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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Elesina V. I., Churilov G. N., Vnukova N. G., Dudnik A. I., Osipova I. V.
Заглавие : Filtration process combined with mechanical action, as a method for efficient extraction of endohedral metallofullerenes from carbon soot
Место публикации : Fuller. Nanotub. Carbon Nanostruct. - 2019. - Vol. 27, Is. 10. - P.803-807. - ISSN 1536383X (ISSN), DOI 10.1080/1536383X.2019.1648439
Примечания : Cited References: 22
Аннотация: The paper presents results of fullerenes and endohedral metallofullerenes extracts studies, isolated from the graphite rods carbon soot spray, and containing Y2O3 in a high frequency arc discharge. Two ways of extraction were applied and compared–(1) the classic method of Soxhlet extraction, and (2) the one developed by our team–extraction based on mechanical action combined with filtration. To implement the method, we used a laboratory version of installation, embodying technical solutions for rapid extraction. Chromatographic and mass spectrometry studies of fullerene extracts obtained by these methods revealed that by combining mechanical action with simultaneous filtration, we can significantly intensify and reduce the process of extracting fullerenes and endohedral metallofullerenes compared to the Soxhlet extraction method. This is especially evident in the release of endohedral metallofullerenes. Our method allows to reduce the release time of fullerenes from 10 g of carbon soot on laboratory installation up to 15 minutes, against the Soxhlet extraction method taking 18 hours. Whilst, the total number of fullerenes extracted by both methods almost coincides (the extraction method using mechanical action allowed us to extract 0.2-0.4 wt. % more), the composition of the isolated fullerene mixtures is different. The relative content of higher fullerenes and endohedral metallofullerenes exceeds when the mechanical action-based extraction method applied. © 2019, © 2019 Taylor & Francis Group, LLC.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Markevich I. A., Drokin N. A., Selyutin G. E.
Заглавие : Impedance Spectroscopy Study of a Polymer Composite with Carbon Nanotubes in Contact with an Electrolyte
Место публикации : Tech. Phys. - 2019. - Vol. 64, Is. 9. - P.1324-1329. - ISSN 1063-7842, DOI 10.1134/S1063784219090093. - ISSN 1090-6525(eISSN)
Примечания : Cited References: 14
Предметные рубрики: BEHAVIOR
CONDUCTIVITY
RELAXATION
Аннотация: The measured frequency dependence of the electric impedance of a composite based on ultra-high molecular weight polyethylene reinforced with carbon nanotubes in contact with an electrolyte is presented. The behavior of the active and reactive impedance components, permittivity, and conductivity in the frequency range from 0.1 Hz to 120 MHz is analyzed. An equivalent electric circuit simulating the dispersion of the impedance of the polymer composite making contact with the electrolyte is proposed. The formation of a double electric layer at the interface between the polymer composite and electrolyte layer is demonstrated and the electrical characteristics of this layer are determined.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tambasov I. A., Voronin A. S., Evsevskaya N. P., Volochaev M. N., Fadeev Y. V., Simunin M. M., Aleksandrovsky A. S., Smolyarova T. Е., Abelian S. R., Tambasova E. V., Gornakov M. O., Eremina V. A., Kuznetsov Y. M., Dorokhin M. V., Obraztsova E. D.
Заглавие : Thermoelectric properties of low-cost transparent single wall carbon nanotube thin films obtained by vacuum filtration
Место публикации : Physica E. - 2019. - Vol. 114. - Ст.113619. - ISSN 13869477 (ISSN), DOI 10.1016/j.physe.2019.113619
Примечания : Cited References: 53. - The study was carried out by a grant of Russian Science Foundation (project No. 17-72-10079). The electron microscopy examination was carried out at the Center for Collective Use of the Krasnoyarsk Scientific Center of the Siberian Branch of the Russian Academy of Sciences (Krasnoyarsk, Russia). V.A.E. and E.D.O. thank RFFI-18-32-00998_mol_a and RFFI-19-02-00859_a projects for support of development of two aqueous phase technique for nanotube separation.
