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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Abramova G. A., Boehm M., Roessli B., Raseh J., Petrakovskiy G. A., Velikanov D. A., Vorotynov A. M., Bovina A. F., Sokolov V. V.
Заглавие : Neutron diffraction measurements of the FexMn1-xS solid solutions
Коллективы : European conference on neutron scattering
Место публикации : 4th European conference on neutron scattering: Lund, Sweden, 25-29 June 2007 : [сб. тезисов]. - p.128
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Grigoriev, Maxim V., Ruseikina, Anna V., Molokeev M. S., Chernyshev, Vladimir А., Aleksandrovsky A. S., Krylov A. S., Krylova S. N., Shestakov N. P., Velikanov D. A., Garmonov, Alexander A., Matigorov, Alexey V., Ostapchuk, Evgeny A., Schleid, Thomas, Safin, Damir A.
Заглавие : Elucidating elusive quaternary selenide EuCeCuSe3: Synthesis, crystal structure, properties and theoretical studies
Колич.характеристики :9 с
Место публикации : J. Rare Earths. - 2024. - Vol. 42, Is. 1. - P.163-171. - ISSN 10020721 (ISSN), DOI 10.1016/j.jre.2022.11.004. - ISSN 25094963 (eISSN)
Примечания : Cited References: 47
Аннотация: We report on the novel heterometallic quaternary selenide EuCeCuSe3, the fabrication of which has been a challenge until this work. The structure of the reported selenide was elucidated from the powder X-ray diffraction data, which revealed the formation of EuCeCuSe3 with excellent yield (96.7%) accompanied with a minor fraction of CeSe2 (3.3%), and was best solved in orthorhombic space group Pnma with the BaLaCuS3 structural type. Thus, the crystal structure of the title compound completes the row of the heterometallic quaternary selenides EuRECuSe3 (RE = La, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Y), of which the cerium-based derivative exclusively belongs to the BaLaCuS3 structural type. The distortion of the CuSe4 polyhedron was compared for the whole series of EuRECuSe3 compounds using the τ4-descriptor for four coordinated ions, which revealed the highest degree of distortion for the Ce3+-containing selenide, followed by the La3+-based derivative. Furthermore, the crystallographic and geometrical parameters of the reported selenide were discussed in comparison to the Ce3+-based sulfides SrCeCuS3 and EuCeCuS3. Ab initio calculations of the crystal structure, a phonon spectrum and elastic constants for the crystal of EuСeCuSe3 were also performed. The types and wavenumbers of fundamental modes were determined and the involvement of ions participating in the phonon modes was assessed. The experimental IR spectrum of the reported selenide was interpreted and found to be in agreement with the calculated spectrum. The experimental direct band gap of EuCeCuSe3 was measured to be 1.36 eV that is consistent with the concept of its origin due to interband transitions between orbitals emerging mainly from 4f (valence band) and 5d (conduction band) levels of the Eu2+ cation. The dependence of the Young's modulus on the direction demonstrates the anisotropy of the elastic properties, while the Vickers hardness for EuCeCuSe3 was calculated to be 5.2 GPa. Finally, the title compound is paramagnetic above 4 K.
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Вид документа : Статья из журнала
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Автор(ы) : Zagorskiy D.L., Semenov S. V., Komogortsev S. V., Balaev D. A., Doludenko I.M., Panina L.V.
Заглавие : Magnetization processes in two-dimensional arrays of iron nanowires
Колич.характеристики :8 с
Место публикации : J. Magn. Magn. Mater. - 2024. - Vol. 595. - Ст.171573. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2023.171573. - ISSN 18734766 (eISSN)
Примечания : Cited References: 48. - This work was supported by Russian Scientific Foundation (RSF) Grant 22-22-00983
Аннотация: Arrays of iron nanowires (NWs) obtained by template-assisted electrodeposition constitute a promising composite material characterized by a combination of high magnetization in the filler and perpendicular magnetic anisotropy. The properties of these composites arise from the interplay between the behavior of individual NWs and their magnetostatic interactions. In this study, we investigated NW arrays with identical wire diameters but varying spatial arrangements. Major hysteresis loops were studied under various field directions relative to the NW axis. Key parameters such as the slope of the magnetization curve, saturation magnetization, and coercive force were quantified. Additionally, FORC (First Order Reversal Curve) measurements were conducted with the field oriented longitudinally with respect to the NW, offering insights into the inhomogeneity of the demagnetizing field influenced by the NW array's configuration. In the sample with the highest NW density, we observed isotropic behavior of the effective demagnetizing field, and we proposed an explanation for this phenomenon using the effective media approach. Micromagnetic simulations revealed that the magnetic behavior of individual NWs with a 100 nm diameter can be described as an interchange between volumes characterized by vortex and uniform magnetization patterns. Calculations of the demagnetizing field using the effective medium model demonstrated excellent agreement with experimental data across arrays featuring different NW densities. Remarkably, the quantitative consistency of coercive field values obtained from micromagnetic simulations and experimental measurements in the range of angles from 0° to 45° for the studied samples underscores the structural homogeneity of the obtained NWs.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Igumenov A. Y., Melnikov I. V., Afanasiev A. A., Popova S. S., Lukinykh S. N., Tambasov I. A.
