбционные свойства наночастиц по удалению катионных и анионных красителей из водных растворов.The work is devoted to the study of the Fe3O4@C magnetic nanoparticles synthesized with the thermal decomposition method using three different synthesis routes: (1) two stage process when preliminary synthesized Fe3O4 nanoparticles were covered by carbon, (2) core-shell nanoparticles were prepared in the one stage process, and (3) these core-shell nanoparticles were covered with the additional carbon shell. The morphology and features of the magnetic and magneto-optical properties of the obtained hybrid nanoparticles were studied. The sorption properties of NPs for the removal of dyes have been studied.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Coondoo I., Panwar N., Krylova S. N., Krylov A. S., Alikin D., Jakka S. K., Turygin A., Shur V. Y., Kholkin A. L.
Заглавие : Temperature-dependent Raman spectroscopy, domain morphology and photoluminescence studies in lead-free BCZT ceramic
Место публикации : Ceram. Int. - 2021. - Vol. 47, Is. 2. - P.2828-2838. - ISSN 02728842 (ISSN), DOI 10.1016/j.ceramint.2020.09.137
Примечания : Cited References: 65. - I.C. would like to thank financial assistance by national funds (OE), through FCT – Fundação para a Ciência e a Tecnologia, I.P., in the scope of the framework contract foreseen in the numbers 4, 5 and 6 of the article 23, of the Decree-Law 57/2016, of August 29, changed by Law 57/2017, of July 19. This work was developed within the scope of the project CICECO-Aveiro Institute of Materials, UIDB/50011/2020 & UIDP/50011/2020, financed by national funds through the Portuguese Foundation for Science and Technology / MCTES . The authors would also like to acknowledge the Ural Center for Shared Use “Modern nanotechnology”, Ural Federal University, Russia and the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS”. The authors would like to thank Dr. E. Venkata Ramana, Department of Physics, University of Aveiro for the dielectric measurements. The work was supported by Government of the Russian Federation (Act 211, 440 Agreement 02.A03.21.0006)
Аннотация: Present work focuses on detailed temperature-dependent X-ray diffraction, Raman scattering, domain configuration, and photoluminescence (PL) studies in the (Ba0·85Ca0.15) (Zr0·10Ti0.90)O3 (BCZT) ceramics. The comprehensive Raman spectroscopy analysis in the present work not only validates the presence of the intermediate orthorhombic phase in BCZT, but also provides evidence of another transition: rhombohedral R3c phase to R3m at low temperature. Temperature behaviour of the lowest frequency transverse optical mode (soft E (TO) phonon) and hard modes was studied. Temperature dependence of peak positions, intensities, and linewidths of Raman phonon modes signalled the presence of phase transitions near −50 ± 5 °C, 0±5 °C, 35±5 °C and 110 ± 10 °C. Evolution of domain morphology occurring at phase transitions above room temperature was studied by piezoresponse force microscopy technique. Analysis of PL spectra revealed disorder/heterogeneity in the sample and indicated the existence of self-trapped excitons. PL spectra are composed of four distinct colour components (~2.55eV:blue, ~2.32eV:green, ~2.08eV:orange and ~1.78eV:red).
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Nemtsev I. V., Komogortsev S. V., Shepeta N. A.