Аннотация: The dispersions of semiconducting (sc-) and metallic (m-) SWCNTs with purity more than 98 and 86%, correspondingly, were obtained by using the aqueous two-phase extraction method. The unseparated (un-) SWCNTs contained ~3/4 of semiconducting and ~1/4 of metallic nanotubes. Thin films based on unseparated, semiconducting and metallic SWCNTs were prepared by vacuum filtration method. An Atomic Force Microscopy (AFM) and a Transmission Electronic Microscopy (TEM) were used to investigate the thin film microstructure. The thin SWCNT film transmittance was measured in the wavelength range of 300–1500 nm. Thermoelectric properties were carried out in the temperature range up to 200 °C. The largest Seebeck coefficient was observed for thin films based on semiconducting SWCNTs. The maximum value was 98 μV/K under the temperature of 170 °C. The lowest resistivity was 7.5·10−4·Ohm·cm at room temperature for thin un-SWCNT films. The power factor for m-SWCNT and un-SWCNT films was 47 and 213 μW m−1 K−2, correspondingly, at room temperature and 74 and 54 μW m−1 K−2 at 200 °C, respectively. For a thin sc-SWCNT film the maximum power factor was 2.8 μW m−1 K−2 at 160 °C. The un-SWCNT film thermal conductivity coefficient was 5.63 and 3.64 W m−1 K−1 and a thermoelectric figure of merit was 0.011 and 0.016 at temperatures of 23 and 50 °C, respectively.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Tambasov I. A., Voronin A. S., Evsevskaya N. P., Volochaev M. N., Aleksandrovsky A. S., Abelyan S. R., Tambasova E. V.
Заглавие : Thermoelectric properties of optically transparent thin films based on single-walled carbon nanotubes
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов, Институт автоматики и процессов управления ДВО РАН, Дальневосточный федеральный университет
Место публикации : Fourth Asian school-conference on physics and technology of nanostructured materials (ASCO-NANOMAT 2018): proceedings. - Vladivostok, 2018. - P.88-89
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tambasov I. A., Voronin A. S., Evsevskaya N. P., Volochaev M. N., Fadeev, Yu. V., Krylov A. S., Aleksandrovskii A. S., Luk'yanenko A. V., Abelyan S. R., Tambasova E. V.
Заглавие : Structural and Thermoelectric Properties of Optically Transparent Thin Films Based on Single-Walled Carbon Nanotubes
Коллективы : Russian Science Foundation [17-72-10079]
Место публикации : Phys. Solid State. - 2018. - Vol. 60, Is. 12. - P.2649-2655. - ISSN 1063-7834, DOI 10.1134/S1063783418120296. - ISSN 1090-6460(eISSN)
Примечания : Cited References: 31. - This work was supported by the Russian Science Foundation (project no. 17-72-10079).
Аннотация: Thin films have been produced via a spray method from commercially available single-walled carbon nanotubes (SWCNTs). A SWCNT film thickness has ranged from ~10 to ~80 nm. The SWCNT diameter has accepted values of 1.6–1.8 nm. The existence of SWCNTs longer than 10 μm is established. The optimal thickness of a SWCNT thin film is found to be ~15 nm at which the transmittance exceeds 85%. The specific resistance of SWCNT thin films goes from ~1.5 × 10–3 to ~3 × 10–3 Ohm cm at room temperature. The pioneering study of the temperature dependences of the Seebeck coefficient and surface resistance is performed for this type of SWCNT. A surface resistance is found to increase with rising temperature. Furthermore, the Seebeck coefficient of SWCNT thin films weakly depends on temperature. Its value for all samples is evaluated to be ~40 μV/K. According to the sign of the Seebeck coefficient, thin films exhibit hole-type conductivity. Moreover, the power factor of a 15-nm thin SWCNT-film decreases with a temperature increase to 140◦C from the value of approximately ~120 to ~60 μW m–1 K–2. A further rise in temperature has led to a gain in the power factor.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Markevich I. A., Selyutin, G. Ye., Poluboyarov V. A., Drokin N. A., Selyutin A. G., Matzko M. A.