Заглавие : Temperature and vibration OTDR measurements with a single mode-multimode-single mode fiber structure
Коллективы : Optical Fibers and Sensors for Medical Diagnostics, Treatment and Environmental Applications
Место публикации : Proc. SPIE. - 2023. - Vol. 12372: Optical Fibers and Sensors for Medical Diagnostics, Treatment and Environmental Applications XXIII 2023 (28 - 30 January 2023, San Francisco, California, United States) Conference code: 187531. - Ст.123720P. - , DOI 10.1117/12.2646114
Примечания : Cited References: 31
Аннотация: We suggest a prototype of a fiber-optic sensor system that is based on a simple singlemode-multimode-singlemode fiber structure and serial OTDR. The sensor has simple structure, made of affordable components, exploits easy measuring principle, immunes to EMI or RFI, and has confident response to measure key environment variables at a very long span. From the experimental results, the relationship between the temperature of water and output signal of the temperature sensor can be determined. After some maths, we can determine the temperature of the water by measuring the optical power loss of the at the SMS structure in a temperature range of 30 to 70 °C. This SMS structure is shown to carry out vibration measurement for 0.1-60 Hz frequencies with high accuracy. The OTDR exploited allows carrying out far-field measurements when SMS structure is spliced in long fiber-optic link.
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Вид документа : Статья из журнала
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Автор(ы) : Muzalevskiy K. V., Ruzicka Z., Roy A., Loranty M., Vasiliev A.
Заглавие : Brief communication: Identification of tundra topsoil frozen/thawed state from SMAP and GCOM-W1 radiometer measurements using the spectral gradient method
Колич.характеристики :10 с
Место публикации : Cryosphere. - 2023. - Vol. 17, Is. 9. - P.4155-4164. - ISSN 19940416 (ISSN), DOI 10.5194/tc-17-4155-2023. - ISSN 19940424 (eISSN)
Примечания : Cited References: 34. - This research has been supported by the state assignment of the Kirensky Institute of Physics, Federal Research Center, Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences (SB RAS). Weather station data collection was support by the Canadian Space Agency, NSERC and frqnt; the US National Science Foundation (PLR-1304464 and PLR-1417745); and the state assignment of the Earth Cryosphere Institute, Tyumen Scientific Centre, SB RAS (121041600043-4)
Аннотация: From 2015 to 2020, using the spectral gradient radiometric method, the possibility of the frozen/thawed (FT) state identification of tundra soil was investigated based on Soil Moisture Active Passive (SMAP) and Global Change Observation Mission - Water Satellite 1 (GCOM-W1) satellite observations of 10 test sites located in the Arctic regions of Canada, Finland, Russia, and the USA. It is shown that the spectral gradients of brightness temperature and reflectivity (measured in the frequency range from 1.4 to 36.5 GHz with horizontal polarization, a determination coefficient from 0.775 to 0.834, a root-mean-square error from 6.6 to 10.7 d and a bias from -3.4 to C6.5 d) make it possible to identify the FT state of the tundra topsoil. The spectral gradient method has a higher accuracy with respect to the identification of the FT state of tundra soils than single-frequency methods based on the calculation of polarization index.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Fomenko E. V., Akimochkina G. V., Knyazev Yu. V., Semenov S. V., Yumashev V. V., Solovyov L. A., Anshits A. G.
Заглавие : Characterization and magnetic properties of sintered glass-ceramics from dispersed fly ash microspheres
Место публикации : Magnetochemistry. - 2023. - Vol. 9, Is. 7. - Ст.177. - ISSN 23127481 (eISSN), DOI 10.3390/magnetochemistry9070177
Примечания : Cited References: 50. - Russian Science Foundation and the Krasnoyarsk Regional Science Foundation, grant number 22-27-20039, https://rscf.ru/project/22-27-20039/ (accessed on 15 March 2023)
Аннотация: The recycling of hazardous industrial waste into high-tech materials with desired properties is of considerable interest since it provides optimal alternatives for its final disposal. Coal fly ash, the major waste generated by coal-fired power plants, contains significant quantities of dispersed microspheres with a diameter smaller than 10 μm, which are anthropogenic atmospheric pollutants PM10. Due to their composition and fine-grained powder morphology, they can be converted into sintered products. In this study, dispersed microspheres from class C fly ash were directly sintered without any additive to form high-strength glass-ceramics with magnetic properties. The optimum processing conditions were achieved at a temperature of 1200 °C, at which samples with a compressive strength of 100.6 MPa were obtained. Sintering reduces the quantity of the glass phase and promotes the formation of larnite, Fe-spinel, ye’elimite, and ternesite. Mössbauer measurements show that the relative concentration of the magnetic phase compared to the paramagnetic one rises almost in order. The sintered sample demonstrates a narrower distribution of the hyperfine magnetic field and a significantly lower value of the coercive field of 25 Oe, which allows proposing such materials as soft magnetic materials. The presented results demonstrate promising industrial applications of hazardous PM10 to minimize solid waste pollution.
