Библиотека института физики им. Л.В. Киренского СО РАН

Главная

Базы данных

Труды сотрудников ИФ СО РАН - результаты поиска

Вид поиска

Каталог книг и брошюр библиотеки ИФ СО РАН

Каталог журналов библиотеки ИФ СО РАН

Труды сотрудников ИФ СО РАН

Область поиска

Формат представления найденных документов:
полный	информационный	краткий

Отсортировать найденные документы по:
автору	заглавию	году издания	типу документа

Поисковый запрос: (<.>A=Kirik, S. D.$<.>)

Общее количество найденных документов : 9
Показаны документы с 1 по 9

Golovnev, N. N.
Enrofloxacinium citrate monohydrate: Preparation, crystal structure, thermal stability and IR-characterization / N. N. Golovnev, A. D. Vasiliev, S. D. Kirik // J. Mol. Struct. - 2012. - Vol. 1021. - P. 112-117, DOI 10.1016/j.molstruc.2012.04.059. - Cited References: 22. - The authors are grateful to the Ministry of Education and Science (Government Contracts # 02.740.11.0629) for the financial support of the investigation. . - ISSN 0022-2860

РУБ Chemistry, Physical
Рубрики:
COCRYSTAL
   ANTIBACTERIAL
   BEHAVIOR
   STATE
   ACID
Кл.слова (ненормированные):
Enrofloxacin -- Citric acid -- Crystal structure -- IR spectra -- Thermal analysis
Аннотация: Enrofloxacinium citrate monohydrate (I), C19H 23FN3O3+В·C6H7O7- В·H2O, [C19H22FN3O3 - enrofloxacin, EnrH] has been crystallized from the mutual solution of citric acid and enrofloxacin in ambient conditions. The colorless crystals have been investigated using X-ray single crystal and powder techniques, and characterized by differential scanning calorimetry, thermogravimetry and infrared spectroscopy. The obtained compound can be considered as a salt with enrofloxacinium in the role of a cation and citrate as an anion. The ions ratio equals to 1:1. The compound crystallizes in the triclinic lattice with a = 9.0489(8) A, b = 9.6531(8) A, c = 14.913(1) A, ? = 98.813(1)В°, ? = 92.029(1)В°, ? = 91.013(1)В°, Z = 2, V = 1286.1(2) A3, S.G. P1?. The crystal structure determination reveals the importance of inter- and intramolecular interactions in the crystal formation. The EnrH2+andH3Cit- molecular ions are packed in alternating layers with water molecules inserted into the citrate layers. A citrate ion in the layer is linked via H-bondings with two adjacent ones and three water molecules. Enrofloxacinium cations are packaged by means of a benched mode and every cation is linked by three intermolecular thymus type H-bondings with nitrogens of adjacent cations and by two links with the oxygen of the citrate ions. The infrared spectra gave the evidence of H-bonding formation in the obtained salt. The ?-stacking interactions are observed between the aromatic cycles of the adjacent cations which are located in an antiparallel style in a layer. В© 2012 Elsevier B.V. All rights reserved.

Смотреть статью,
Scopus,
WoS,
Читать в сети ИФ
Держатели документа:
Siberian Federal University, Svobodny Ave. 79, Krasnoyarsk 660041, Russian Federation
Kirensky Institute of Physics SB RAS, Krasnoyarsk 660036, Russian Federation
Institute of Chemistry and Chemical Technology SB RAS, Krasnoyarsk 660036, Russian Federation

Доп.точки доступа:
Vasiliev, A. D.; Васильев, Александр Дмитриевич; Kirik, S. D.; Головнёв, Николай Николаевич
}
Найти похожие

    Kirik, S. D.
    Monitoring MCM-41 synthesis by X-ray mesostructure analysis / S. D. Kirik, V. A. Parfenov, S. M. Zharkov // Micropor. Mesopor. Mater. - 2014. - Vol. 195. - P. 21-30, DOI 10.1016/j.micromeso.2014.04.012. - Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025. . - ISSN 1387-1811. - ISSN 1873-3093
   Перевод заглавия: Контроль синтеза МСМ-41 с помощью рентгеновского мезоструктурного анализа

РУБ Chemistry, Applied + Chemistry, Physical + Nanoscience & Nanotechnology + Materials Science, Multidisciplinary
Рубрики:
ORDERED MESOPOROUS MATERIALS
   ORDERED MESOPOROUS MATERIALS
   IN-SITU
   POWDER DIFFRACTION
   SILICA/SURFACTANT COMPOSITES
   ELECTRON-MICROSCOPY
   MOLECULAR-SIEVES
   STABLE MCM-41
   SILICA
   ADSORPTION
Кл.слова (ненормированные):
Hydrothermal stability -- MCM-41 -- Mesostructure -- TEM -- X-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.

