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A Novel Magnetic Transition in Magnetite Fe3O4 between 12-16 GPa [Text] / Y. Ding, D. Haskel [et al.] // Phys. Rev. Lett. - 2008. - Vol. 100. - P045508

Доп.точки доступа:
Ding, Y.; Haskel, D.; Ovchinnikov, S.G.; Tseng, Y.-Ch.; Orlov, Yu.S.; Mao, N-K.
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Babkin, E. V.
Characteristics of magnetite magnetoresistance / E. V. Babkin, N. I. Kiselev, V. G. Pynko // Fiz. Tverd. Tela. - 1995. - Vol. 37, Is. 11. - P. 3547-3549. - Cited References: 5 . - ISSN 0367-3294

РУБ Physics, Condensed Matter

WOS
Доп.точки доступа:
Kiselev, N. I.; Pyn'ko, V. G.; Пынько, Виталий Григорьевич
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BABKIN, E. V.
ELECTRIC-FIELD EFFECT ON THE MAGNETIC-ANISOTROPY OF MAGNETITE / E. V. BABKIN, N. G. CHERKUNOVA // Fiz. Tverd. Tela. - 1984. - Vol. 26, Is. 6. - P. 1818-1822. - Cited References: 14 . - ISSN 0367-3294

РУБ Physics, Condensed Matter

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Доп.точки доступа:
CHERKUNOVA, N. G.
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BABKIN, E. V.
INVESTIGATION OF QUANTUM SIZE EFFECT IN MAGNETITE FILMS / E. V. BABKIN, N. G. CHERKUNOVA, S. G. OVCHINNIKOV // Solid State Commun. - 1984. - Vol. 52, Is. 8. - P. 735-738, DOI 10.1016/0038-1098(84)90400-9. - Cited References: 8 . - ISSN 0038-1098

РУБ Physics, Condensed Matter

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Scopus
Держатели документа:
L.V. Kirensky Institute of Physics, Siberian Department, the USSR Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
ИФ СО РАН
Доп.точки доступа:
CHERKUNOVA, N. G.; OVCHINNIKOV, S. G.; Овчинников, Сергей Геннадьевич
}
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Barinov, G. I.
Influence of high-pressure thermal-treatment on the phase compound and phase-transformation kinetics of a system magnetite-wustite / G. I. Barinov, Y. V. Babkin // Izvestiya vysshikh uchebnykh zavedenii Fizika. - 1990. - Vol. 33, Is. 5. - P. 95-96 ; Russian Physics Journal ; Известия высших учебных заведений. Физика. - Cited References: 4 . - ISSN 0021-3411

РУБ Physics, Multidisciplinary

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Доп.точки доступа:
Babkin, Y. V.

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Characterization and magnetic properties study for magnetite nanoparticles obtained by pulsed laser ablation in water / V. A. Svetlichnyi [et al.] // Appl. Phys. A. - 2017. - Vol. 123, Is. 12. - Ст. 763, DOI 10.1007/s00339-017-1390-7. - Cited References: 40. - This work was conducted as a government task of the Ministry of Education and Science of the Russian Federation, Project Number 3.9604.2017/8.9. . - ISSN 0947-8396
Кл.слова (ненормированные):
Magnetite -- Pulsed laser ablation -- Nanoparticles -- Dispersion
Аннотация: Magnetite (Fe3O4) nanoparticles of 1–10 nm (with the maximum at 2 nm) were obtained via pulsed laser ablation of iron target in water in form of a stable dispersion without addition of surfactants and stabilizers. The structure of the material obtained was investigated using transmission electron microscopy, scanning electron microscopy, and Brunauer–Emmett–Teller methods. To investigate the composition of the particles in the sample, such methods as Fourier transform infrared spectroscopy, Raman spectroscopy, differential scanning calorimetry, and X-ray diffraction, were applied. Magnetite phase was found to be sufficiently pure, it was not contaminated by other iron oxide phases and contained not more than 0.5% of metallic iron in form of large particles. The study of the magnetic properties of the magnetite nanoparticles obtained has shown that they exhibit ferrimagnetic behavior at room temperature with the paramagnetic contribution explained by the presence of fine superparamagnetic particles.