Заглавие : Influence of ultrasonic treatment on mechanical and electro-physical characteristics of UHMWPE/MWCNT composites
Коллективы : All-Russian Conference (with International Participation) "Hot Topics of Solid State Chemistry : From New Ideas to New Materials"
Место публикации : Mater. Today: Proc. - 2020. - Vol. 25. - P.532-535. - ISSN 2214-7853, DOI 10.1016/j.matpr.2020.02.746
Примечания : Cited References: 20
Предметные рубрики: NANOCOMPOSITE
Аннотация: The influence of ultrasonic treatment on the strength and dielectric properties of composites based on ultra-high molecular weight polyethylene (UHMWPE) and multi-walled carbon nanotubes (MWCNT) is studied. It is revealed that the ultrasonic treatment of composite melt at 130 °C results in the uniform distribution of nanotubes in the UHMWPE matrix, an increase in the degree of composite crystallinity by 10%, an increase in abrasion resistance by 37%, an increase in elongation at rupture by a factor of 2. The change in the physical and mechanical properties of the composite is caused by the change in the polymer matrix structure, taking place as a result of ultrasonic action, and does not depend on the presence of nanotubes in the polymer matrix.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Stebeleva O. P., Kashkina L. V., Petrakovskaya E. A., Rubleva T. V., Nikitin S. L., Vshivkova O. A.
Заглавие : Nonequilibrium carbon black suspensions used in synthesis of polymer composite material
Коллективы : International Scientific Conference on Metrological Support of Innovative Technologies
Место публикации : International Scientific Conference on Metrological Support of Innovative Technologies (2 ; 2020 ; 4 March ; Krasnoyarsk). Journal of Physics: Conference Series. - 2020. - Vol. 1515, Is. 2. - Ст.022003. - , DOI 10.1088/1742-6596/1515/2/022003
Примечания : Cited References: 9
Аннотация: Nowadays polymer matrix-based composite material with various carbon fillers are widely used to protect radioequipment from different interference, to improve characteristics of radar absorbing coatings. Current synthesis processes are sophisticated and rather costly. The challenge is to develop new methods of producing composite materials by efficient knowledge intensive technologies to reduce the cost of products. The paper studies possibility of producing composite material on the basis of elastic polyurethane foam with carbon fillers using polyurethane impregnation in nonequilibrium black carbon suspension. Suspension composition: running water and carbon-bearing powders of nanometer range: fullerene black carbon, Taunite (multi-layer carbon nano tube material), technical carbon T900, wood soot. Nonequilibrium suspension was produced by treatment in hydrodynamic generator of rotor type (cavitation mode). Angular rotation speed of the rotor ω = 10000 rpm.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Moseenkov S. I., Kuznetsov V. L., Zavorin A. V., Golubtsov G. V., Korovin, E. Yu., Suslyaev V. I., Ishchenko A. V., Serkova A. N., Sergeenko D. I., Velikanov D. A.
Заглавие : Electrophysical properties of composites based on polyethylene modified with multi-walled carbon nanotubes with high content of Fe-Co-catalyst
Коллективы : Russian Science FoundationRussian Science Foundation (RSF) [17-73-20293]
Место публикации : Russ. J. Appl. Chem. - 2020. - Vol. 93, Is. 4. - P.586-594. - ISSN 1070-4272, DOI 10.1134/S107042722004014X. - ISSN 1608-3296(eISSN)
Примечания : Cited References: 30. - This work was financially supported by the Russian Science Foundation, project no. 17-73-20293.
Предметные рубрики: POLYMER COMPOSITES
NANOPARTICLES
ACTIVATION
NANOCOMPOSITES
Аннотация: The effect of the residual catalyst for the synthesis of multi-walled carbon nanotubes (MWCNTs) on the electrophysical properties of MWCNT-polyethylene composites produced by melt mechanical mixing was studied. The residual catalyst content was varied by changing the MWCNTs synthesis time. The nanotubes used in the work were characterized using transmission and scanning electron microscopy, atomic emission analysis, X-ray phase analysis, and magnetic permeability measurements. The structure of the synthesized composites was studied using optical and scanning electron microscopy. The dependences of the specific magnetization on the applied magnetic field, bulk electrical conductivity on the volumetric content of the filler in the composite, and the frequency dependences of the reflection, transmission, and absorption of electromagnetic radiation in the range 0.01-18 GHz were obtained. It was established that the obtained composites are characterized by a uniform distribution of nanotubes in the polymer matrix, and the dependence of the bulk electrical conductivity on the content of MWCNTs in the composite has a percolation character. Variation in the synthesis time of nanotubes allows producing MWCNTs with a high content of ferromagnetic particles, which are an alloy close in stoichiometry to the composition of the active component of the catalyst. It was shown that the use of composites modified with MWCNTs with a high content of residual catalyst is more effective for absorbing electromagnetic radiation due to an increase in their magnetic losses.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Fel'k V. A., Komogortsev S. V.