Заглавие : Soft magnetic FeCo films produced by green chemistry technique
Коллективы : International Conference on High-Tech and Innovations in Research and Manufacturing
Место публикации : J. Phys.: Conf. Ser. - 2020. - Vol. 1582, Is. 1. - Ст.012077. - DOI 10.1088/1742-6596/1582/1/012077
Примечания : Cited References: 10. - This work was funded by the Russian Foundation for Basic Research, the Government of the Krasnoyarsk Territory, the Krasnoyarsk Regional Fund for the Support of Scientific and Technical Activities (project no. 18-42-240006 Nanomaterials with magnetic properties determined by the topological features of the nanostructure). The authors thank the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS for the provided equipment
Аннотация: The saturation magnetizations, local magnetic anisotropy field and coercivity values of FeCo film plated under various processing conditions have been investigated to optimize soft magnetic properties. Herein, we introduce a very promising processing technique based on the electrodeless deposition of FeCo film with carbohydrates as reducing agents. The produced FeCo film demonstrated significantly better saturation magnetization values and less contaminations, compared to those for the sample preparing with conventional reducing agent (sodium hypophosphite). The surface morphology and coercivities of FeCo films are dependent on the iron content and type of reducing agent. The coercive force values range from 12 up to 30 Oe and the saturation magnetization from 150 to 240 emu/g depending on the bath composition and deposition parameters. Maximum of saturation magnetization magnitude is reached for FeCo film with 30% cobalt. The local anisotropy field value of FeCo alloys increases with a decrease in Fe content for all reducing agent types.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Logutenko O. A., Titkov A. I., Vorob'yov A. M., Balaev D. A., Shaikhutdinov K. A., Semenov S. V., Yukhin Y. M., Lyakhov N. Z.
Заглавие : Effect of molecular weight of sodium polyacrylates on the size and morphology of nickel nanoparticles synthesized by the modified polyol method and their magnetic properties
Место публикации : Eur. Polym. J. - 2018. - Vol. 99. - P.102-110. - ISSN 00143057 (ISSN), DOI 10.1016/j.eurpolymj.2017.12.017
Примечания : Cited References: 26. - This work was supported by the Russian Science Foundation, research project No. 15-13-00113.
Ключевые слова (''Своб.индексиров.''): nickel nanoparticles--sodium polyacrylate--polyol--reduction--magnetic properties
Аннотация: Nickel nanoparticles were synthesized by the reduction of nickel chloride with hydrazine hydrate in a polyol medium in the presence of sodium polyacrylates (Na-PA) having molecular weights (Mw) of 1200, 5100 and 8000. The size and morphology of the resulting nickel nanoparticles were characterized by X-ray diffraction, scanning and transmission electron microscopy. Polymers having lower Mw values were found to be more efficient in reducing the nickel particle size. A decrease in the polymer concentrations yielded the smaller particles. Magnetic measurements showed that the as-prepared powders are ferromagnetic and their saturation magnetization and coercivity are size-dependent. Compared with bulk nickel, the nanoparticles exhibit an enhanced coercivity which is due to their small size and a decreased saturation magnetization resulted from the surface oxidation of the powder. The synthesis procedure offers a simple approach to preparing nickel nanopowders on a large scale which could be used as magnetic recording materials, including high-density memory storage devices.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrov D. A., Ivantsov R. D., Zharkov S. M., Lin C.-R., Shu F.-R., Tseng Y.-T.
Заглавие : Synthesis, morphology, and visible magnetic circular dichroism of Ni-C nanoparticles
Место публикации : J. Sib. Fed. Univ. Math. Phys. - 2016. - Vol. 9, Is. 4. - P.481-484. - ISSN 1997-1397, DOI 10.17516/1997-1397-2016-9-4-481-484; Журн. СФУ. Сер. "Математика и физика"
Примечания : Библиогр.: 2. - This work was supported by the RFBR grant 14-02-01211 and MOST 102-2112-M-153-002-MY3.
Ключевые слова (''Своб.индексиров.''): mcd--nanoparticles--ni-c--tem--наночастицы--мкд--электронная микроскопия
Аннотация: Ni-C nanoparticles powder (NP) was synthesized using high-temperature pyrolysis of nickel nitrate in an organic solvent. The NP was characterized by transmission electron microscopy (TEM), energy dispersive x-ray spectroscopy (EDXS) and selected-area electron diffraction (SAED). Structural characterization of the samples confirmed the formation of small, medium and large Ni nanoparticles with face-centered cubic structure (fcc) and enlarged lattice parameter. Magnetic circular dichroism (MCD) of samples with different mean particle sizes showed a red shift with decrease of mean particle size. © Siberian Federal University. All rights reserved.Порошок наночастиц Ni-C был синтезирован с помощью высокотемпературного пиролиза нитрата никеля в органическом растворителе. Наночастицы были исследованы с помощью просвечивающей электронной микроскопии, энергодисперсионной рентгеновской спектроскопии и дифракции электронов выбранной зоны. Структурная характеризация образцов подтвердила образование маленьких, средних и больших наночастиц никеля с гранецентрированной кубической структурой и увеличенным параметром решётки. Магнитный круговой дихроизм образцов с различными средними размерами частиц показал красное смещение при уменьшении среднего размера частиц.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Morozov E. V., Falaleev O. V., Martyanov O. N.