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Вид документа : Статья из журнала
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Автор(ы) : Pankrats A. I., Zharkov S. M., Zeer G. M., Gudim I. A.
Заглавие : Antiferromagnetic resonance and magnetic anisotropy in PrxY1−xFe3(BO3)4 crystals in the region of the magnetic structure transformation “easy axis – easy plane”
Место публикации : J. Alloys Compd. - 2022. - Vol. 909. - Ст.164821. - ISSN 09258388 (ISSN), DOI 10.1016/j.jallcom.2022.164821
Примечания : Cited References: 37. - The authors acknowledge the assistance of R. Mironov in some resonance measurements. The SEM and EDS investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020–0011) of the Ministry of Science and Higher Education of the Russian Federation
Аннотация: The spin dynamics, magnetic structures and magnetic anisotropy of single crystals PrxY1−xFe3(BO3)4 have been studied using antiferromagnetic resonance (AFMR) in a wide range of frequencies, magnetic fields, and temperatures. The frequency-field dependences of AFMR for the crystals with x = 0.25 and 0.45 are characteristic of antiferromagnets with the easy plane (EP) anisotropy. The crystals with x = 0.75 and 1.0 exhibit frequency-field dependences that are typical for antiferromagnets with the easy axis (EA) anisotropy. In these crystals, a significant decrease in the effective anisotropy fields of praseodymium upon the transition to the spin-flop state has been found. It is shown that this is the main reason for the large lability intervals, within which the regions of coexistence of the collinear and spin-flop states overlap. In the crystal with x = 0.67, the magnetic field applied along the trigonal axis of the crystal leads to the spin reorientation transition from the EA to the EP state. A magnetic phase diagram of the states on the plane "magnetic field - temperature" is built. In this crystal, the effective anisotropy field of praseodymium also decreases upon the transition to the field-induced EP state. Diamagnetic dilution of the praseodymium subsystem leads to the contribution of this subsystem to the total anisotropy field depending almost linearly on the praseodymium concentration.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Grigoriev, Maxim V., Solovyov, Leonid A., Ruseikina, Anna V., Aleksandrovsky A. S., Chernyshev, Vladimir A., Velikanov D. A., Garmonov, Alexander A., Molokeev M. S., Oreshonkov A. S., Shestakov N. P., Matigorov, Alexey V., Volkova, Svetlana S., Ostapchuk, Evgeniy A., Kertman, Alexander V., Schleid, Thomas, Safin, Damir A.
Заглавие : Quaternary selenides EuLnCuSe3: Synthesis, structures, properties and in silico studies
Место публикации : Int. J. Mol. Sci. - 2022. - Vol. 23, Is. 3. - Ст.1503. - ISSN 1422-0067(eISSN), DOI 10.3390/ijms23031503
Примечания : Cited References: 90
Предметные рубрики: RARE-EARTH
CRYSTAL-STRUCTURES
MAGNETIC-PROPERTIES
THERMOELECTRIC PERFORMANCE
Аннотация: In this work, we report on the synthesis, in-depth crystal structure studies as well as optical and magnetic properties of newly synthesized heterometallic quaternary selenides of the Eu+2Ln+3Cu+1Se3 composition. Crystal structures of the obtained compounds were refined by the derivative difference minimization (DDM) method from the powder X-ray diffraction data. The structures are found to belong to orthorhombic space groups Pnma (structure type Ba2MnS3 for EuLaCuSe3 and structure type Eu2CuS3 for EuLnCuSe3, where Ln = Sm, Gd, Tb, Dy, Ho and Y) and Cmcm (structure type KZrCuS3 for EuLnCuSe3, where Ln = Tm, Yb and Lu). Space groups Pnma and Cmcm were delimited based on the tolerance factor t’, and vibrational spectroscopy additionally confirmed the formation of three structural types. With a decrease in the ionic radius of Ln3+ in the reported structures, the distortion of the (LnCuSe3) layers decreases, and a gradual formation of the more symmetric structure occurs in the sequence Ba2MnS3 → Eu2CuS3 → KZrCuS3. According to magnetic studies, compounds EuLnCuSe3 (Ln = Tb, Dy, Ho and Tm) each exhibit ferrimagnetic properties with transition temperatures ranging from 4.7 to 6.3 K. A negative magnetization effect is observed for compound EuHoCuSe3 at temperatures below 4.8 K. The magnetic properties of the discussed selenides and isostructural sulfides were compared. The direct optical band gaps for EuLnCuSe3, subtracted from the corresponding diffuse reflectance spectra, were found to be 1.87–2.09 eV. Deviation between experimental and calculated band gaps is ascribed to lower d states of Eu2+ in the crystal field of EuLnCuSe3, while anomalous narrowing of the band gap of EuYbCuSe3 is explained by the low-lying charge-transfer state. Ab initio calculations of the crystal structures, elastic properties and phonon spectra of the reported compounds were performed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ruseikina A. V., Grigoriev M. V., Solovyov L. A., Chernyshev V. A., Aleksandrovsky A. S., Krylov A. S., Krylova S. N., Shestakov N. P., Velikanov D. A., Garmonov A. A., Matigorov A. V., Eberle M. A., Schleid T., Safin D. A.