Смотреть статью,
Scopus,
WoS,
Читать в сети ИФ
Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Inst Chem & Chem Technol SB RAS, Krasnoyarsk 660036, Russia
Kirensky Inst Phys SB RAS, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Parfenov, V. A.; Zharkov, S. M.; Жарков, Сергей Михайлович
}
Найти похожие

Manufacturing solution for producing cobalt-ferrite films [Текст] / T. N. Patrusheva [et al.] // Chem. Mater. Eng. - 2014. - Vol. 2(2). - P. 33 - 36DOI 10.13189/cme.2014.020202
Аннотация: An extraction-pyrolytic technique and its usage for obtaining pure products from secondary manufacturing solutions are considered in this paper. Nanostructure ferrite thin films were prepared using the extraction-pyrolytic technique. It was shown that the extraction from modeling liquid of waste solution allows obtaining the pure single phase product. Fe2CoO4 magnetic films with grain sizes 18–20 nm were obtained by cycling pyrolysis of wet films deposited by the spin coating technique.

Смотреть статью,
Читать в сети ИФ

Доп.точки доступа:
Patrusheva, T. N.; Патрушева, Тамара Николаевна; Podorojnyak, S. A.; Polyakova, K. P.; Полякова, Клавдия Павловна; Kirik, S. D.; Menshikov, V. V.; Levchenko, S. I.; Patrushev, V. V.; Adrianova, M. A.; Gerasimova, G. E.
}
Найти похожие

Template synthesis of CMK-3 nanostructured carbon material and study of its properties / I. V. Ponomarenko [et al.] // Glass Phys. Chem. - 2014. - Vol. 40, Is. 1. - P. 79-87, DOI 10.1134/S1087659614010180 . - ISSN 1087-6596
Кл.слова (ненормированные):
adsorption of N2 -- CMK-3 mesostructured carbon -- mesoporous mesostructured silicates -- SBA-15 -- template synthesis -- transmission electron microscopy -- X-ray diffraction
Аннотация: Mesostructured carbon has been obtained by template synthesis. SBA-15 mesostructured silicate has been used as a template. The effect of the properties of a template on the ordering of a replica has been studied. It has been shown with the use of X-ray diffraction, gas adsorption, and electron microscopy that there are evident correlations of the conditions of synthesis of a template with the ordering of a carbon replica, which can be guided by the synthesis of materials. The ordering of a replica significantly depends on the mesopore volume of the initial template and thickness of the pore wall. One should use templates with the highest possible mesopore volume and minimal wall thickness to obtain highly ordered replicas. These templates can be prepared during the treatment of synthesized materials at temperatures close to 100 C. It has been determined that, when there is SBA-15, the presence of micropores is a necessary condition for the preparation of carbon replicas that retain the structure of the template. © 2014 Pleiades Publishing, Ltd.

Scopus,
Читать в сети ИФ
Держатели документа:
Institute of Chemistry and Chemical Engineering, Russian Academy of Sciences, Siberian Branch, Akademgorodok 50/24, Krasnoyarsk 660036, Russian Federation
Siberian Federal University, pr. Svobodnyi 79, Krasnoyarsk 660049, Russian Federation

Доп.точки доступа:
Ponomarenko, I. V.; Parfenov, V. A.; Zaitseva, Y. N.; Zharkov, S. M.; Жарков, Сергей Михайлович; Kirik, S. D.
}
Найти похожие

New bismuth borophosphate Bi4BPO10: Synthesis, crystal structure, optical and band structure analysis / N. A. Babitsky [et al.] // Mater. Chem. Phys. - 2015. - Vol. 163. - P. 286-292, DOI 10.1016/j.matchemphys.2015.07.042. - Cited References: 32. - The study was performed with the financial support of the Ministry of Science and Education of the Russian Federation, Projects 3049, 3098, item 1025, "Fund for Assistance to Small Innovative Enterprises in Science and Technology" (Grant program "UMNIK" 2013 II half GU1/2014), ICDD Grant-in-Aid, #93-10 . - ISSN 0254-0584

