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    The physicochemical properties of polyhydroxyalkanoates with different chemical structures / T. G. Volova [et al.] // Polym. Sci. Ser. A. - 2013. - Vol. 55, Is. 7. - P. 427-437, DOI 10.1134/S0965545X13070080. - Cited References: 41 . - 11. - ISSN 0965-545X
   Перевод заглавия: Физико-химические свойства полигидроксиалканоатов с разной химической структурой

РУБ Polymer Science
Рубрики:
MICROBIAL SYNTHESIS
   RALSTONIA-EUTROPHA
   COMAMONAS-ACIDOVORANS
   AEROMONAS-HYDROPHILA
   POLY(3-HYDROXYBUTYRATE-CO-4-HYDROXYBUTYRATE)
   BIOSYNTHESIS
   COPOLYMERS
   POLY(3-HYDROXYBUTYRATE-CO-3-HYDROXYHEXANOATE)
   POLYMERS
Аннотация: A set of polyhydroxyalkanoates are synthesized, and a comparative study of their physicochemical properties is performed. The molecular masses and polydispersities of polyhydroxyalkanoates are found to be independent of their chemical structures. It is shown that the temperature characteristics and degrees of crystallinity of polyhydroxyalkanoates are affected by the chemical compositions of the monomers and their quantitative contents in the polymers. The incorporation of 4-hydroxybutyrate, 3-hydroxyvalerate, and 3-hydroxyhexanoate units into the chain of poly(3-hydroxybutyrate) decreases its melting point and thermal degradation temperature relative to these parameters of a homogeneous poly(3-hydroxybutyrate) sample (175 +/- 5A degrees C and 275 +/- 5A degrees C, respectively). The higher the content of the second monomer units in the poly(3-hydroxybutirate) chain, the greater the changes. The degrees of crystallinity of polyhydroxyalkanoate copolymers are generally lower than that of poly(3-hydroxybutyrate) (75 +/- 5%). The effect on the ratio of the amorphous and crystalline phases of the copolymer samples becomes more pronounced in the series 3-hydroxy-valerate-3-hydroxyhexanoate-4-hydroxybutyrate. The prepared samples exhibit different properties ranging from rigid thermoplastic materials to engineering elastomers.

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Держатели документа:
Russian Acad Sci, Siberian Branch, Inst Biophys, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Inst Fundamental Biol & Biotechnol, Krasnoyarsk 660041, Russia
Siberian State Technol Univ, Krasnoyarsk 660049, Russia
Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
MIT, Cambridge, MA 02139 USA;

Доп.точки доступа:
Volova, T. G.; Волова, Татьяна Григорьевна; Zhila, N. O.; Жила, Наталья Олеговна; Shishatskaya, E. I.; Шишацкая, Екатерина Игоревна; Mironov, P. V.; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Sukovatyi, A. G.; Суковатый, Алексей Григорьевич; Sinskey, A. J.
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Light passage through the polymer film of liquid crystal droplets with modified boundary conditions / V. A. Loiko [et al.] // Semiconductor Physics, Quantum Electronics and Optoelectronics. - 2013. - Vol. 16, № 1. - P. 185-189. - This work was performed under the aegis of the Integration Project and supported by the Belarusian Republican Foundation for Fundamental Research, Project No. F12SO-007
Кл.слова (ненормированные):
polymer dispersed liquid crystal -- transmittance -- scattering -- light modulation
Аннотация: A method to analyze coherent transmission coefficients and the small-angle light scattering structure of PDLC layer with homogeneous and inhomogeneous boundary conditions on the droplets surface is discussed. For PDLC films with inhomogeneous boundary conditions at the polymer -- liquid crystal interface, asymmetry of the angular structure of light scattering with respect to the polar angle is revealed. Besides, experimental results on transmittance are presented.