Заглавие : New insight into the wax precipitation process: in situ NMR imaging study in a cold finger cell
Место публикации : Energy Fuels: American Chemical Society, 2016. - Vol. 30, Is. 11. - P.9003-9013. - ISSN 08870624 (ISSN), DOI 10.1021/acs.energyfuels.6b01535
Примечания : Cited References: 69. - This research was performed with the financial support of the Russian Science Foundation (Project No. 15-19-00119).
Ключевые слова (''Своб.индексиров.''): cells--crude oil--cytology--deposits--diffusion--gelation--magnetic resonance imaging--ostwald ripening--phase separation--polymer blends--deposit formation--deposit structures--diffusion controlled growth--dominant mechanism--lower temperatures--morphology and dynamics--phase-separation process--temperature regimes--image processing
Аннотация: A cold finger cell intended for the wax deposition measurements was fabricated and integrated into an NMR imaging probe for the noninvasive study of wax precipitation processes in situ. The cell was first tested with a model system; then, a series of experiments with different thermal gradients applied to the cell were performed for a waxy crude oil. NMR imaging of the operating cell revealed the formation of a deposit with the morphology and dynamics strongly correlating with the temperature regime. At higher temperatures of cold finger, the incipient wax gel ages uniformly, giving rise to the hard and thin inner layer of deposit accompanied by a branched loosely consolidated outer layer. Conversely, the lower temperatures facilitate formation of a thick deposit which no longer ages uniformly and slow down the diffusion-controlled growth of the branched deposit structure. The results obtained are consistent with the majority of the data previously reported. Thus, gelation of the wax at temperatures below the cloud point and subsequent thermal-driven diffusion processes are considered to be the dominant mechanisms of the deposit formation. The counter diffusion and Ostwald ripening aging concepts were found to be relevant in the case of the cold finger study and account for the phenomena observed in this work. The information obtained via NMR imaging is highly complementary to the results obtained by other techniques that can aid in understanding the essential processes behind the wax precipitation phenomena. The approach developed can be effectively extended to study any thermal-driven phase separation process. © 2016 American Chemical Society.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Menzyanova N. G., Pyatina S. А., Nikolaeva E. D., Shabanov A. V., Nemtsev I. V., Stolyarov D. P., Dryganov D. B., Sakhnov E. V., Shishatskaya E. I.
Заглавие : Screening of biopolymeric materials for cardiovascular surgery toxicity—Evaluation of their surface relief with assessment of morphological aspects of monocyte/macrophage polarization in atherosclerosis patients
Место публикации : Toxicol. Rep. - 2019. - Vol. 6. - P.74-90. - ISSN 22147500 (ISSN), DOI 10.1016/j.toxrep.2018.11.009
Примечания : Cited References: 85. - The study was supported by the Russian Science Foundation , Project No 17-15-01352 .