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Держатели документа:
Tomsk State University, Lenina ave., 36, Tomsk, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50, bld. 38, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Svetlichnyi, V. A.; Shabalina, A. V.; Lapin, I. N.; Goncharova, D. A.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Sokolov, A. Е.; Соколов, Алексей Эдуардович
}
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Characterization and magnetotransport properties of textured Fe3O4 films / A. S. Tarasov [et al.] // VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016) : abstracts / ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk : KIP RAS SB, 2016. - Ст. O10.21. - P. 465. - References: 2. - This work was partially supported by RFBR project no. 14-02-00234, the RAS «Far East» Program No 0262-2015-0057 . - ISBN 978-5-904603-06-9
Кл.слова (ненормированные):
magnetite -- texture film -- spin-dependent transport

Доп.точки доступа:
Tarasov, A. S.; Тарасов, Антон Сергеевич; Rautskii, M. V.; Рауцкий, Михаил Владимирович; Lukyanenko, A. V.; Лукьяненко, Анна Витальевна; Volochaev, M. N.; Волочаев, Михаил Николаевич; Eremin, E. V.; Еремин, Евгений Владимирович; Korobtsov, V .V.; Коробцов, Владимир Викторович; Balashev, V. V.; Балашев В. В.; Vikulov, V. A.; Solovyov, L. A.; Соловьев, Леонид Александрович; Volkov, N. V.; Волков, Никита Валентинович; Euro-Asian Symposium "Trends in MAGnetism"(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); "Trends in MAGnetism", Euro-Asian Symposium(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); Институт физики им. Л.В. Киренского Сибирского отделения РАН

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Core-shell exchange interaction effect in the approach to magnetic saturation of a magnetite-like nanoparticle / S. V. Komogortsev, S. V. Stolyar, R. S. Iskhakov, A. A. Mohov // V International Baltic Conference on Magnetism. IBCM : Book of abstracts. - 2023. - P. 40

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS
Federal Research Center KSC SB RAS

Доп.точки доступа:
Komogortsev, S. V.; Комогорцев, Сергей Викторович; Stolyar, S. V.; Столяр, Сергей Викторович; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Mohov, A. A.; International Baltic Conference on Magnetism(5 ; 2023 ; Aug. 20-24 ; Svetlogorsk, Russia); Балтийский федеральный университет им. И. Канта
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Core-shell magnetite nanoparticles: morphology, magnetic properties, organic dyes adsorption / O. S. Ivanova, I. S. Edelman, E. S. Svetlitsky [et al.] // International conference "Functional materials" : book of abstracts / ed. V. N. Berzhansky ; org. com. S. G. Ovchinnikov [et al.]. - Simferopol, 2023. - P. 114. - Cited References: 1. - РФН № 23-22-10025

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Держатели документа:
Kirensky Institute of Physics, FRC KSC SB RAS,
Siberian Federal University
National Pingtung University, 90003, Pingtung City, Taiwan

Доп.точки доступа:
Berzhansky, V. N. \ed.\; Бержанский, Владимир Наумович; Ovchinnikov, S. G. \org. com.\; Овчинников, Сергей Геннадьевич; Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S. (Edel'man, I. S.); Эдельман, Ирина Самсоновна; Svetlitsky, E. S.; Sokolov, A. Е.; Соколов, Алексей Эдуардович; Zharkov, S. M.; Жарков, Сергей Михайлович; Petrov, D. A.; Петров, Дмитрий Анатольевич; Sukhachev, A. L.; Сухачев, Александр Леонидович; Toropova, E. S.; Chun-Rong Lin; Ying-Zhen Chen; "Functional materials", International conference(2023 ; Oct. 2-6 ; Crimea, Foros); Крымский федеральный университет имени В.И. Вернадского
}
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10.