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Держатели документа:
B.I. Stepanov Institute of Physics, National Academy of Sciences of Belarus, Nezalezhnastsi ave., Minsk, 220072 Belarus
L.V. Kirensky Institute of Physics, Siberian Branch of the Russian Academy of Sciences Krasnoyarsk,660036, Russia

Доп.точки доступа:
Loiko, V. A.; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Konkolovich, A. V.; Miskevich, A. A.
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Domain structures in nematic liquid crystals on a polycarbonate surface / A. M. Parshin [и др.] // Int. J. Mol. Sci. - 2013. - Vol. 14, Is. 8. - P. 16303-16320, DOI 10.3390/ijms140816303 . - ISSN 1422-0067
Кл.слова (ненормированные):
liquid crystal -- domain -- polymer structure
Аннотация: Alignment of nematic liquid crystals on polycarbonate films obtained with the use of solvents with different solvations is studied. Domain structures occurring during the growth on the polymer surface against the background of the initial thread-like or schlieren texture are demonstrated. It is established by optical methods that the domains are stable formations visualizing the polymer surface structures. In nematic droplets, the temperature-induced transition from the domain structure with two extinction bands to the structure with four bands is observed. This transition is shown to be caused by reorientation of the nematic director in the liquid crystal volume from the planar alignment to the homeotropic state with the pronounced radial configuration of nematic molecules on the surface. The observed textures are compared with different combinations of the volume LC orientations and the radial distribution of the director field and the disclination lines at the polycarbonate surface.

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Доп.точки доступа:
Parshin, A. M.; Gunyakov, V. A.; Гуняков, Владимир Алексеевич; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Shabanov, V. F.; Шабанов, Василий Филиппович
}
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Spectral properties of photonic crystal structure with the polymer dispersed liquid crystal film as a defect layer : Сontributed paper / V. Ya. Zyryanov [et al.] // 12th Eur. Conf. Liq. Cryst. (ECLC-2013). - 2013. - Ст. PI.II

Материалы конференции,
Материалы конференции

Доп.точки доступа:
Zyryanov, V.Ya.; Зырянов, Виктор Яковлевич; Gunyakov, V. A.; Гуняков, Владимир Алексеевич; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Myslivets, S. A.; Мысливец, Сергей Александрович; Arkhipkin, V. G.; Архипкин, Василий Григорьевич; Shabanov, V. F.; Шабанов, Василий Филиппович; Lee, W.; European Conference on Liquid Crystals(12 ; 2013 ; Sept. ; 22-27)
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Small-angle light scattering and transmittance of polymer film, containing liquid crystal droplets with inhomogeneous boundary conditions / V. A. Loiko [et al.] // J. Quant. Spectrosc. Radiat. Transf. - 2012. - Vol. 113, Is. 18. - P. 315-322, DOI 10.1016/j.jqsrt.2012.03.026. - Cited References: 28 . - ISSN 0022-4073

РУБ Spectroscopy
Рубрики:
NEMATIC DROPLETS
Кл.слова (ненормированные):
Liquid crystals -- Light scattering -- Soft matter -- Composite materials -- Polymer-dispersed liquid crystal films
Аннотация: Light scattering by a monolayer of oriented liquid crystal (LC) droplets in polymer matrix is considered. A method for modeling transmittance and angular distribution of scattered light by a monolayer of LC droplets with cylindrical symmetry of the director configuration is developed. It is based on the anomalous diffraction and interference approximations. The internal structures of nematic LC droplets are calculated on base of the free energy minimization problem solution using the relaxation method. The results for monolayers of spherical LC droplets with homogeneous and inhomogeneous boundary conditions are obtained. It is shown that for monolayers containing droplets with inhomogeneous boundary conditions of the "tangential-normal" type there is an asymmetry of the angular structure of the transmitted light over the polar angle. (c) 2012 Elsevier Ltd. All rights reserved.