Заглавие : Ferromagnetic resonance in micro and nanotubes
Коллективы : Российская академия наук, Уральское отделение РАН, Институт физики металлов им. М. Н. Михеева Уральского отделения РАН, Уральский федеральный университет им. первого Президента России Б.Н. Ельцина, Российский фонд фундаментальных исследований, Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium
Место публикации : Euro-asian symposium "Trends in magnetism" (EASTMAG-2019): Book of abstracts/ чл. конс. ком.: S. G. Ovchinnikov, N. V. Volkov [et al.] ; чл. прогр. ком. D. M. Dzebisashvili [et al.]. - 2019. - Vol. 1. - Ст.B.P17. - P.189-190. - ISBN 978-5-9500855-7-4 (Шифр В33/E12-125657784)
Примечания : Cited References: 1. - The study was carried out with the financial support of the Russian Foundation for Basic Research, the Government of the Krasnoyarsk Region, the Krasnoyarsk Regional Science Foundation as part of the research project No. 18-42-240006 ”Nanomaterials with magnetic properties determined by topological features of the nanostructure”
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Dudnik A. I., Osipova I. V., Nikolaev N. S., Churilov G. N.
Заглавие : Comparative analysis of two methods for synthesis of fullerenes at different helium pressures
Коллективы : RFBRRussian Foundation for Basic Research (RFBR) [18-32-20011]
Место публикации : Fuller. Nanotub. Carbon Nanostruct. - 2020. - Vol. 28, Is. 9. - P.697-701. - ISSN 1536-383X, DOI 10.1080/1536383X.2020.1746281. - ISSN 1536-4046(eISSN)
Примечания : Cited References: 16. - The reported study was funded by RFBR according to the research project No 18-32-20011
Предметные рубрики: PLASMA
YIELD
DISCHARGE
PARAMETERS
DEPENDENCE
C60
Аннотация: The results of the effect of helium pressure in the chamber on the amount and composition of the produced fullerenes (C60, C70, etc.) synthesized in the arc plasma with graphite electrodes are presented. The findings obtained when the arc is powered by a direct (DC) and alternating (AC) currents of low frequency were compared in the same chamber with the electrodes located at the same angle to each other. These two methods are drastically different. The complete conversion of graphite into fullerene soot in AC occurs, but a part of the graphite is converted into a cathode deposit that does not contain fullerenes in DC, the relative amount of which increases when decreasing the helium pressure in the chamber. The highest fullerene content in fullerene soot of 10.2 wt.% is produced at a pressure of 127.5 kPa in AC arc, but in DC arc, the highest content of fullerenes in fullerene soot of 8.3 wt.% is produced at a pressure of 33.3 kPa.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Elesina V. I., Dudnik A. I., Vnukova N. G.
Заглавие : Ultrafast method of fullerenes extraction from carbon condensate
Место публикации : Fuller. Nanotub. Carbon Nanostruct. - 2019. - Vol. 27, Is. 3. - P.225-232. - ISSN 1536383X, DOI 10.1080/1536383X.2018.1543277
Примечания : Cited References: 46. - The authors are grateful to Alexey Popov (Leibniz Institute for Solid State and Materials Research, Dresden, German) for his contribution in conducting mass spectrometer studies.