Core–shell Fe3O4@C nanoparticles for the organic dye adsorption and targeted magneto-mechanical destruction of Ehrlich ascites carcinoma cells / O. S. Ivanova, I. S. Edelman, Ch.-R. Lin [et al.] // Materials. - 2023. - Vol. 16, Is. 1. - Ст. 23, DOI 10.3390/ma16010023. - Cited References: 65. - This research was funded partly by the Ministry of Science and Higher Education of the Russian Federation, project FWES-2021-0035. C.-R.L., Y.-Z.C. and A.A.S. thank the National Science and Technology Council of Taiwan for the financial support, Grants NSTC № 108-2923-M-153-001-MY3 and № 110-2112-M-153-005-. Magnetic investigations were carried out in the Center for Collective Use of the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” . - ISSN 1996-1944
Кл.слова (ненормированные):
magnetite nanoparticles -- adsorption -- organic dyes -- aptamers -- magnetically induced cell destruction
Аннотация: The morphology, structure, and magnetic properties of Fe3O4 and Fe3O4@C nanoparticles, as well their effectiveness for organic dye adsorption and targeted destruction of carcinoma cells, were studied. The nanoparticles exhibited a high magnetic saturation value (79.4 and 63.8 emu/g, correspondingly) to facilitate magnetic separation. It has been shown that surface properties play a key role in the adsorption process. Both types of organic dyes—cationic (Rhodomine C) and anionic (Congo Red and Eosine)—were well adsorbed by the Fe3O4 nanoparticles’ surface, and the adsorption process was described by the polymolecular adsorption model with a maximum adsorption capacity of 58, 22, and 14 mg/g for Congo Red, Eosine, and Rhodomine C, correspondingly. In this case, the kinetic data were described well by the pseudo-first-order model. Carbon-coated particles selectively adsorbed only cationic dyes, and the adsorption process for Methylene Blue was described by the Freundlich model, with a maximum adsorption capacity of 14 mg/g. For the case of Rhodomine C, the adsorption isotherm has a polymolecular character with a maximum adsorption capacity of 34 mg/g. To realize the targeted destruction of the carcinoma cells, the Fe3O4@C nanoparticles were functionalized with aptamers, and an experiment on the Ehrlich ascetic carcinoma cells’ destruction was carried out successively using a low-frequency alternating magnetic field. The number of cells destroyed as a result of their interaction with Fe3O4@C nanoparticles in an alternating magnetic field was 27%, compared with the number of naturally dead control cells of 6%.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC Siberian Branch, Russian Academy of Sciences, Krasnoyarsk 660036, Russia
Institute of Engineering Physics and Radioelectronics, Siberian Federal University, Krasnoyarsk 660041, Russia
Department of Applied Physics, National Pingtung University, Pingtung City 90003, Taiwan
Laboratory of Biomolecular and Medical Technologies, Krasnoyarsk State Medical University Named after Prof. V.F. Voino-Yasenetsky, Krasnoyarsk 660022, Russia
Laboratory for Digital Controlled Drugs and Theranostics, Federal Research Center KSC Siberian Branch, Russian Academy of Sciences, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Lin, Chun-Rong; Svetlitsky, E. S.; Светлицкий, Евгений Сергеевич; Sokolov, A. Е.; Соколов, Алексей Эдуардович; Lukyanenko, Kirill A.; Sukhachev, A. L.; Сухачев, Александр Леонидович; Shestakov, N. P.; Шестаков, Николай Петрович; Chen, Ying-Zhen; Spivakov, Aleksandr A.
}
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11.

Crystal texture-dependent magnetic and magnetotransport properties of half-metallic Fe3O4 films grown on oxidized Si substrates by reactive deposition / V. V. Balashev [et al.] // J. Alloys Compd. - 2020. - Vol. 815. - Ст. 152398, DOI 10.1016/j.jallcom.2019.152398. - Cited References: 58. - his work is supported in part by the Russian Ministry of Science and Higher Education under the state tasks ( 3.5178.2017/8.9 and 3.4956.2017 ), by Act 211 of the Government of the Russian Federation (contract No. 02.A03.21.0011 ) and by the Comprehensive Program of Basic Research of the Far Eastern Branch of the Russian Academy of Sciences “Far East” 2018–2020 № 18-3-022 ( 0226-18-0031 ). . - ISSN 0925-8388
Кл.слова (ненормированные):
Magnetite -- Crystal texture -- Reactive deposition -- Magnetoresistance -- Magnetic saturation -- FORC
Аннотация: Nanocrystalline magnetite (Fe3O4) films with various preferred crystallite orientations were grown on oxidized silicon surface by reactive iron deposition in an oxygen atmosphere. Depending on the partial pressure of oxygen (PO2), the evolution of the structural, magnetic, and magnetotransport properties of the grown films was investigated. We found that the growth of films containing only the Fe3O4 phase occurs in a certain PO2 range, and the magnetite crystallites may have (311) or (110) preferred orientation. It was revealed that films with (311) and (110) textures have a column structure. An increase in the PO2 leads to a structure transformation from (311) to (110) texture with larger crystallites. A film with (110) texture showed higher values of saturation magnetization, magnetoresistance and spin polarization. The analysis of approach to magnetic saturation revealed that the local magnetic anisotropy of crystallites in textured films is much higher than the anisotropy of bulk magnetite due to the large surface contribution. The FORC diagram method in combination with the approach to magnetic saturation proved the existence of the exchange coupling between large and small grains. Our results open the reliable route for crystal texture-depending manipulation of functional properties of thin magnetite films for advanced spintronic applications.