Ключевые слова (''Своб.индексиров.''): monocytes--macrophages--cell morphology--polyhydroxyalkanoates--atherosclerosis--intravascular stenting
Аннотация: The morphotypes of human macrophages (MPh) were studied in the culture on nano-structured biopolymer substrates, made from polyhydroxyalcanoates (PHAs) of five various monomer compositions, followed by the solvent evaporation. Its surface relief, which was further in direct contact with human cells in vitro, was analyzed by atomic force microscopy (AFM) and scanning electron microscopy (SEM). It was shown, that the features of the micro/nano relief depend on the monomeric composition of the polymer substrates. Monocytes (MN) of patients with atherosclerosis and cardiac ischemia, undergoing stenting and conventional anti-atherosclerotic therapy, were harvested prior and after stenting. MN were isolated and cultured, with the transformation into MPh in direct contact with biopolymer culture substrates with different monomer composition and nano-reliefs, and transformed into MPh, in comparison with the same process on standard culture plastic. Sub-populations of cells with characteristic morphology in each phenotypic class were described, and their quantitative ratios for each sample of polymers were counted as an intermediate result in the development of “smart” material for cardiovascular devices. The results obtained allow us to assume, that the processes of MPh differentiation and polarization in vitro depend not only on the features of the micro/nano relief of biopolymer substrates, but also on the initial state of MN in vivo and general response of patients.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Nemtsev I. V., Shabanova, Olga V., Shestakov N. P., Cherepakhin A. V., Zyryanov V. Ya.
Заглавие : Morphology stability of polymethylmethacrylate nanospheres formed in water-acetone dispersion medium
Место публикации : Appl. Phys. A. - 2019. - Vol. 125, Is. 10. - Ст.738. - ISSN 0947-8396, DOI 10.1007/s00339-019-3036-4. - ISSN 1432-0630(eISSN)
Примечания : Cited References: 93
Предметные рубрики: OPAL PHOTONIC CRYSTALS
POLY(METHYL METHACRYLATE)
UP-CONVERSION
Аннотация: The aim of this study is to develop a manufacturing technique of polymethylmethacrylate (PMMA) nanospheres to produce a more stable opal template. Water-acetone mixture was used as a dispersion medium to synthesize a PMMA opal structure. Morphology features, IR vibrational spectra and glass transition temperatures of the PMMA nanospheres formed in the water-acetone dispersion medium (nanospheres A) have been studied comparing with the same prepared in distilled water solution without acetone (nanospheres B). A dependence of a shrinkage degree of the nanoparticles on the acetone volume has been investigated. It has been revealed that under an electron beam action the shrinkage degree of the nanospheres A is in the range of 7-16% while the shrinkage of the nanospheres B is 18-25% at the same conditions. The nanospheres A are less flexible and soft as compared to the nanospheres B. Additionally, an ability of the PMMA nanoparticles fabricated in the water-acetone dispersion medium to form the ordered opal structures is demonstrated to be the similar to the nanospheres B.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Atuchin V. V., Aleksandrovsky A. S., Bazarov B. G., Bazarova J. G., Chimitova, Olga D., Denisenko, Yuriy G., Gavrilova T. A., Krylov A. S., Maximovskiy, Eugene A., Molokeev M. S., Oreshonkov A. S., Pugachev, Alexey M., Surovtsev, Nikolay V.
Заглавие : Exploration of structural, vibrational and spectroscopic properties of self-activated orthorhombic double molybdate RbEu(MoO4)2 with isolated MoO4 units
Коллективы : RFBR [16-52-48010, 17-52-53031, 18-03-00557]; Ministry of Science and Higher Education of the Russian Federation [0339-2016-0007]; Act 211 Government of the Russian Federation [02.A03.21.0011]; Ministry of Education and Science of the Russian Federation [4.1346.2017/4.6]
Место публикации : J. Alloy. Compd. - 2019. - Vol. 785. - P.692-697. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2019.01.013. - ISSN 1873-4669(eISSN)
Примечания : Cited References: 42. - The reported study was funded by RFBR according to research projects 16-52-48010, 17-52-53031 and 18-03-00557. Besides, this study was supported by the Ministry of Science and Higher Education of the Russian Federation (project 0339-2016-0007). The work was supported by Act 211 Government of the Russian Federation, contract No 02.A03.21.0011. Additionally, the work was partially supported by the Ministry of Education and Science of the Russian Federation (4.1346.2017/4.6).