Ключевые слова (''Своб.индексиров.''): solution extraction--mechanical extraction--fullerenes--soxhlet
Аннотация: The Soxhlet extraction method (SE) only used in the extraction of fullerenes from carbon condensate (CC) obtained in the fullerene production facility, which in the literature is often referred to as carbon black, does not provide complete extraction. Fullerenes can also be extracted from the CC suspension and the solvent by the mechanical extraction method (ME) and show higher degree of extraction efficiency. This method combined with filtration process takes only a few minutes and allows a significant reduction in solvent consumption. Extraction via the ME method application makes it possible to carry out extraction of fullerenes twenty times faster than by the SE method. It can be used as an independent method, bypassing the extraction by the SE method, and also as an additional one. Application of the ME method allows additional extraction of fullerenes weight percentage from the CC, after extracting fullerenes from it applying the SE method. In this instance the higher fullerenes prevail in the essences extracted by the ME method with their content reaching as high as 39.50 wt%. The obtained samples of fullerene mixtures (FM) are characterized by the methods of high-performance liquid chromatography and mass spectrometry. Analysis of the results shows that the composition of the FM, isolated by the ME method, differs from the compositions extracted via the ME method.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Simunin M. M., Ivanchenko F. S., Shiverskii A. V., Fadeev, Yu. V., Tambasov I. A., Nemtsev I. V., Matsynin A. A., Khartov S. V.
Заглавие : Preparation and investigation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes
Коллективы : Russian Foundation for Basic Research [16-32-00302 mol_a]; RFBR; Government of Krasnoyarsk Krai; Krasnoyarsk Krai Foundation [16-42-243059 r_mol_a, 16-42-243006 r_mol_a, 16-48-242092 r_ofi_m]
Место публикации : Tech. Phys. Lett.: MAIK Nauka-Interperiodica / Springer, 2017. - Vol. 43, Is. 9. - P.783-786. - ISSN 1063-7850, DOI 10.1134/S1063785017090127. - ISSN 1090-6533(eISSN)
Примечания : Cited References:7. - This study was supported by the Russian Foundation for Basic Research (RFBR project no. 16-32-00302 mol_a) and jointly by the RFBR, Government of Krasnoyarsk Krai, and the Krasnoyarsk Krai Foundation for the Support of Scientific and Technological Work within scientific projects nos. 16-42-243059 r_mol_a, 16-42-243006 r_mol_a, and 16-48-242092 r_ofi_m.
Предметные рубрики: SOLAR-CELLS
Аннотация: The preparation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes by the spray method is described. The influence of the successive treatment of each functional layer in acid media with different activities on the optical and electric film characteristics is considered. The composite with the surface resistance of 89 Ω/sq at the transparency of 85.3% (550 nm) on a polymer substrate is obtained.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zelenovskiy P. S., Davydov A. O., Krylov A. S., Kholkin A. L.
Заглавие : Raman study of structural transformations in self-assembled diphenylalanine nanotubes at elevated temperatures
Коллективы : International GeoRAMAN Conference
Место публикации : J. Raman Spectrosc. - 2017. - Vol. 48, Is. 11. - P.1401-1405. - ISSN 0377-0486, DOI 10.1002/jrs.5084. - ISSN 1097-4555(eISSN)
Примечания : Cited References:50. - The equipment of the Ural Center for Shared Use 'Modern nanotechnology' UrFU was used. The research was supported by the President of Russian Federation grant for young scientists (Contract 14.Y30.15.6554-MK) and by the Government of the Russian Federation (Act 211, Agreement 02.A03.21.0006). A.K. acknowledges the Turkish-Portuguese project TUBITAK/0006/2014 and CICECO-Aveiro Institute of Materials (Ref. FCT UID/CTM/50011/2013) financed by national funds through the FCT/MEC and, when applicable, co-financed by FEDER under the PT2020 Partnership Agreement.