Заглавие : A Challenge toward novel quaternary sulfides SrLnCuS3 (Ln = La, Nd, Tm): Unraveling synthetic pathways, structures and properties
Место публикации : Int. J. Mol. Sci. - 2022. - Vol. 23, Is. 20. - Ст.12438. - ISSN 14220067 (ISSN), DOI 10.3390/ijms232012438
Примечания : Cited References: 62. - The research was funded by the Tyumen Oblast Government, as part of the West-Siberian Interregional Science and Education Center’s project No. 89-DON (3). This work was supported by state assignment of the Ministry of Science and Higher Education of the Russian Federation (Project Reg. No. 720000Φ.99.1.Б385AA13000)
Аннотация: We report on the novel heterometallic quaternary sulfides SrLnCuS3 (Ln = La, Nd, Tm), obtained as both single crystals and powdered samples. The structures of both the single crystal and powdered samples of SrLaCuS3 and SrNdCuS3 belong to the orthorhombic space group Pnma but are of different structural types, while both samples of SrTmCuS3 crystallize in the orthorhombic space group Cmcm with the structural type KZrCuS3. Three-dimensional crystal structures of SrLaCuS3 and SrNdCuS3 are formed from the (Sr/Ln)S7 capped trigonal prisms and CuS4 tetrahedra. In SrLaCuS3, alternating 2D layers are stacked, while the main backbone of the structure of SrNdCuS3 is a polymeric 3D framework [(Sr/Ln)S7]n, strengthened by 1D polymeric chains (CuS4)n with 1D channels, filled by the other Sr2+/Ln3+ cations, which, in turn, form 1D dimeric ribbons. A 3D crystal structure of SrTmCuS3 is constructed from the SrS6 trigonal prisms, TmS6 octahedra and CuS4 tetrahedra. The latter two polyhedra are packed together into 2D layers, which are separated by 1D chains (SrS6)n and 1D free channels. In both crystal structures of SrLaCuS3 obtained in this work, the crystallographic positions of strontium and lanthanum were partially mixed, while only in the structure of SrNdCuS3, solved from the powder X-ray diffraction data, were the crystallographic positions of strontium and neodymium partially mixed. Band gaps of SrLnCuS3 (Ln = La, Nd, Tm) were found to be 1.86, 1.94 and 2.57 eV, respectively. Both SrNdCuS3 and SrTmCuS3 were found to be paramagnetic at 20-300 K, with the experimental magnetic characteristics being in good agreement with the corresponding calculated parameters.
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10.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Орлов, Виталий Александрович, Григорьев Э. В.
Заглавие : Лабораторный комплекс по физике с элементами автоматизации измерений и обработки результатов
Коллективы : Международная конференция по фотонике и информационной оптике, Российская академия наук, Национальный исследовательский ядерный университет "МИФИ"
Место публикации : XI Международная конференция по фотонике и информационной оптике: сборник научных трудов. - Москва, 2022. - С. 218-221. - ISBN 978-5-7262-2842-6
Примечания : Библиогр.:
Аннотация: Многие студенты инженерных специальностей университетов уже в школьные годы прошли хорошую подготовку в специализированных физико-математических классах, насыщенную физическим экспериментом. Оказавшись в стенах университета, такой студент вновь оказывается в физической лаборатории, где предлагаются вполне стандартные, уже знакомые, опыты (с незначительными вариациями). Это обстоятельство тормозит развитие пытливого ума, приводит к нерациональной трате материальных средств, оборудования, времени студента и преподавателя. Предлагаемый проект направлен на проектирование и создание комплекса лабораторного физического практикума и демонстрационного эксперимента, отвечающего современному уровню развития физической науки. Many students of engineering specialties of universities, already in their school years, were well trained in specialized physics and mathematics classes, saturated with physical experiments. Once within the walls of the university, such a student again finds himself in a physics laboratory, where quite standard, already familiar, experiments are offered (with minor variations). This circumstance inhibits the development of an inquiring mind, leads to an irrational waste of material resources, equipment, time of the student and teacher. The proposed project is aimed at designing and creating a complex of laboratory physical practice and a demonstration experiment that meets the modern level of development of physical science.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ruseikina A. V., Chernyshev V. A., Velikanov D. A., Aleksandrovsky A. S., Shestakov N. P., Molokeev M. S., Grigoriev M. V., Andreev O. V., Garmonov A. A., Matigorov A. V., Melnikova L. V., Kislitsyn A. A., Volkova S. S.