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Держатели документа:
School of Natural Sciences, Far Eastern Federal University, Vladivostok, Russian Federation
Institute of Automation and Control Processes, FEB RAS, Vladivostok, Russian Federation
Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Siberian State Aerospace University, Krasnoyarsk, Russian Federation
National Research South Ural State University, Chelyabinsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Balashev, V. V.; Ermakov, K. S.; Samardak, A. Y.; Ognev, A. V.; Samardak, A. S.; Komogortsev, S. V.; Комогорцев, Сергей Викторович; Volochaev, M. N.; Волочаев, Михаил Николаевич; Tarasov, A. S.; Тарасов, Антон Сергеевич; Korobtsov, V. V.
}
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12.

Day plots of bacterial magnetite from sediments of Lake Shira (Khakassia, Russia) / S. V. Semenov [et al.] // VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016) : abstracts / ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk : KIP RAS SB, 2016. - Ст. P12.1. - P. 557. - References: 3. - The work was supported by Russian Foundation for Basic Research and Krasnoyarsk Regional Scientific Foundation, Grant No. 15-45-04272 . - ISBN 978-5-904603-06-9
Кл.слова (ненормированные):
nanoparticles -- magnetic hysteresis -- bacterial magnetite

Доп.точки доступа:
Semenov, S. V.; Семёнов, Сергей Васильевич; Balaev, D. A.; Балаев, Дмитрий Александрович; Shaikhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Rogozin, D. Yu.; Рогозин, Денис Юрьевич; Euro-Asian Symposium "Trends in MAGnetism"(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); "Trends in MAGnetism", Euro-Asian Symposium(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); Институт физики им. Л.В. Киренского Сибирского отделения РАН

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13.

    Day plots of bacterial magnetite from sediments of shira lake (Khakassia, Russia) / S. V. Semenov [et al.] // J. Sib. Fed. Univ. Math. Phys. - 2017. - Vol. 10, Is. 2. - P. 252-256 ; Журн. СФУ. Сер. "Математика и физика", DOI 10.17516/1997-1397-2017-10-2-252-256. - Cited References: 4 . - ISSN 1997-1397
   Перевод заглавия: Графики Дэя для бактериального магнетита из донных отложений озера Шира (Хакасия, Россия)
Кл.слова (ненормированные):
Nanoparticles -- Magnetic hysteresis -- Bacterial magnetite -- наночастицы -- магнитный гистерезис -- бактериальный магнетит
Аннотация: The domain state of magnetite detected in sediments of Shira lake (Khakassia, Russia) was examined by means of magnetic hysteresis. Analysis of experimental data obtained on samples from different parts of bottom sediment cores in terms of Day plots allowed us to conclude that magnetite particles are in the pseudo-single-domain state. This indicates respectively small size of magnetite particles (˂ 100 nm) and reveals their bacterial origin. Biogenic magnetite buried in the bottom sediments can indicate the climatic changes in the Shira lake level in the Late Holocene.
Исследовано доменное состояние магнетита, обнаруженного в донных отложениях озера Шира (Хакасия, Россия). Из анализа экспериментальных данных по намагниченности образцов с разных участков керна донных отложений, а также на основе графиков Дэя сделан вывод, что частицы магнетита находятся в псевдооднодоменном состоянии. Это указывает на малый размер частиц магнетита (˂ 100 nm) и подтверждает их бактериальное происхождение. Биогенный магнетит, содержащийся в донных отложениях, может служить индикатором климатических изменений в уровне озера Шира в позднем голоцене.

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Держатели документа:
Kirensky Institute of Physics SB RAS, Akademgorodok, 50/38, Krasnoyarsk, Russian Federation
Siberian Federal University, Svobodny, 79, Krasnoyarsk, Russian Federation
Institute of Biophysics SB RAS, Akademgorodok, 50/50, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Semenov, S. V.; Семёнов, Сергей Васильевич; Balaev, D. A.; Балаев, Дмитрий Александрович; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Rogozin, D. Y.

}
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14.