Предметные рубрики: PEPTIDE NANOTUBES
PIEZOELECTRIC PROPERTIES
WATER
MICROTUBES
Ключевые слова (''Своб.индексиров.''): peptide nanotubes--diphenylalanine--phase transition--cyclization--water
Аннотация: Self-assembled peptide diphenylalanine (NH2-Phe-Phe-COOH, FF) is one of the most important emergent functional materials, demonstrating wide range of fascinating physical and chemical properties including biocompatibility, chemical variability, exceptional rigidity, outstanding piezoelectric, pyroelectric and ferroelectric responses. Up to now, the phase transitions in FF nanotubes were investigated by scanning and transmission electron microscopy, atomic force microscopy, differential scanning calorimetry, thermogravimetry and mass spectroscopy. The Raman spectroscopy was implemented at room temperature only, and the microscopic details of these transitions remained unknown. In this work, the structural transformations in FF nanotubes at elevated temperatures (up to tubes destruction at 160 °C) were studied by Raman spectroscopy. Two structural transformations were observed in this region: hexagonal to orthorhombic transition at about 100 °C and the cyclization of FF molecules at about 150 °C. For the first time, these transformations were considered in the context of reconstruction of the water subsystem in the nanotubes, thus demonstrating the strong relation between the peptide tube and the state of the water inside. Using an effective frequency of nanotubes' lattice vibrations, we found that many effects observed earlier by other methods are induced by the variation of the water subsystem. The analysis of certain lines in the middle part of the Raman spectrum allowed us to describe the microscopic details of FF molecule cyclization. These results improve the understanding of the role of water in the origin of outstanding properties of FF nanotubes and thus promote developing new functional devices on their basis.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kovaleva E. A., Kuzubov A. A., Avramov P. V., Kholtobina A. S., Kuklin A. V., Tomilin F. N., Sorokin P. B.
Заглавие : A key role of tensile strain and surface termination in formation and properties of La0.7Sr0.3MnO3 composites with carbon nanotubes
Место публикации : Comput. Mater. Sci.: Elsevier, 2017. - Vol. 139. - P.125-131. - ISSN 09270256 (ISSN), DOI 10.1016/j.commatsci.2017.07.021
Примечания : Cited References: 39. - This work was supported by National Research Foundation of Republic of Korea under Grant No. NRF-2017R1A2B4004440 and the government contract of the Ministry of Education and Science of the Russian Federation to Siberian Federal University (Grant No. 16.1455.2017/PCh). The authors would like to thank Joint Supercomputer Center of RAS, Moscow; Center of Equipment for Joint Use of Siberian Federal University, Krasnoyarsk; and Information Technology Centre, Novosibirsk State University for providing the access to their supercomputers. P.B.S gratefully acknowledges the financial supports of the Ministry of Education and Science of the Russian Federation in the framework of Increase Competitiveness Program of NUST «MISiS» (No. К2-2017-001) and RFBR, according to the research project No. 16-32-60138 mol_a_dk. E.A. Kovaleva would also like to acknowledge the program of the President of Russian Federation for Leading Scientific Schools Support (Grant No. 2016 NSh-7559.2016.2).
Ключевые слова (''Своб.индексиров.''): carbon nanotubes--lsmo--interface--spin polarization
Аннотация: Atomic and electronic structure of LSMO-based composites with carbon nanotubes were studied by means of density functional theory with respect to the termination of LSMO surface. The deformation of the tubes caused by the lattice mismatch with the substrate leads to a major change in their electronic structure. The surface terminated with Mn-O layer provides much stronger interaction with carbon nanotubes than Sr-O terminated one does. The interaction with transition metal atoms is essential for spin polarization of the nanotube while no spin injection was observed for Sr-O-supported tubes. © 2017 Elsevier B.V.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Popov A. A., Vnukova N. G., Dudnik A. I., Samoylova N., Glushenko G. A.
Заглавие : Controlled synthesis of fullerenes and endohedral metallofullerenes in high frequency arc discharge
Место публикации : Fuller. Nanotub. Carbon Nanostruct.: Taylor and Francis, 2016. - Vol. 24, Is. 11. - P.675-678. - ISSN 1536383X (ISSN), DOI 10.1080/1536383X.2016.1207062
Примечания : Cited References: 16. - The work is supported by the Ministry of Education and Science of Russia (Russian-Japanese joined project, Agreement № 14.613.21.0010, ID RFMEFI61314X0010).
Ключевые слова (''Своб.индексиров.''): fullerene--endohedral metallofullerenes--high frequency arc discharge--pressure--mass spectrum
Аннотация: The article presents the high-frequency arc discharge setup operating in helium atmosphere and applicable for the syntheses of carbon condensate with different dispersion and structure, along with fullerenes and endohedral metallofullerenes. It also highlights how the change of helium pressure in chamber can control the amount and composition of products in carbon condensate. The setup can be applied for the purposes of analysis, for instance in order to obtain information about the process of fullerenes and endohedral met-allofullerenes formation. Also, the fact that the yield of higher fullerenes is increasing with the pressure rise, whereas the yield of endohedral metallofullerenes is decreasing suggests different formation mechanisms. © 2016 Taylor & Francis Group, LLC.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Popov A. K., Nefedov I. S., Myslivets S. A.