Заглавие : Regularities of the property changes in the compounds EuLnCuS3 (Ln = La-Lu)
Место публикации : J. Alloys Compd. - 2021. - Vol. 874. - Ст.159968. - ISSN 09258388 (ISSN), DOI 10.1016/j.jallcom.2021.159968
Примечания : Cited References: 102. - The work was supported by the Ministry of Science and Higher Education of the Russian Federation under Project No. FEUZ-2020-0054 ; by the " YMNIK " program research project No. 14977GY/2019; by the Ministry of Science and Higher Education of the Russian Federation under project RFMEFI59420X0019
Аннотация: This work contains the results of complex experimental research of the compounds EuLnCuS3 (Ln = La-Lu) enhanced by the DFT calculations. It is aimed at the data replenishment with particular attention to the revelation of regularities in the property changes, in order to extend the potential applicability of the materials of the selected chemical class. The ab initio calculations of the fundamental vibrational modes of the crystal structures were in good agreement with experimental results. The wavenumbers and types of the modes were determined, and the degree of the ion participation in the modes was also estimated. The elastic properties of the compounds were calculated. The compounds were found out to be IR-transparent in the range of 4000–400 cm–1. The estimated microhardness of the compounds is in the range of 2.68–3.60 GPa. According to the DSC data, the reversible polymorphous transitions were manifested in the compounds EuLnCuS3 (Ln = Sm, Gd-Lu): for EuSmCuS3 Tα↔β = 1437 K, ΔНα↔β = 7.0 kJ·mol-1, Tβ↔γ = 1453 K, ΔНβ↔γ = 2.6 kJ·mol-1; for EuTbCuS3 Tα↔β = 1478 K, ΔНα↔β = 1.6 kJ·mol-1, Tβ↔γ = 1516 K, ΔНβ↔γ = 0.9 kJ·mol-1, Tγ↔δ = 1548 K, ΔНγ↔δ = 1.6 kJ·mol-1; for EuTmCuS3 Tα↔β = 1543 K, Tβ↔γ = 1593 K, Tγ↔δ = 1620 K; for EuYbCuS3 Tα↔β = 1513 K, Tβ↔γ = 1564 K, Tγ↔δ = 1594 K; for EuLuCuS3 Tα↔β = 1549 K, Tβ↔γ = 1601 K, Tγ↔δ = 1628 K. In the EuLnCuS3 series, the transition into either ferro- or ferrimagnetic states occurred in the narrow temperature range from 2 to 5 K. The tetrad effect in the changes of incongruent melting temperature and microhardness conditioned on rLn3+ as well as influencing of phenomenon of crystallochemical contraction were observed. For delimiting between space groups Cmcm and Pnma in the compounds ALnCuS3, the use of the tolerance factor t’ = IR(A)·IR(C) + a×IR(B)2 was verified.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Popova M. N., Chukalina E. P., Erofeev D. A., Gudim I. A., Golosovsky I. V., Gukasov A., Mukhin A. A., Malkin B. Z.
Заглавие : High-resolution optical spectroscopy, magnetic properties, and single-crystal neutron diffraction of multiferroic HoFe3(BO3)4: Magnetic structure
Место публикации : Phys. Rev. B. - 2021. - Vol. 103, Is. 9. - Ст.094411. - ISSN 24699950 (ISSN), DOI 10.1103/PhysRevB.103.094411
Примечания : Cited References: 65. - Financial support of the Russian Science Foundation under Grant No. 19-12-00413 is acknowledged. I.V.G. acknowledges financial support of the neutron scattering studies from the Russian Foundation for Basic Research under Grant No. 20-02-00109. The analysis of the measured neutron diffraction data was performed by A.A.M. with support of the Russian Science Foundation under Grant No. 16-12-10531
Аннотация: The magnetic structure is usually determined by the neutron diffraction measurements. However, in the case of complex multisublattice magnetics, this method fails to give an unambiguous result. Here, on the example of multiferroic HoFe3(BO3)4, we show that in the case of rare-earth (RE) compounds the right magnetic structure can be determined by additionally using optical spectroscopy and a theoretical analysis based on spectroscopic data. HoFe3(BO3)4 demonstrates a series of phase transitions and interesting magnetic and magnetoelectric properties. The available information on the magnetic structure of the compound, necessary for understanding and utilizing these properties, is contradictory. To resolve the existing ambiguities, we apply a combined approach. The high-resolution spectroscopy data deliver a set of the Ho3+ crystal-field (CF) levels in the paramagnetic and both easy-plane and easy-axis magnetic phases. These data are used to determine CF and Ho3+-Fe3+ exchange parameters and, then, to calculate the temperature dependencies of the magnetic susceptibility tensor of HoFe3(BO3)4. Based on these calculations, we suggest an easy-plane antiferromagnetic structure with a collinear arrangement of the Fe spins along the a axis and induced noncolinear moments of magnetically nonequivalent Ho ions. The suggested structure is further confirmed by single-crystal elastic neutron scattering experiments. We argue that specific features of the magnetic properties of RE iron borates isostructural to HoFe3(BO3)4 are governed by the energy patterns and the symmetry properties of the wave functions of the lower CF levels of the RE ground multiplet in the crystal field of the C2 symmetry.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ruseikina A. V., Molokeev M. S., Chernyshev V. А., Aleksandrovsky A. S., Krylov A. S., Krylova S. N., Velikanov D. A., Grigoriev M. V., Maximov N. G., Shestakov N. P., Garmonov A. A., Matigorov A. V., Tarasov A. S., Rautskii M. V., Khritokhin N. А., Melnikova L. V., Tretyakov N. Y.