Предметные рубрики: MORPHOLOGY-CONTROLLED SYNTHESIS
LUMINESCENCE PROPERTIES
Ключевые слова (''Своб.индексиров.''): rubidium europium molybdate--solid state reaction--rietveld refinement--dsc--raman luminescence
Аннотация: RbEu(MoO4)2 is synthesized by the two-step solid state reaction method. The crystal structure of RbEu(MoO4)2 is defined by Rietveld analysis in space group Pbcn with cell parameters a = 5.13502(5), b = 18.8581(2) and c = 8.12849(7) Å, V = 787.13(1) Å3, Z = 4 (RB = 0.86%). This molybdate possesses its phase transition at 817 K and melts at 1250 K. The Raman spectra were measured with the excitation at λ = 1064 and 514.5 nm. The photoluminescence spectrum is evaluated under the excitation at 514.5 nm. The absolute domination of hypersensitive 5D0→7F2 transition is observed. The ultranarrow 5D0→7F0 transition in RbEu(MoO4)2 is positioned at 580.2 nm being 0.2 nm blue shifted, with respect to that in Eu2(MoO4)3.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Menzyanova, Natalia G., Pyatina, Svetlana V., Nikolaeva, Elena D., Shabanov A. V., Nemtsev I. V., Stolyarov D. P., Dryganov, Dmitry B., Sakhnov, Eugene V., Vinokurova, Daria A., Shishatskaya, Ekaterina I.
Заглавие : Morphological aspects of monocyte/macrophage polarization on biopolymer scaffolds in atherosclerosis patients
Место публикации : J. Biotechnol. Biomater. - 2018. - Vol. 8, Is. 3. - Ст.1000284. - ISSN 2155-952X, DOI 10.4172/2155-952X.1000284
Примечания : Cited References: 67. - The study was supported by the State budget allocated to the fundamental research at the Russian Academy of Sciences (project No 01201351505).
Ключевые слова (''Своб.индексиров.''): monocytes--macrophages--cell morphology--polyhydroxyalkanoates--pha--copolymers--atherosclerosis--intravascular stenting
Аннотация: The morphotypes of human macrophages (MPh) were studied in the culture on nano-structured substrates, made from polyhydroxyalcanoates (PHAs) of various monomer compositions, prepared by casting polymer solutions on a defatted glass and followed by the solvent evaporation. Its surface relief, being further in direct contact with human cells in vitro was analyzed by AFM and SEM scanning. It was shown, that the features of micro/nano relief depend on the monomeric composition of polymer substrates. Monocytes (MNs) of patients with atherosclerosis and cardiac ischemia undergoing stenting and conventional anti-atherosclerotic therapy were harvested prior to and after stenting. After isolation MNs were cultured and transformed into MPh in direct contact with biopolymer culture substrates with different monomer composition and Nano-reliefs in comparison with culture plastic. Sub-populations of cells with characteristic morphology in each phenotypic class were described and their ratios for five samples of polymers were counted as an intermediate result in the development of “smart” material for blood vessel recovery. The results obtained allow us to assume that the processes of MPh differentiation and polarization in vitro depend not only on the features of the micro/nano relief of biopolymer substrates but also on the initial state of MNs in vivo and the general response of patients.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Зосько Н. А., Кенова Т. А., Александровский, Александр Сергеевич, Жижаев А. М., Таран О. П.