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Доп.точки доступа:
Loiko, V. A.; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Maschke, U.; Konkolovich, A. V.; Miskevich, A. A.; Conference on Electromagnetic and Light Scattering (13 ; 2011 ; Sept. ; 26-30 ; Taormina, Italy)
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Investigation of transmittance and small-angle light scattering by monolayer of liquid crystal droplets with modified boundary conditions / V. A. Loiko [et al.] // Mol. Cryst. Liquid Cryst. - 2012. - Vol. 561, Is. 1. - P. 194-202, DOI 10.1080/15421406.2012.687237. - Cited References: 24 . - ISSN 1542-1406

РУБ Crystallography
Рубрики:
NEMATIC DROPLETS
   ANOMALOUS DIFFRACTION
   APPROXIMATION
   FILM
Кл.слова (ненормированные):
Light modulation -- light scattering -- polymer dispersed liquid crystal -- optical transmittance
Аннотация: A numerical method for modelling transmittance and angular distribution of light scattered by a Polymer Dispersed Liquid Crystal (PDLC) film, containing droplets with inhomogeneous boundary conditions, is proposed. It is based on the anomalous diffraction approximation and an interference approximation. The internal structures of nematic LC droplets are calculated on the basis of the free energy minimization problem solution using the relaxation method. The results for a monolayer of spherical LC droplets with modified boundary conditions caused by the local increase of the concentration of surface-active ions at the polymer-LC interface are discussed.

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Доп.точки доступа:
Loiko, V. A.; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Konkolovich, A. V.; Misckevich, A. A.; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Maschke, U.; International Topical Meeting: Optics of Liquid Crystals (14th ; Sept 25 - Oct 1, 2011 ; Yerevan, Armenia)
}
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A thermospectral setup for evaluating the content of unbound components in microscopic samples of an epoxy polymer / N. S. Naumkin [et al.] // Instrum. Exp. Tech. - 2012. - Vol. 55, Is. 2. - P. 294-297, DOI 10.1134/S0020441212010198. - Cited References: 5. - This study was supported by the Center of Collective Use of the Krasnoyarsk Scientific Center (Siberian Branch, Russian Academy of Sciences), the Presidium of the Russian Academy of Sciences (project no. 27.1), the Department of Physical Sciences, Russian Academy of Sciences, (project no. 9.1), and the Siberian Branch, Russian Academy of Sciences (integration project no. 5). . - ISSN 0020-4412

РУБ Engineering, Multidisciplinary + Instruments & Instrumentation

Аннотация: A setup and a technique for optical measurements intended for evaluating the content of unbound compounds in an epoxy polymer are described. The principle of operation of the setup is based on measurements of the spectra of absorption of infrared (IR) radiation by condensed products of evaporation of unbound components. The needed mass of a sample is about 0.01 g. The results of measurements of the IR radiation absorption as a function of the concentrations of the mixture components-ED-22 epoxy resin, isomethyltetrahydrophthalic anhydride (hardener), and a cure promoter (N integral D-606/2)-are presented. The relative content of chemically unbound components in the structure of a polymer matrix is evaluated as a function of the hardener concentration, thus allowing determination of the stoichiometric ratio of the initial components of an epoxy mixture. The obtained results are compared to those obtained by the extraction method.

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Публикация на русском языке Термоспектральная установка для оценки содержания несвязанных компонентов в микрообразцах эпоксидного полимера [Текст] / Н. С. Наумкин [и др.] // Приборы и техн. эксперим. - М. : Наука, 2012. - № 2. - С. 155-158

Держатели документа:
[Naumkin, N. S.
Shestakov, N. P.
Ivanenko, A. A.
Shestakov, A. B.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
[Shestakov, N. P.
Ivanenko, A. A.] Russian Acad Sci, Kirenskii Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia
[Kargin, V. F.] Russian Acad Sci, Siberian Branch, Inst Chem & Chem Technol, Krasnoyarsk 660049, Russia