Заглавие : Synthesis, structure, and properties of EuScCuS3 and SrScCuS3
Место публикации : J. Solid State Chem. - 2021. - Vol. 296. - Ст.121926. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2020.121926
Примечания : Cited References: 72. - The work was supported by the Ministry of Science and Higher Education of the Russian Federation under Project No. FEUZ-2020-0054; by RFBR Grant 18-02-00754 ; by the “UMNIK” program research project № 14977GY/2019; by the Ministry of Science and Higher Education of the Russian Federation (contract no. 05.594.21.0019 , unique identification number RFMEFI59420X0019). Maxim S. Molokeev, Anton S. Tarasov and Mikhail V. Rautskii acknowledge additional funding from Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation. The subset research was performed in Research Resource Center “Natural Resource Management and Physico-Chemical Research.” The use of equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center « Krasnoyarsk Science Center SB RAS» is acknowledged
Аннотация: The crystal structures of the first-synthesized compound EuScCuS3 and previously known SrScCuS3 are refined by Rietveld analysis of X-ray powder diffraction data. The structures are found to belong to orthorhombic crystal system, space group Cmcm, structural type KZrCuS3, with a = 3.83413(3) Å, b = 12.8625(1) Å, c = 9.72654(8) Å (SrScCuS3) and a = 3.83066(8) Å, b = 12.7721(3) Å, c = 9.7297(2) Å (EuScCuS3). The temperatures and enthalpies of incongruent melting are the following: Тm = 1524.5 К, ΔHm = 21.6 kJ•mol−1 (SrScCuS3), and Тm = 1531.6 К, ΔHm = 26.1 kJ•mol−1 (EuScCuS3). Ab initio calculations of the crystal structure and phonon spectrum of the compounds were performed. The types and wavenumbers of fundamental modes were determined and the involvement of ions participating in the IR and Raman modes was assessed. The experimental IR and Raman spectra were interpreted. EuScCuS3 manifests a ferromagnetic transition at 6.4 K. The SrScCuS3 compound is diamagnetic. The optical band gaps were found to be 1.63 eV (EuScCuS3) and 2.24 eV (SrScCuS3) from the diffuse reflectance spectra. The latter value is in good agreement with that calculated by the DFT method. The narrower band gap of EuScCuS3 is explained by the presence of 4f-5d transition in Eu2+ ion that indicates a possibility to control the band gap of the chalcogenides by the inclusion of Eu. The activation energy of crystal structure defects, being the source of additional absorption in the NIR spectral range, was found to be 0.29 eV.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Maximova O. A., Ovchinnikov S. G., Lyashchenko S. A.
Заглавие : Analytical calculation of dielectric permittivity tensor from magneto-optical ellipsometry measurements
Коллективы : Government of the Russian Federation [075-15-2019-1886]
Место публикации : J. Phys. A: IOP PUBLISHING LTD, 2021. - Vol. 54, Is. 29. - Ст.295201. - ISSN 1751-8113, DOI 10.1088/1751-8121/abfe72. - ISSN 1751-8121(eISSN)
Примечания : Cited References: 24. - This study was supported by the Government of the Russian Federation (Agreement No. 075-15-2019-1886)
Предметные рубрики: FILMS
Аннотация: Magneto-optical ellipsometry combines ellipsometry and magneto-optical Kerr effect measurements which are two powerful techniques. The main difficulty is usually in data processing as a number of parameters should be extracted from measured ellipsometric (ψ, Δ) and magneto-ellipsometric (δψ, δΔ) parameters. Standard procedure of solving magneto-ellipsometry equations involves numerical calculations. In this paper we show that it is possible to find out all elements of dielectric permittivity tensor without numerical calculation methods. It means that the inverse problem of magneto-optical ellipsometry can be solved analytically in the case of expansion of magneto-ellipsometric parameters δψ and δΔ with respect to two small parameters. We present a full set of mathematical expressions that enable us to calculate complex refraction index and complex magneto-optical parameter of a sample from magneto-optical ellipsometry measurements, thereby obtaining diagonal and off-diagonal complex elements of dielectric permittivity tensor. This analytical approach can be used in case of the contribution from magnetism into reflection coefficients being small.