Заглавие : Синтез и фотоэлектрокаталитическая активность анодных наноструктурированных TiO2 пленок
Коллективы : [02872021-0023]
Место публикации : Журн. СФУ. Химия. - 2021. - Т. 14, № 3. - С. 396-405. - ISSN 1998-2836, DOI 10.17516/1998-2836-0249; J. Sib. Fed. Univ. Chem. - ISSN 2313-6049(eISSN)
Примечания : Библиогр.: 25. - Работа выполнена в рамках государственного задания ФИЦ КНЦ СО РАН (проект 0287-2021-0023) с использованием оборудования Красноярского регионального центра коллективного пользования ФИЦ КНЦ СО РАН. Авторы выражают признательность Н. Г. Максимову за снятие диффузных спектров отражения и В. Ф. Шабанову за плодотворную дискуссию
Аннотация: Методом электрохимического окисления получены наноструктурированные пленки диоксида титана, исследовано влияние напряжения анодирования на морфологию поверхности, оптические и фотоэлектрокаталитические характеристики полученных нанотрубок. Показано, что напряжение анодирования оказывает существенное влияние на структуру нанопленок и, соответственно, на их фотоэлектрокаталитическую активность. Методом катодного осаждения Cu2O на анодированный TiO2 получен фотоанод с гетеропереходом. Установлено, что фотоэлектроактивность такого анода при потенциале 1В (отн. Ag/AgCl/3,5MKCl) на 15% выше, чем активность исходной наноструктурированной TiO2 пленки.Nanostructured titanium dioxide films were prepared by electrochemical oxidation technique, anodization voltage effect on structure morphology, optical and photoelectrocatalytic performances of the nanotubes were studied. The anodization voltage is shown to significantly affect structure of nanofilms and, accordingly, their photoelectrocatalytic activity. An active heterojunction photoanode was synthesised with electrode position of Cu2O onanodized TiO2. The anode photoelectroact ivity under bias 1V (Ag/AgCl/3,5M KCl) is found to be 15 % higher than that of the original nanostructured TiO2 film.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Edelman I. S., Ivantsov R. D., Lin C. -R., Zharkov S. M., Velikanov D. A., Molokeev M. S., Zeer G. M., Chen Y. -Z., Spivakov A. A.
Заглавие : Evolution of morphology and magnetic properties of α-Fe2−xCrxO3 nanoparticles in dependence on Cr concentration
Место публикации : J. Magn. Magn. Mater. - 2022. - Vol. 564. - Ст.170101. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2022.170101
Примечания : Cited References: 69. - The work was supported financially by the Russian Foundation for Basic Research, Grant № 19-52-52002 and Ministry of Science and Technology of Taiwan, Grants MOST № 108-2923-M-153-001-MY3, № 110-2811-M-153-001 and № 110-2112-M-153-005. The support was obtained also from the Joint Scientific Center of the Siberian Federal University supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation, where the electron microscopy studies were carried out
Аннотация: Hematite, α-Fe2O3, one of the most widely studied magnetic compounds known to mankind since ancient times, has amazing properties and continues to puzzle researchers to this day. In this work, we found exceptionally strong changes in the morphology and magnetic properties of hematite nanoparticles upon doping with rather low concentrations of chromium. Nanoparticles α-Fe2−xCrxO3 with x varied from zero to 0.15 were prepared by solvothermal method using FeCl3·6H2O, CrCl3·6H2O, and 1,2-diaminopropane, (CH2)3(NH2)2, as precursors and temperature 180 °C for 6 h. The X-ray diffraction data showed the presence of only one crystal phase α-Fe2O3 for all x meanings with growing average crystalline size as the x increases. For the parent α-Fe2O3 powdered samples, the transmission electron microscopy revealed very long narrow nanorods with rounded ends that transform into spindles of increasing volume and cross section diameter as the Cr concentration increases. Vibrating sample magnetometry (VSM) and magnetic circular dichroism (MCD) study of the nanoparticles behavior in dependences on temperature and magnetic field revealed many unusual peculiarities. Among them there are strong increase of NPs magnetization with x increase (usually opposite picture is observed), the Morin transition temperature TM dependence on magnetic field, VSM sees the Morin transition in samples with small x only while MCD – in all samples, magnetization field dependences also are different when measured with VSM and MCD, and so on. Qualitative considerations were proposed to explain the observed phenomena.
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17.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Lukyanenko A. V., Tarasov A. S., Yakovlev I. A., Varnakov S. N.
Заглавие : Effect of synthesis conditions and buffer layers on morphology and phase formation during the growth of an epitaxial Mn5Ge3 film on Si(111)
Коллективы : Российская академия наук, Физико-технический институт им. Е.К. Завойского ФИЦ Казанского научного центра РАН, Казанский (Приволжский) федеральный университет, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : VIII Euro-Asian symposium "Trends in magnetism" (EASTMAG-2022): Book of abstracts/ program com. S. G. Ovchinnikov [et al.]. - 2022. - Vol. 1, Sect.: Spintronics and magnetic nanostructures. - Ст.A.P22. - P.135-136. - ISBN 978-5-94469-051-7
Примечания : Cited References: 8. - Support by Krasnoyarsk Regional Fund of Science is acknowledged
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Иванова, Оксана Станиславовна, Великанов, Дмитрий Анатольевич, Диденко О. Н., Зайковский В. И.