Доп.точки доступа:
Naumkin, N. S.; Shestakov, N. P.; Шестаков, Николай Петрович; Ivanenko, A. A.; Иваненко, Александр Анатольевич; Kargin, V. F.; Shestakov, A. B.
}
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Magnetic-field-induced structural transition in polymer-dispersed liquid crystals / A. M. Parshin [et al.] // Mol. Cryst. Liquid Cryst. - 2012. - Vol. 557, Is. 1. - P. 50-59, DOI 10.1080/15421406.2011.632237. - Cited References: 19. - This study was supported by the Presidium of the Russian Academy of Sciences (Project no. 24.1) and the Siberian Branch of the Russian Academy of Sciences (grant no. 43). . - ISSN 1542-1406

РУБ Crystallography
Рубрики:
FRANK CONSTANTS
   ELECTRIC-FIELD
   NEMATIC DROPS
   ANISOTROPY
   ALIGNMENT
   FILMS
   ORDER
Кл.слова (ненормированные):
Anchoring energy -- magnetic field -- polymer-dispersed liquid crystals -- structural transition -- temperature fluctuations
Аннотация: The structural transition occurring in droplets of nematic liquid crystals formed in a polymer in magnetic field is studied. The transition is caused by field-driven weakening of tangential surface anchoring and develops following two scenarios: bipolar structure/homogeneous structure or bipolar structure/radial structure. The first scenario suggests a cyclic transition occurring upon thermal fluctuations without field. The structural transition is considered within a model of the biaxial liquid crystal/polymer interface. The model describes tendency of the nematic director to align tangentially on a droplet's surface, normally under the action of flexoelectric polarization, and axially along the magnetic-field-imposed easy orientation axis.

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Держатели документа:
[Parshin, A. M.
Nazarov, V. G.
Zyryanov, V. Ya.
Shabanov, V. F.] Krasnoyarsk Sci Ctr, LV Kirensky Inst Phys, Krasnoyarsk, Russia

Доп.точки доступа:
Parshin, A. M.; Паршин, Александр Михайлович; Nazarov, V. G.; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Shabanov, V. F.; Шабанов, Василий Филиппович
}
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Polarizing properties of a stretched film of a polymer-dispersed liquid crystal with a surfactant dopant / M. H. Egamov [et al.] // J. Opt. Technol. - 2014. - Vol. 81, Is. 7. - P. 414-417, DOI 10.1364/JOT.81.000414. - Cited References: 17. - This work was carried out with the partial support of Grant 12-03-00816 of the Russian Foundation for Basic Research, Grants 24.32 and 24.29 of the Presidium of the Russian Academy of Sciences, and joint project 30 of the Siberian Section of the Russian Academy of Sciences (SO RAN), and a joint project of the SO RAN and the National Scientific Council of Taiwan. . - ISSN 1070-9762. - ISSN 1091-0786

РУБ Optics
Рубрики:
ANISOTROPY
Аннотация: The transmittance anisotropy of a composite polymer-liquid-crystal film has been studied as it varies with the degree to which it is elongated. The composite film includes polyvinyl alcohol, the nematic liquid crystal 4-n-pentyl-4'-cyanobiphenyl, and the surfeiting cetyltrimethylammonium bromide, which initiates homeotropic adhesion of the nematic to the surface of the polymer. It is shown that, when the film is uniaxially stretched, the transmittance of the orthogonally polarized component of directly transmitted radiation and accordingly the degree of polarization abruptly increase, reaching saturation when it is stretched to twice its length. Such variation of the film's macroscopic optical properties can be caused by an orientational-structural transition to a homogeneous configuration of the director in deformed droplets of the nematic and makes it possible to substantially improve the optical characteristics of light polarizers based on such composite media. (C) 2014 Optical Society of America.