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15.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Максимова, Ольга Александровна, Овчинников, Сергей Геннадьевич, Лященко, Сергей Александрович
Заглавие : Как оценить величину магнитооптического параметра ферромагнетика по магнитоэллипсометрическим измерениям
Коллективы : "Новое в магнетизме и магнитных материалах", международная конференция, Научный совет по физике конденсированных сред РАН, МИРЭА - Российский технологический университет, Московский государственный университет им. М.В. Ломоносова, Магнитное общество России
Место публикации : Новое в магнетизме и магнитных материалах: сборник трудов XXIV международной конференции/ прогр. ком.: Р. С. Исхаков, С. Г. Овчинников [и др.]. - 2021. - Т. 3, Секция 12: Магнитооптика и фотомагнетизм. - С. 214-217
Примечания : Библиогр.: 9. - Исследование выполнено за счет гранта Российского научного фонда №21-12-00226
Аннотация: Представлены результаты исследования, направленного на расчет величины магнитооптического параметра Q, определяющего магнитооптические свойства ферромагнетика и входящего в недиагональные компоненты тензора диэлектрической проницаемости, по данным спектральных магнитоэллипометрических измерений.This paper is to report about the results of the research aimed at the calculation of the magneto-optical parameter Q, which defines magneto-optical properties of the ferromagnetic materials and is included into off-diagonal components of the dielectric tensor, from magneto-ellipsometry data
Материалы конференции,
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Muzalevskiy K. V., Karavaysky A. Yu.
Заглавие : Shielded open-circuited probe for in-situ measurements of soil permittivity in Very high frequency (VHF) and Ultra high frequency (UHF) bands
Коллективы : SB RAS project [0287-2021-0034]
Место публикации : Trans. Inst. Meas. Control. - 2021. - Vol. 43, Is. 16. - P.3566-3572. - ISSN 0142-3312, DOI 10.1177/01423312211037791. - ISSN 1477-0369(eISSN)
Примечания : Cited References: 30. - The author(s) disclosed receipt of the following financial support for the research, authorship, and/or publication of this article: This work was supported by the SB RAS project No. 0287-2021-0034
Предметные рубрики: DIELECTRIC CHARACTERIZATION
MOISTURE
Аннотация: In this paper, the shielded open-circuited probe operating in the wide frequency range from 75MHz to 2GHz is proposed. The probe is made of an SubMiniature version A (SMA) flange connector. The central rod of the SMA connector emerges from a coaxial transition in the flange and shielded by four rods. The robe design allows us to calculate of the probe reflection coefficient S11 used simple analytical transmission line model (TEM wave mode), the parameters of which were calibrated on a set of substances with a known frequency spectrum of permittivity. The refractive index (RI) and normalized attenuation coefficient (NAC) retrieval technique is based on solving the inverse problem of minimizing the residual norm between measured and calculated frequency spectra of reflection coefficient S11. After calibration, the root-mean-square error (determination coefficient) between the measured and calculated module and phase of the reflection coefficient S11 for the sets of calibration media air, distilled water, butanol, pure ice, water solution with NaCl of salinity of 8.9% do not exceed 0.26dB (0.995) and 0.03 rad (0.999), respectively, in the frequency range from 75MHz to 2GHz. The root-mean-square error (determination coefficient) between the measured RI and NAC spectra for four soil cover samples (variation of the clay fraction from 10.5 g/g to 47.6 g/g) using the proposed probe and a precision coaxial cell not exceeds 0.109 (0.993) and 0.057 (0.986), respectively, in the frequency range from 75 MHz to 2 GHz. As a result, it is experimentally shown that RI и NAC can be measured by the proposed non-precision probe with an error comparable to the precision coaxial cell.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Fomin S. V., Muzalevskiy K. V.