Dimethylsulfoxide as a media for one-stage synthesis of the Fe3O4-based ferrofluids with a controllable size distribution / V. L. Kirillov [et al.] // Mater. Chem. Phys. - 2019. - Vol. 225. - P. 292-297, DOI 10.1016/j.matchemphys.2019.01.003. - Cited References: 36. - This work was supported by the Russian Science Foundation , project no. 17-12-01111. . - ISSN 0254-0584
Кл.слова (ненормированные):
Ferrofluid -- Magnetite nanoparticles -- One-step synthesis -- Superparamagnetic nanoparticles -- Ferromagnetic resonance
Аннотация: The ultrafine (d = 4 nm) magnetite ferrofluid with a narrow nanoparticle size distribution has been synthesized in one stage at room temperature from a solution of iron(II) and (III) chlorides in dimethylsulfoxide (DMSO) with the propylene epoxide admixture. This is the first example of obtaining a stable concentrated ultrafine magnetite/DMSO ferrofluid at room temperature. X-ray diffraction, transmission electron microscopy, ferromagnetic resonance, Mossbauer spectroscopy, and magnetostatic study have been used to elucidate the role of DMSO and the H2O/DMSO ratio in the formation of a stable colloid with a desired nanoparticle size. The initial stages of the magnetite nanoparticles formation have been investigated by the ferromagnetic resonance technique.

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Держатели документа:
Boreskov Institute of Catalysis, Russian Academy of Sciences, Siberian Branch, Novosibirsk, 630090, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Kirillov, V. L.; Yakushkin, S. S.; Balaev, D. A.; Балаев, Дмитрий Александрович; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Semenov, S. V.; Семёнов, Сергей Васильевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Bayukov, O. A.; Баюков, Олег Артемьевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Yatsenko, D. A.; Martyanov, O. N.
}
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15.

Dressability of abagas hematite-magnetite ores / V. I. Kilin [et al.] // J. Min. Sci. - 2012. - Vol. 48, Is. 2. - P. 363-368, DOI 10.1134/S1062739148020189. - Cited References: 3 . - ISSN 1062-7391
Кл.слова (ненормированные):
magnetite -- hematite -- ilvaite -- dry -- wet -- high-gradient magnetic separation -- jigging
Аннотация: A number of magnetic separation processes are used to study preparability of two main hematite-magnetite and magnetite-muscovite ore types extacted it the Abagas iron ore deposit. The dry magnetic separation results were judged as acceptable for the rough processing stage, while the products of the wet magnetic separation were the high-grade iron ore concentrates. The two-stage beneficiation tests on complex hematite-magnetite ores demonstrated much higher cumulative iron recovery from the test ore.

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Публикация на русском языке Изучение обогатимости гематит-магнетитовых руд Абагасского месторождения [Текст] / В. И. Килин [и др.] // Физ.-техн. проблемы разраб. полез. ископаемых. - Новосибирск : Изд-во СО РАН, 2012. - № 2. - С. 160-166

Держатели документа:
[Kilin, V. I.] EVRAZRUDA, Novokuznetsk 654027, Russia
[Yakubailik, E. K.
Kostenenko, L. P.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Ganzhenko, I. M.] Siberian Fed Univ, Krasnoyarsk 660041, Russia

Доп.точки доступа:
Kilin, V. I.; Килин, В. И.; Yakubailik, E. K.; Якубайлик, Эдуард Константинович; Kostenenko, L. P.; Костененко, Лариса Павловна; Ganzhenko, I. M.
}
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16.

DROKIN, N. A.
PHOTOCONDUCTIVITY IN TIN-DOPED MAGNETITE / N. A. DROKIN, E. Y. AKSENOVA, Y. A. MAMALUI // Fiz. Tverd. Tela. - 1984. - Vol. 26, Is. 6. - P. 1837-1838. - Cited References: 5 . - ISSN 0367-3294

РУБ Physics, Condensed Matter

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Доп.точки доступа:
AKSENOVA, E. Y.; MAMALUI, Y. A.
}
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17.