РУБ Materials Science, Multidisciplinary
Рубрики:
INITIO MOLECULAR-DYNAMICS
   AUGMENTED-WAVE METHOD
   POWDER DATA
   SYSTEM
   PHASES
Кл.слова (ненормированные):
Inorganic compounds -- Crystal growth -- Crystal structure -- Band-structure
Аннотация: New bismuth borophosphate Bi4BPO10 was obtained by spontaneous crystallization from the melt of correspondent composition at 804 °C. Crystal structure with orthorhombic lattice parameters: a = 22.5731(3) Å, b = 14.0523(2) Å, c = 5.5149(1) Å, V = 1749.34(4), Z = 8, SG Pcab was determined by X-ray powder diffraction technique. The [Bi2O2]2+ -layers, which are typical for bismuth oxide compounds, transform into cationic endless strips of 4 bismuth atoms width directed along the c-axis in Bi4BPO10. The strips combining stacks are separated by flat triangle [BO3]3- -anions within stacks. Neighboring stacks are separated by tetrahedral [PO4]3--anions and shifted relatively to each other. Bismuth atoms are placed in 5-7 vertex oxygen irregular polyhedra. Bi4BPO10 is stable up to 812 °C, then melts according to the peritectic law. The absorption spectrum in the range 350-700 nm was obtained and the width of the forbidden band was estimated as 3.46 eV. The band electronic structure of Bi4BPO10 was modeled using DFT approach. The calculated band gap (3.56 eV) is in good agreement with the experimentally obtained data. © 2015 Elsevier B.V. All rights reserved.

Смотреть статью,
Scopus,
WOS,
Читать в сети ИФ
Держатели документа:
Siberian Federal University, 79 Svobodny Av, Krasnoyarsk, Russian Federation
Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Babitsky, N. A.; Leshok, D. Y.; Mikhaleva, N. S.; Kuzubov, A. A.; Кузубов, Александр Александрович; Zhereb, V. P.; Kirik, S. D.
}
Найти похожие

Transparent conductive ITO coatings obtained by pyrolysis of metal extracts / T. N. Patrusheva [et al.] // J. Appl. Chem. Sci. Int. - 2015. - Vol. 3, Is. 1. - P. 21-28 . - ISSN 2395-3705
Кл.слова (ненормированные):
Indium-tin oxide -- thin films -- extraction-pyrolysis technique -- liquid precursors -- nanocrystalline structure
Аннотация: Thin films of indium-tin oxide (ITO) have been prepared by pyrolysis of liquid organic-extracts of indium and tin. The films were deposited on glass substrate in the atmospheric condition. Extraction-pyrolytic method adopted here uses cheap starting materials and provides the required stoichiometric ratio by mixing the stable liquid precursors in appropriate concentration. Thermal decomposition processes are induced in the narrow temperature range of 350–400°C. The zirconium-yttrium oxide (ZYO) sublayer was deposited on glass substrate in advance to provide homo epitaxial growth. This would induce reduction in intrinsic stress of the films due to matching in thermal expansion coefficient with ITO film. XPS studies showed the absence of impurity elements in these extraction-pyrolytic technique derived ITO films and the spectra is quite similar to that for ITO films deposited in vacuum environment. ITO film has a nanocrystalline structure with grain size of about 6 nm.

Смотреть статью

Доп.точки доступа:
Patrusheva, T. N.; Патрушева, Тамара Николаевна; Snezhko, N. Yu.; Belousov, A. L.; Rizhenkov, A. V.; Mikhlin, Y. L.; Михлин, Юрий Леонидович; Kirik, S. D.; Bondarenko, G. N.; Бондаренко, Галина Николаевна; Zharkov, S. M.; Жарков, Сергей Михайлович; Romanov, A. A.
}
Найти похожие

    Пленки аморфного и кристаллического оксида никеля, полученные экстракционно-пиролитическим методом для электрохромных ячеек / А. Л. Белоусов [и др.] // Хим. технол. - 2019. - Т. 20, № 5. - С. 215-221, DOI 10.31044/1684-5811-2019-20-5-215-221. - Библиогр.: 8 . - ISSN 1684-5811
   Перевод заглавия: Films of amorphous and crystalline nickel oxide, produced by extraction-pyrolitic method for electrochromic cells
Кл.слова (ненормированные):
экстракты никеля -- экстракционно-пиролитическая технология -- тонкие пленки -- отжиг -- электрохромная ячейка -- nickel extract -- extraction-pyrolitic technology -- thin film -- annealing -- electrochromic cell
Аннотация: Представлены исследования тонких пленок оксида никеля, полученных экстракционно-пиролитическим методом на стеклянных и кварцевых подложках при температурах 380-600 °С. Пленки охарактеризованы методами атомно-силовой микроскопии и рентгеновской дифракции. Показано, что на стекле формируются аморфные, а на кварце - кристаллические пленки оксида никеля. Размер зерна в пленках зависит от температуры отжига, при этом повышенные температуры отжига приводят к рекристаллизации и снижению размера зерна в пленках NiO от 130 до 35 нм.
Study results of thin films of nickel oxide, produced by the extraction-pyrolitic method on glass and quartz substrates at temperatures 380-600 °С are presented. The film characteristics were obtained by the methods of atomic-force microscopy and X-ray diffraction. It has been found out that amorphous films are formed on glass and crystalline ones of nickel oxide are formed on quartz. Grain dimensions in the films depend on annealing temperature.