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Публикация на русском языке Поляризующие свойства вытянутой пленки капсулированного полимером жидкого кристалла с примесью сурфактанта [Текст] / М. Х. Эгамов [и др.] // Оптич. журн. : Санкт-Петербургский НИУ ИТМО, 2014. - Т. 81 № 7. - С. 67-71

Доп.точки доступа:
Egamov, M. H.; Эгамов, Мухтор Хасанович; Gerasimov, V. P.; Герасимов, Виктор Петрович; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Loiko, V. A.; Russian Foundation for Basic Research [12-03-00816]; Presidium of the Russian Academy of Sciences [24.32, 24.29]; Siberian Section of the Russian Academy of Sciences (SO RAN); SO RAN; National Scientific Council of Taiwan
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10.

Electrospinning of polyhydroxyalkanoate fibrous scaffolds: effects on electrospinning parameters on structure and properties / T. . Volova [et al.] // J. Biomater. Sci.-Polym. Ed. - 2014. - Vol. 25, Is. 4. - P. 370-393, DOI 10.1080/09205063.2013.862400. - Cited References: 52. - This study was financially supported by Project 'Biotechnologies of novel biomaterials: innovative biopolymers and devices for biomedicine' (Agreement No. 1 of 15.02.2013 to Agreement No. 11.G34.31.0013) in accordance with Resolution No. 220 of the Government of the Russian Federation of April 9, 2010, 'On measures designed to attract leading scientists to the Russian institutions of higher learning' and Grant of the RF President for supporting young Doctors of Sciences No. MD-3112.2012.4. . - ISSN 0920-5063. - ISSN 1568-5624

РУБ Engineering, Biomedical + Materials Science, Biomaterials + Polymer Science
Рубрики:
TISSUE ENGINEERING APPLICATIONS
   FIBER MATS
   POLY 3-HYDROXYBUTYRATE
   POLY(3-HYDROXYBUTYRATE-CO-3-HYDROXYVALERATE)
   BIOCOMPATIBILITY
   PROLIFERATION
   FABRICATION
   NANOFIBERS
   COPOLYMERS
   MEMBRANES
Кл.слова (ненормированные):
electrospinning -- polyhydroxyalkanoates -- ultrafine fibers -- physical-mechanical properties -- fibroblast cells
Аннотация: IIn this study, electrospinning was used to prepare ultrafine fibers from PHAs with different chemical compositions: P(3HB) and copolymers: P(3HB-co-4HB), P(3HB-co-3HV), and P(3HB-co-3HHx). The main process parameters that influence ultrafine fiber diameter and properties (polymer concentration, solution feeding rate, working distance, and applied voltage) have been investigated and their effects evaluated. The study revealed electrospinning parameters for the production of high-quality ultrafine fibers and determined which parameters should be varied to tailor the properties of the products. This study is the first to compare biological and physical-mechanical parameters of PHAs with different chemical compositions as dependent upon the fractions of monomers constituting the polymers and ultrafine fiber orientation. Mechanical strength of aligned ultrafine fibers prepared from different PHAs is higher than that of randomly oriented ones; no significant effect of ultrafine fiber orientation on surface properties has been found. None of the fibrous scaffolds produced by electrospinning from PHAs had any adverse effects on attachment, growth, and viability of NIH 3T3 mouse fibroblast cells, and all of them were found to be suitable for tissue engineering applications.

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Держатели документа:
Russian Acad Sci, Inst Biophys, Siberian Branch, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Inst Fundamental Biol & Biotechnol, Krasnoyarsk 660041, Russia
Russian Acad Sci, LV Kirenskii Inst Phys, Siberian Branch, Krasnoyarsk 660036, RussiaИФ СО РАН;

Доп.точки доступа:
Volova, T.; Волова, Татьяна Григорьевна; Goncharov, D.; Sukovatyi, A. G.; Суковатый, Алексей Григорьевич; Shabanov, A. V.; Шабанов, Александр Васильевич; Nikolaeva, E.; Shishatskaya, E.; Project 'Biotechnologies of novel biomaterials: innovative biopolymers and devices for biomedicine' [1, 11.G34.31.0013]; Government of the Russian Federation [220]; RF President for supporting young Doctors of Sciences [MD-3112.2012.4]
}
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