Заглавие : Hyperbolic carbon nanoforest for phase matching of ordinary and backward electromagnetic waves: Second harmonic generation
Место публикации : ACS Photonics: American Chemical Society, 2017. - Vol. 4, Is. 5. - P.1240-1244. - ISSN 23304022 (ISSN), DOI 10.1021/acsphotonics.7b00146
Примечания : Cited References: 14. - This material is based on work supported in part by the U.S. Army Research Laboratory through the U.S. Army Research Office under Grant Number W911NF-14-1-0619 and by the Russian Foundation for Basic Research under Grant RFBR 15-02-03959A.
Ключевые слова (''Своб.индексиров.''): backward electromagnetic waves--carbon nanotubes--hyperbolic metamaterials--second harmonic generation
Аннотация: We show that a deliberately engineered dispersive metamaterial slab can enable the coexistence and phase matching of ordinary fundamental and contra-propagating backward second harmonic electromagnetic waves. Energy flux and phase velocity are contra-directed in the backward waves, which is the extraordinary phenomenon that gives rise to unique nonlinear optical propagation processes. We demonstrate that frequencies, phase, and group velocities, as well as the losses inherent to the guided electromagnetic modes supported by such metamaterial, can be tailored to maximize the conversion of frequencies and to reverse the propagation direction of the generated second harmonic wave. Such a possibility, which is of paramount importance for nonlinear photonics, is proven using a numerical model describing the hyperbolic metamaterial made of carbon nanotubes standing on the metal surface. Extraordinary properties of the backward-wave second harmonic generation in the reflection direction and of the corresponding frequency doubling metareflector in the THz are investigated with a focus on the pulsed regime. © 2017 American Chemical Society.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Маркевич И. А., Селютин Г. Е., Дрокин, Николай Александрович, Беляев, Борис Афанасьевич
Заглавие : Синтез и электрофизические свойства композитов на основе сверхвысокомолекулярного полиэтилена и углеродных нанотрубок
Место публикации : Журн. СФУ. Техн. и технол. - 2018. - Т. 11, № 2. - С. 190-197. - ISSN 1999-494X, DOI 10.17516/1999-494X-0022; J. Sib. Fed. Univ. Eng. Technol.
Примечания : Библиогр.: 8. - Работа выполнена при поддержке Фонда содействия развитию малых форм предприятий в научно-технической сфере в рамках договора № 9594ГУ/2015 от 01.02.2016.
Ключевые слова (''Своб.индексиров.''): композиты--сверхвысокомолекулярный полиэтилен--углеродные нанотрубки--диэлектрическая проницаемость--проводимость--composites--ultrahigh-molecular-weight polyethylene--carbon nanotubes--dielectric permittivity--conductivity
Аннотация: Получены композиты на основе сверхвысокомолекулярного полиэтилена и углеродных нанотрубок методом смешивания компонентов в ксилоле при определенных температурах. Комплексные проводимости и диэлектрические проницаемости образцов материалов измерены в диапазоне частот от 100 Гц до 1 ГГц. Установлены условия синтеза как электропроводящих, так и диэлектрических композитов. При этом величина проводимости зависит не только от концентрации углеродных нанотрубок, но и от структуры их распределения в полимерной матрице, которая, в свою очередь, зависит от температурных условий получения композита.Composites based on ultrahigh-molecular-weight polyethylene and carbon nanotubes were obtained by mixing the components in xylene at certain temperatures. The complex conductivities and permittivities of the material samples were measured in the frequency range from 100 Hz to 1 GHz. The conditions for the synthesis of both electrically conducting and dielectric composites were established. The conductivity depends not only on the concentration of carbon nanotubes, but also on the structure of their distribution in the polymer matrix, which in turn depends on the temperature conditions for obtaining the composite.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Dudnik A. I., Drokin N. A., Vnukova N. G., Tomashevich E. V., Bondarev V. S.