Effect of surfactants on the structure, phase composition, and magnetic properties of FexSy nanoparticles synthesized by thermal decomposition / R. D. Ivantsov, C.-R. Lin, Y.-Z. Chen [et al.] // Nanobiotechnol. Rep. - 2022. - Vol. 17, Is. 3. - P. 336-344, DOI 10.1134/S2635167622030089. - Cited References: 27. - This study was supported by the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project no. 19-42-240005: “Features of the Electronic Structure, Magnetic Properties, and Optical Excitations in Nanocrystals of Multifunctional Magnetic Chalcogenides Fe3S4 and FeSe” and the Russian Foundation for Basic Research and the Ministry of Science and Technology of Taiwan, joint projects nos. 19-52-52002 and 109-2112-M-153-003 and 108-2923-M-153-001-MY3. - The electron-microscopy study was carried out at the Laboratory of Electron Microscopy of the Center for Collective Use of the Siberian Federal University within the state assignment of the Ministry of Science and Higher Education of the Russian Federation (research code FSRZ-2020-0011). The magnetic measurements were carried out on a vibrating sample magnetometer at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences . - ISSN 2635-1676
Кл.слова (ненормированные):
Agglomeration -- Crystal impurities -- Fourier transform infrared spectroscopy -- High resolution transmission electron microscopy -- Magnetic properties -- Magnetite -- Magnetization -- Nanomagnetics -- Sulfur compounds -- Synthesis (chemical) -- Thermogravimetric analysis -- Thermolysis -- Electron diffraction analysis -- Greigites -- Hexadecylamine -- Inverse spinel structures -- Iron sulfide -- Isostructural -- Octadecyl amine -- Organic shells -- Structures phase -- Synthesised -- Surface active agents
Аннотация: The effect of surfactants on the structure, morphology, and magnetic properties of FexSy iron-sulfide nanoparticles synthesized by thermal decomposition is studied. Oleylamine, hexadecylamine, and octadecylamine are used as surfactants. It is established by X-ray and electron-diffraction analysis combined with Mossbauer spectroscopy that, in samples 1 and 2 prepared using oleylamine and hexadecylamine, respectively, the Fe3S4 greigite phase dominates, with an inverse spinel structure isostructural to the iron oxide Fe3O4 magnetite with minor Fe9S11 impurities. Deviations in the distribution of iron cations over the tetrahedral and octahedral sites relative to the bulk greigite crystals are observed. The nanoparticles synthesized using octadecylamine (sample 3) are found to be multiphase with a greigite fraction of ~20%. In all three cases, as showed the results of transmission electron microscopy and Fourier transform infrared spectroscopy together with thermogravimetry analysis, the magnetic nanoparticles have an organic shell chemically bonded to their magnetic core, which prevents the agglomeration of the particles. This shell is much more massive in samples 2 and 3. The magnetization values for samples 1 and 2 are similar to those of greigite nanoparticles reported in publications, while the magnetization of sample 3 is several times lower, in accordance with the greigite fraction in it. The combination of fairly high magnetization with a massive organic shell allows one to consider hexadecylamine to be a promising surfactant for the synthesis of iron-sulfide nanoparticles protected from external impact and agglomeration.

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Публикация на русском языке Влияние ПАВ на структуру, фазовый состав и магнитные свойства наночастиц FexSy, полученных методом термического разложения [Текст] / Р. Д. Иванцов, Ч. Р. Лин, Ю. Ж. Чэнь [и др.] // Рос. нанотехнол. - 2022. - Т. 17 № 3. - С. 358-367

Держатели документа:
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Department of Applied Physics, National Pingtung University, Pingtung City, 90003, Taiwan
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Lin, C. -R.; Chen, Y. -Z.; Ivanova, O. S.; Иванова, Оксана Станиславовна; Altunin, R. R.; Knyazev, Yu. V.; Князев, Юрий Владимирович; Molokeev, M. S.; Молокеев, Максим Сергеевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Shestakov, N. P.; Шестаков, Николай Петрович; Sukhachev, A. L.; Сухачев, Александр Леонидович; Edelman, I. S.; Эдельман, Ирина Самсоновна
}
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18.