Заглавие : A dielectric model for frozen mineral soils at a frequency of 435 MHz
Место публикации : Remote Sens. Lett. - 2021. - Vol. 12, Is. 9. - P.944-950. - ISSN 2150704X (ISSN), DOI 10.1080/2150704X.2021.1947537
Примечания : Cited References: 16. - This work was supported by the state assignment of the Ministry of Science and Higher Education of the Russian Federation [project No. 0287-2021-0034]
Аннотация: A single frequency refractive mixing dielectric model at 435 MHz for frozen mineral soils is proposed. The model was created based on the laboratory dielectric measurements of three soil samples in the ranges of soil moisture from 0.01cm3 cm−3 to 0.42cm3 cm−3, temperature from– 30°C to– 1°C, clay content (by weight) from 9.1% to 41.3%. Coefficient of determination R2 and root mean square error (RMSE) predicted by the model and measured values for real () and imaginary () part of the complex relative permittivity (CRP) are = 0.988 (= 0.323) and = 0.987 (= 0.100). Compared to well-known spectroscopic models, this model is simpler in practical engineering use. The input parameters of the model are the volumetric soil moisture, temperature and the content of the clay fraction. The output parameters are the real and imaginary parts of the CRP. The created model may be used to develop new remote sensing retrieval algorithms of temperature, the content of unfrozen water and ice in the root zone of frozen soils for northern regions.ε 'ε ''R2ε 'RMSEε 'R2ε ''RMSEε ''
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Velikanov D. A.
Заглавие : High-sensitivity measurements of the magnetic properties of materials at cryogenic temperatures
Место публикации : Inorg. Mater.: Appl. Res. - 2020. - Vol. 11, Is. 4. - P.801-808. - ISSN 20751133 (ISSN), DOI 10.1134/S2075113320040413
Примечания : Cited References: 17. - This study was supported by the Russian Foundation for Basic Research, the Government of Krasnoyarsk Krai, and the Krasnoyarsk Territorial Foundation for Support of Scientific and R&D Activity, project no. 17-42-240080 “Study of the Effect of the Size, Morphology, and Fabrication Technology on the Functional Properties of Biomagnetic Nanodevices Based on 3 d Metals and Their Oxides.”
Аннотация: An original magnetometer based on a dc superconducting quantum interferometer is described. The design features of the device are discussed and functional diagrams of its new units are presented. The magnetic moment measurement methods that optimize the measurement process are proposed. Examples of the investigations carried out on the samples of different materials are given. The factors affecting the reliability of the magnetic measurements are considered.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Turchin P. P., Turchin V. I., Yurkevich S. V., Sukhodaev P. O., Raikova I. S.
Заглавие : Application of DMA 242 C for quasi-static measurements of piezoelectric properties of solids
Место публикации : J. Sib. Fed. Univ. Math. Phys. - 2020. - Vol. 13, Is. 1. - P.97-103. - ISSN 19971397 (ISSN), DOI 10.17516/1997-1397-2020-13-1-97-103; Журн. СФУ. Матем. и физика
Примечания : Cited References: 26. - The reported study was funded by Russian Foundation for Basic Research project no. 18-42-240016, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: "Electromechanical Properties and Anisotropy of Acoustic Wave Propagation in Yttrium Aluminoborates Single Crystals"
Аннотация: An experimental device for quasi-static measurements of piezoelectric moduli dijk, based on the possibilities of precision variations in mechanical stresses with the device DMA 242 C in the frequency range 0-100 Hz has been developed. A special sample holder and a charge amplifier are used in the measuring scheme. The measurements of piezoelectric moduli values of trigonal piezoelectric single crystalls La3Ga5SiO14 (P321) and YAl3(BO3)4 (R32), as well as hexagonal ZnO (P63mc) have been carried out.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Knyazev Yu. V., Tarasov A. S., Platunov M. S., Trigub A. L., Bayukov O. A., Boronin A. I., Solovyov L. A., Rabchevskii E. V., Shishkina N. N., Anshits A. G.
Заглавие : Structural and electron transport properties of CaFe2O4 synthesized in air and in helium atmosphere
Место публикации : J. Alloys Compd. - 2020. - Vol. 820. - Ст.153073. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2019.153073. - ISSN 1873-4669 (eISSN)
Примечания : Cited References: 37. - The reported study was partially supported by the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science (grant #18-42-243011) and the UMNIK Program.
Аннотация: The samples with the CaFe2O4-type crystal structure were obtained by the solid-state reaction method at 1000 °C in the air and the helium atmosphere for the first time. We investigated the modification of the structural and electronic properties of the obtained samples. Mössbauer, XAFS-, XPS-spectroscopies, and dc-, ac-conductivity measurements were carried out. Mössbauer and XAFS-spectroscopies showed that the local environment of Fe and Ca cations does not change in the case of the inert atmosphere synthesis. Nevertheless, a sharp six-order increase in the electrical resistance observed at room temperature for the sample obtained in the in the helium atmosphere. Moreover, calculated from dc-conductivity data activation energy rises from 0.327 for the air-synthesized sample to 0.585 eV for helium-obtained one. This behavior indicates significant modification of in-band-gap energy structure, which correlated with thermally activated charge carriers. Our ac-conductivity measurements in the frequency range of 1 kHz–2 MHz for the CaFe2O4 obtained in the air showed the presence of defect levels in the energy band structure. Oxygen pressure reduction during the synthesis results in levels vanishing. Therefore, we suppose the key role of oxygen atoms in the transport properties of the material, which is indirectly confirmed by XPS data. In prospect, CaFe2O4 can be used in promising gas analyzers.
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