Заглавие : Obtaining of hydroxylated fullerenes Y@C82OX(OH)Y, Y2@C82OX(OH)Y, Y2C2@C82OX(OH)Y and electrophysical characteristic of composite film based thereon
Место публикации : Fuller. Nanotub. Carbon Nanostruct. - 2018. - Vol. 26, Is. 12. - P.799-803. - ISSN 1536383X (ISSN), DOI 10.1080/1536383X.2018.1501559
Примечания : Cited References: 33. - We thank A.A. Popov and his team (The Leibniz Institute for Solid State and Materials Research, Dresden, Germany) for research conducted via mass-spectrometer MALDI-TOF Bruker BIFLEX TM III.
Ключевые слова (''Своб.индексиров.''): endohedral metallofullerene--impedance spectroscopy--polarization
Аннотация: The article presents, for the first time, the results of the research on composite film obtained from hydroxylated endohedral metallofullerenes (EMF) Y@C82, Y2@C82, with Y2C2@C82 and highest fullerenes as dopant. The composite film has been established to have electric conductivity and to be a ferroelectric with the value of residual polarization of ∼0.75 μC/cm2. The impedance spectroscopy of this sample allowed us to determine dispersion of dielectric permittivity and conductivity in the range of frequencies of 0.5 Hz–100 MHz. It is stated that the value of the high-frequency dielectric permittivity of films is ε′∞ = 2.8. However, with reduction in the electric field frequency, real and imaginary parts of ε increase to values ∼104–105. Such increase in dielectric permittivity is connected with increase in polarizing caused by accumulation of mobile electric charges (electrons of ions, protons) on boundaries of the structural defects of a film, which are divided by thin dielectric interlayers. The film is solid electrolyte with the ionic conductivity of ∼5 × 10−7 S/cm.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Isakova V. G., Osipova I. V., Dudnik A. I., Cherepakhin A. V., Zharikova N. V., Nemtsev I. V., Volochaev M. N.
Заглавие : Decoration of carbon nanomaterial powders with dispersed platinum metal particles
Коллективы : Center for Shared Use of the Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
Место публикации : Russ. J. Appl. Chem. - 2018. - Vol. 91, Is. 7. - P.1209-1216. - ISSN 1070-4272, DOI 10.1134/S1070427218070212. - ISSN 1608-3296(eISSN)
Примечания : Cited References: 22. - The study was performed with the support and equipment of the Center for Shared Use of the Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences.
Предметные рубрики: NANOPARTICLES
PALLADIUM
FULLERENE
ELECTRODE
NANOTUBES
OXIDATION
Ключевые слова (''Своб.индексиров.''): carbon nanomaterials--platinum metal nanoparticles--in situ one-step method
Аннотация: Carbon nanomaterials (fullerite, detonation nanodiamonds, Taunit, fullerenol, fullerene-containing black) were decorated with platinum group metal nanoparticles in situ in one step by low-temperature combustion (~250–270°С) of a powdered mixture of platinum metal acetylacetonate [Pt-M(асас)n, Pt-М = Pt(II), Pd(II), Rh(III), Ir(III), acac = CH3COCHCOCH3, n is the oxidation state of Pt-М] with carbon nanomaterials in air. As shown by thermal analysis, the process is based on thermal oxidative degradation of the organometallic complex, catalyzed by carbon nanomaterials, with oxidation (combustion) of the organic moiety and release of the metal into the condensed phase. The thermal process in an open system occurs in the glowing mode (210–250°С); the size of the nanoparticles formed is 7–30 nm. Under the conditions restricting the air access to the reaction mixture and free outflow of gaseous products formed by oxidation of acac ligands, the nanoparticle size decreases to 3–10 nm. The particle size depends on the metal amount in the initial powder mixture and on the support morphology.
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20.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Churilov G. N.
Заглавие : Two new discharges for production of fullerenes and nanotubes
Коллективы : International Winterschool on Electronic Properties of Novel Materials
Место публикации : Progress in fullerene research/ ed. H. Kuzmany [et al.]. - Singapore ; New Jersey ; London: World Scientific, 1994. - P.135-138. - ISBN 978-9810218874 (Шифр -292987024). - ISBN 981-02-1887-7
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