Effects of modified magnetite nanoparticles on bacterial cells and enzyme reactions / L. S. Bondarenko, E. S. Kovel, K. A. Kydralieva [et al.] // Nanomaterials. - 2020. - Vol. 10, Is. 8. - Ст. 1499. - P. 1-20, DOI 10.3390/nano10081499. - Cited References: 83. - This research was funded by the Russian Foundation for Basic Research (#19-315-50048, #19-33-90149, and #18-29-19003) . - ISSN 2079-4991
Кл.слова (ненормированные):
Magnetite nanoparticles -- Humic acids-coated magnetite nanoparticles -- Silica-coated magnetite nanoparticles -- Zeta potential -- Hydrodynamic diameter -- Toxicity -- Bioluminescence -- Bacterial assay -- Enzymatic assay -- Oxidative stress -- Photobacterium phosphoreum -- NADH:FMN-oxidoreductase -- Luciferase
Аннотация: Current paper presents biological effects of magnetite nanoparticles (MNPs). Analyzing effects of MNP’ characteristics (zeta-potential and hydrodynamic diameters) on bacteria and their enzyme reactions was the main focus. Photobacterium phosphoreum and bacterial enzymatic reactions were chosen as bioassays. Three types of MNPs were under study: bare Fe3O4, Fe3O4 modified with 3-aminopropyltriethoxysilane (Fe3O4/APTES), and humic acids (Fe3O4/HA). Effects of the MNPs were studied at a low concentration range (< 2 mg/L) and attributed to availability and oxidative activity of Fe3+, high negative surface charge, and low hydrodynamic diameter of Fe3O4/HA, as well as higher Fe3+ content in suspensions of Fe3O4/HA. Low-concentration suspensions of bare Fe3O4 provided inhibitory effects in both bacterial and enzymatic bioassays, whereas the MNPs with modified surface (Fe3O4/APTES and Fe3O4/HA) did not affect the enzymatic activity. Under oxidative stress (i.e., in the solutions of model oxidizer, 1,4-benzoquinone), MNPs did not reveal antioxidant activity, moreover, Fe3O4/HA demonstrated additional inhibitory activity. The study contributes to the deeper understanding of a role of humic substances and silica in biogeochemical cycling of iron. Bioluminescence assays, cellular and enzymatic, can serve as convenient tools to evaluate bioavailability of Fe3+ in natural dispersions of iron-containing nanoparticles, e.g., magnetite, ferrihydrite, etc.

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Держатели документа:
Moscow Aviation Institute (National Research University), Moscow, 125993, Russian Federation
Institute of Physics SB RAS, FRC KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Institute of Biophysics SB RAS, FRC KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Institute of Problems of Chemical Physics RAS, Moscow Region, Chernogolovka, 142432, Russian Federation
University of Szeged, Szeged, H-6720, Hungary
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Bondarenko, L. S.; Kovel, E. S.; Ковель, Екатерина Сергеевна; Kydralieva, K. A.; Dzhardimalieva, G. I.; Illes, E.; Tombacz, E.; Kicheeva, A. G.; Kudryasheva, N. S.
}
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19.

Fe3O4/Au nanocomposites: Characterization and cytotoxicity effects in vitro / R. N. Yaroslavtsev, A. V. Tyumentseva, D. A. Velikanov [et al.] // Mater. Chem. Phys. - 2024. - Vol. 322. - Ст. 129524, DOI 10.1016/j.matchemphys.2024.129524. - Cited References: 44 . - ISSN 0254-0584. - ISSN 1879-3312
Кл.слова (ненормированные):
Magnetic nanoparticles -- Magnetite -- Gold nanoparticles -- Cytotoxicity
Аннотация: Magnetic nanocomposites containing iron oxide and gold components take great attention last years because of their relative biocompatibility and the ability to combine the magnetic properties of iron and the chemical bonding properties of gold for the possible drug delivery or diagnostics for various diseases. However, such particles have some toxicity to living cells, and the effect depends on many factors, including size, shape, the ratio of components in the composites, and the type of cells affected. And thus, the search for compositions and technologies for producing iron-gold particles with improved properties and reduced cytotoxicity remains relevant. The aim of the study was to synthesize and characterize Fe3O4/Au nanocomposites and evaluate their influence on living cells using the example of cell line HEK293. Fe3O4 nanoparticles (NPs) were synthesized by co-precipitation of Fe2+/Fe3+ water solution in alkaline conditions and then boiled with HAuCl4 in 0.1 M sodium citrate. The NPs properties were estimated by transmission electron microscopy (TEM), vibration magnetometry and ferromagnetic resonance (FMR). According to magnetometric measurements, nanoparticles are mainly in a superparamagnetic state. By fitting magnetization curves, the magnetic characteristics of nanoparticles were determined: saturation magnetization (59.3 emu/g) and magnetic anisotropy constant (K = 0.86·105 erg/cm3). The average particle size estimated from magnetic measurements was 8.7 nm. Considering the presence of a magnetically dead layer, this is in good agreement with the TEM results. The temperature dependence of the FMR linewidth was analyzed using two models. As a result, the parameters MSV and K/MS were determined. The models used showed good agreement. The values of the anisotropy constant (K = 1.06·105 erg/cm3) and the average particle size (6.8 nm) are estimated. The effect of the NPs on the HEK293 cells was studied by MTT-assay, flow cytometry and RT-PCR. The exposure with the NPs lead to a significant decrease of cell metabolic activity in HEK293 cell culture, but this effect was not accompanied by cell death. It was shown that the expression of antioxidant enzymes SOD1 and GPX1 was reduced at the mRNA stage. So the NPs synthesized may affect gene expression and metabolism of HEK293 cells, but this does not have fatal consequences for cell viability.