Заглавие : Магнитные свойства и морфология наночастиц феррита марганца в стекле
Место публикации : Журнал Сибирского федерального университета. Серия: Математика и физика. - Красноярск: Федеральное государственное автономное образовательное учреждение высшего образования Сибирский федеральный университет, 2011. - Т. 4, № 4. - С. 470-478. - ISSN 1997-1397
УДК : 537.622
Предметные рубрики:
Ключевые слова (''Своб.индексиров.''): magnetic properties--manganese ferrite nanoparticles--magnetization temperature depen- dence--магнитные свойства--наночастицы феррита марганца--температурная зависимость намагниченности
Аннотация: Работа посвящена сравнительному исследованию структуры и магнитных свойств стекол, ак- тивированных Fe и Mn, в которых при термообработках формируются наночастицы феррита марганца. Морфология наночастиц исследована с помощью электронной микроскопии высокого разрешения. Полевые и температурные зависимости намагниченности исследованы в интервале температур 1,8-300 K в полях до 5 T. Показано что, магнитные свойства стекла определяются морфологией наночастиц.The paper is dedicated to the comparative investigation of the magnetic properties and structure of oxide glasses doped with Fe and Mn. Manganese ferrite nanoparticles arise in the glasses as a result of an additional thermal treatment. The particles morphology is investigated with the high resolution electron microscopy. The glasses magnetization is investigated in the temperature interval 1,8-300 K in mag- netic field up to 5 T. The glasses magnetic properties are shown to be governed by the nanoparticles morphology.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Shalygina T. A., Rudenko M. S., Nemtsev I. V., Parfenov V. A., Voronina S. Yu.
Заглавие : Plasma-chemical method of silicon carbide modification to obtain particles with controlled surface morphology
Место публикации : Tech. Phys. Lett. - 2022. - Vol. 48, Is. 2. - P.57-60. - ISSN 10637850 (ISSN), DOI 10.21883/TPL.2022.02.53582.19042. - ISSN 10906533 (eISSN)
Примечания : Cited References: 9. - This study was conducted under state assignment from the Ministry of Science and Higher Education of the Russian Federation for the ”Smart Materials and Structures“ research laboratory (project No. FEFE-2020-0015 ”Development of Multipurpose Smart Materials and Structures Based on Modified Polymer Composite Materials Remaining Functional in Extreme Conditions“)
Аннотация: A plasma-chemical method for the modification of silicon carbide particles is presented, which makes it possible to obtain particles with a controlled surface morphology. The variable parameter of particle processing was the ratio of the fraction of plasma-forming (Ar) and additional (H) gases. It was shown that at Ar/H = 100/0, the formation of a carbon shell is observed; at Ar/H ratios of 91/9 and 84/16, the particles are characterized by a carbon shell decorated with silicon nanoparticles or nanowires, respectively. The modified particles were analyzed using scanning electron microscopy and Raman spectroscopy.
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20.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ivanova O. S., Edelman I. S., Svetlitsky E. S., Sokolov A. Е., Zharkov S. M., Petrov D. A., Sukhachev A. L., Toropova E. S., Chun-Rong Lin, Ying-Zhen Chen
Заглавие : Core-shell magnetite nanoparticles: morphology, magnetic properties, organic dyes adsorption
Коллективы : "Functional materials", International conference, Крымский федеральный университет имени В.И. Вернадского
Место публикации : Ovchinnikov S. G. International conference "Functional materials": book of abstracts/ ed. V. N. Berzhansky ; org. com. S. G. Ovchinnikov [et al.]. - Simferopol, 2023. - P.114
Примечания : Cited References: 1. - РФН № 23-22-10025
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