РИНЦ,
Читать в сети ИФ

Переводная версия Amorphous and Crystalline Nickel Oxide Films Obtained by the Extraction-Pyrolysis Method for Electrochromic Cells [Текст] / A. L. Belousov, T. N. Patrusheva, A. A. Karacharov [et al.] // Theor. Found. Chem. Eng. - 2020. - Vol. 54 Is. 4.- P.699-705

Держатели документа:
Балтийский государственный технический университет Военмех им. Д. Ф. Устинова
Институт общей и неорганической химии РАН
Институт физики им. Киренского СО РАН
Институт химии и химической технологии СО РАН
Сибирский федеральный университет

Доп.точки доступа:
Белоусов, А.Л.; Belousov A.L.; Патрушева, Т.Н.; Patrusheva T.N.; Карачаров, А.А.; Karacharov A.A.; Иваненко, Александр Анатольевич; Ivanenko, A. A.; Кирик, С.Д.; Kirik S.D.; Холькин, А.И.; Kholkin A.I.
}
Найти похожие

Amorphous and Crystalline Nickel Oxide Films Obtained by the Extraction-Pyrolysis Method for Electrochromic Cells / A. L. Belousov, T. N. Patrusheva, A. A. Karacharov [et al.] // Theor. Found. Chem. Eng. - 2020. - Vol. 54, Is. 4. - P. 699-705, DOI 10.1134/S0040579520040041. - Cited References: 8. - This work was performed as part of the program "Research and Development for the Priority Areas of the Russian Science-and-Technology Sector for 2014-2020"; Grant Agreement no. 075-15-2019-1843; the Project Unique Identifier RFMEFI60719X0307 . - ISSN 0040-5795. - ISSN 1608-3431

РУБ Engineering, Chemical
Рубрики:
NIO THIN-FILMS
Кл.слова (ненормированные):
nickel extract -- extraction-pyrolysis technology -- thin film -- annealing -- electrochromic cell
Аннотация: This paper reports studies of thin films of nickel oxide obtained by the extraction–pyrolysis method on glass and quartz substrates at temperatures of 380–600°C. The films have been characterized by atomic force microscopy and X-ray diffraction. It is shown that amorphous and crystalline nickel oxide films are formed on the glass. The grain size depends on the annealing temperature, while increased annealing temperatures lead to recrystallization and a decrease in the grain size in NiO films from 130 to 35 nm.

Смотреть статью,
Scopus,
WOS,
Читать в сети ИФ

Публикация на русском языке Пленки аморфного и кристаллического оксида никеля, полученные экстракционно-пиролитическим методом для электрохромных ячеек [Текст] / А. Л. Белоусов [и др.] // Хим. технол. - 2019. - Т. 20 № 5. - С. 215-221

Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Baltic State Tech Univ VOENMEX, St Petersburg 190005, Russia.
Russian Acad Sci, Siberian Branch, Inst Chem & Chem Technol, Krasnoyarsk 660036, Russia.
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.
Russian Acad Sci, Kurnakov Inst Gen & Inorgan Chem, Moscow 119991, Russia.

Доп.точки доступа:
Belousov, A. L.; Patrusheva, T. N.; Karacharov, A. A.; Ivanenko, A. A.; Иваненко, Александр Анатольевич; Kirik, S. D.; Khol'kin, A. I.; program "Research and Development for the Priority Areas of the Russian Science-and-Technology Sector for 2014-2020" [075-15-2019-1843]; [RFMEFI60719X0307]
}
Найти похожие

Magnetic properties of nanoparticles synthesized on the base of MCM-41 / Komogortsev S.V., Iskhakov R.S., Chekanova L.A., Denisova E.A. // Moscow Int. Symp. on Magnet. (MISM-2008) : June 20-25, 2008, Moscow : book of abstract. - 2008. - Ст. 22PO-8-49. - p. 302. - Библиогр.: 2. - Support by Russian program “Development of Science in High School” (2006-2008)–RNP.2.1.1.7376; the grant RFBR 07-02-01172-а; National Science Fund (2008, PhD RAS) are acknowledged

Читать в сети ИФ

Доп.точки доступа:
Komogortsev, S. V.; Комогорцев, Сергей Викторович; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Chekanova, L. A.; Чеканова, Лидия Александровна; Denisova, E. A.; Денисова, Елена Александровна; Balaev, D. A.; Балаев, Дмитрий Александрович; Patrusheva, T. N.; Патрушева, Тамара Николаевна; Kirik, S. D.; Khomchenko, A. S.; Moscow International Symposium on Magnetism(4 ; 2008 ; Jun. ; Moscow); Московский государственный университет им. М.В. Ломоносова; Российский фонд фундаментальных исследований
}
Найти похожие