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Держатели документа:
Krasnoyarsk Science Center, Federal Research Center KSC SB RAS, Akademgorodok 50, Krasnoyarsk, 660036, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50, bld. 38, Krasnoyarsk, 660036, Russia

Доп.точки доступа:
Yaroslavtsev, R. N.; Ярославцев, Роман Николаевич; Tyumentseva, A.V.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Vazhenina, I. G.; Важенина, Ирина Георгиевна; Volochaev, M. N.; Волочаев, Михаил Николаевич; Stolyar, S. V.; Столяр, Сергей Викторович
}
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20.

Functionalized magnetite nanoparticles: Characterization, bioeffects, and role of reactive oxygen species in unicellular and enzymatic systems / A. G. Kicheeva, E. S. Sushko, L. S. Bondarenko [et al.] // Int. J. Mol. Sci. - 2023. - Vol. 24, Is. 2. - Ст. 1133, DOI 10.3390/ijms24021133. - Cited References: 125. - This research was funded by Russian Science Foundation, N 22-73-10222 . - ISSN 1661-6596. - ISSN 1422-0067
Кл.слова (ненормированные):
magnetite nanoparticles -- surface modification -- humic acids -- organosilane -- reactive oxygen species -- toxicity -- bioluminescence assay -- bacteria -- enzymes -- oxidative stress -- prooxidant -- ferroptosis
Аннотация: The current study evaluates the role of reactive oxygen species (ROS) in bioeffects of magnetite nanoparticles (MNPs), such as bare (Fe3O4), humic acids (Fe3O4-HA), and 3-aminopropyltriethoxysilane (Fe3O4-APTES) modified MNPs. Mössbauer spectroscopy was used to identify the local surrounding for Fe atom/ions and the depth of modification for MNPs. It was found that the Fe3O4-HA MNPs contain the smallest, whereas the Fe3O4-APTES MNPs contain the largest amount of Fe2+ ions. Bioluminescent cellular and enzymatic assays were applied to monitor the toxicity and anti-(pro-)oxidant activity of MNPs. The contents of ROS were determined by a chemiluminescence luminol assay evaluating the correlations with toxicity/anti-(pro-)oxidant coefficients. Toxic effects of modified MNPs were found at higher concentrations (>10−2 g/L); they were related to ROS storage in bacterial suspensions. MNPs stimulated ROS production by the bacteria in a wide concentration range (10−15–1 g/L). Under the conditions of model oxidative stress and higher concentrations of MNPs (>10−4 g/L), the bacterial bioassay revealed prooxidant activity of all three MNP types, with corresponding decay of ROS content. Bioluminescence enzymatic assay did not show any sensitivity to MNPs, with negligible change in ROS content. The results clearly indicate that cell-membrane processes are responsible for the bioeffects and bacterial ROS generation, confirming the ferroptosis phenomenon based on iron-initiated cell-membrane lipid peroxidation.

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Держатели документа:
Institute of Biophysics of Siberian Branch of Russian Academy of Sciences, Federal Research Center “Krasnoyarsk Science Center” of Siberian Branch of Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Institute of Physics of Siberian Branch of Russian Academy of Sciences, Federal Research Center “Krasnoyarsk Science Center” of Siberian Branch of Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Department of General Engineering, Moscow Aviation Institute, Moscow, 125993, Russian Federation
Department of Chemistry, Lomonosov Moscow State University, Moscow, 119991, Russian Federation
Sklifosovsky Research Institute for Emergency Medicine, Moscow, 129010, Russian Federation
Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences, Chernogolovka, 142432, Russian Federation
Institute for Polymers, Composites and Biomaterials, National Research Council of Italy, P.le Fermi, 1, Portici, 80055, Italy
Biophysics Department, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Kicheeva, A. G.; Sushko, E. S.; Сушко, Екатерина Сергеевна; Bondarenko, L. S.; Kydralieva, K. A.; Pankratov, D. A.; Tropskaya, N. S.; Dzeranov, A. A.; Dzhardimalieva, G. I.; Zarrelli, M.; Kudryasheva, N. S.
}
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